scholarly journals Colorimetric Determination of Urinary Creatinine in Proteinuria Patients by Chromaticity Analysis of Gold Nanoparticle Colloidal Solutions

2020 ◽  
Vol 36 (12) ◽  
pp. 1495-1500
Author(s):  
Chutiparn LERTVACHIRAPAIBOON ◽  
Akira BABA ◽  
Kazunari SHINBO ◽  
Keizo KATO
Keyword(s):  
Gold Nanoparticle ◽  
Colorimetric Determination ◽  
Colloidal Solutions ◽  
Urinary Creatinine

Synthesis of 3,4-diaminobenzenethiol and its application in gold nanoparticle-based colorimetric determination of copper ions

RSC Advances ◽  
2016 ◽  
Vol 6 (107) ◽  
pp. 105119-105124 ◽  
Author(s):  
Chi Zhang ◽  
Li-Qiang Lu ◽  
Pan Deng ◽  
Xi-Ke Tian ◽  
Ming-Yang Liu ◽  
...  
Keyword(s):  
Gold Nanoparticle ◽  
Benzene Ring ◽  
Functional Groups ◽  
Copper Ions ◽  
Colorimetric Determination ◽  
Determination Of Copper

3,4-Diaminobenzenethiol can react with AuNPs via a strong covalent Au–S bond. The exposed amino functional groups on the benzene ring from neighboring AuNPs could bind to copper ions, resulting in AuNP aggregation.

Low-Cost Synthesis of Gold Nanoparticles from Reused Traditional Gold Leaf and its Application for Sensitive and Selective Colorimetric Sensing of Creatinine in Urine

2020 ◽  
Vol 16 (3) ◽  
pp. 287-297
Author(s):  
Arjnarong Mathaweesansurn ◽  
Nathawut Choengchan ◽  
Putthiporn Khongkaew ◽  
Chutima M. Phechkrajang
Keyword(s):  
Gold Nanoparticles ◽  
Limit Of Detection ◽  
Low Cost ◽  
Poly Vinyl Alcohol ◽  
Colorimetric Determination ◽  
Au Nps ◽  
Urinary Creatinine ◽  
Gold Leaf ◽  
Colorimetric Response

Background: Gold nanoparticles (Au NPs) are normally prepared using standard gold (III) trichloride which is much expensive and irritant. This work is aimed at demonstrating simple and low-cost synthesis of Au NPs from the reused traditional gold leaf which is cost-free and less toxic. Methods: The reused gold leaf was donated by the local temple. It was digested and used as the precursor for the preparation of the Au NPs by Turkevich method. Poly (vinyl alcohol) (PVA) was employed as a stabilizer. The as-prepared Au NPs were applied for the colorimetric determination of creatinine in urine without any sample pretreatment. Results: Long-term stability of the gold colloids was achieved for at least 3 months. Morphology and purity of the as-prepared Au NPs were the same as the ones prepared from standard gold (III) salt and standard gold foil. Colorimetric response of the Au NPs was linear to the standard creatinine up to 200 mg L-1. The limit of detection (0.16 mg L-1 or 1.41 μM) was enough sensitive for urinary creatinine detection in patients with kidney disease. Good recoveries (97-108%) and fast analysis time (3 min) were achieved. The developed method was successfully validated against the HPLC method. Conclusion: Facile and cost-effective synthesis of the Au NPs from the reused traditional gold leaf, was accomplished. The as-prepared Au NPs were successfully applied for the determination of urinary creatinine with high sensitivity and selectivity.

Colorimetric determination of copper(II) using a polyamine-functionalized gold nanoparticle probe

2015 ◽  
Vol 182 (9-10) ◽  
pp. 1677-1683 ◽  
Author(s):  
Yuanfu Zhang ◽  
Rui Li ◽  
Qingwang Xue ◽  
Haibo Li ◽  
Jifeng Liu
Keyword(s):  
Gold Nanoparticle ◽  
Colorimetric Determination ◽  
Determination Of Copper

A Method for the Colorimetric Determination of β-Glucuronidase in Urine, Serum, Tissue; Assay of Enzymatic Activity in Health and Disease

1959 ◽  
Vol 36 (2) ◽  
pp. 193-201 ◽  
Author(s):  
Julius A. Goldbarg ◽  
Esteban P. Pineda ◽  
Benjamin M. Banks ◽  
Alexander M. Rutenburg
Keyword(s):  
Enzymatic Activity ◽  
Colorimetric Determination ◽  
Health And Disease ◽  
Urine Serum

Colorimetric Determination of Fluoride in Drinking Groundwater using a Polymeric Zirconium Complex of 5-(2-Carboxyphenylazo)-8-Hydroxyquinoline

2013 ◽  
Vol 12 (7) ◽  
pp. 460-465
Author(s):  
Sameer Amereih ◽  
Zaher Barghouthi ◽  
Lamees Majjiad
Keyword(s):  
Drinking Water ◽  
Detection Limit ◽  
Complex Formation ◽  
Molar Absorptivity ◽  
Colorimetric Determination ◽  
Zirconium Complex ◽  
Reliable Determination ◽  
Percentage Recovery ◽  
Quantitation Limit

A sensitive colorimetric determination of fluoride in drinking water has been developed using a polymeric zirconium complex of 5-(2-Carboxyphenylazo)-8-Hydroxyquinoline as fluoride reagents. The method allowed a reliable determination of fluoride in range of (0.0-1.5) mg L-1. The molar absorptivity of the complex formation is 7695 ± 27 L mol-1 cm-1 at 460 nm. The sensitivity, detection limit, quantitation limit, and percentage recovery for 1.0 mg L-1 fluoride for the proposed method were found to be 0.353 ± 0.013 μg mL-1, 0.1 mg L-1, 0.3 mg L-1, and 101.7 ± 4.1, respectively.

Colorimetric Determination of Amoxicillin in Pure and some Pharmaceutical Formulations Via Reaction with Potassium Permanganate as Oxidant Reagent

2019 ◽  
Vol 10 (02) ◽  
Author(s):  
Abbas Shebeeb Al-kadumi ◽  
Sahar Rihan Fadhel ◽  
Mohammed Abdullah Ahmed ◽  
Luma Amer Musa
Keyword(s):  
Potassium Permanganate ◽  
Pharmaceutical Preparations ◽  
Pharmaceutical Formulations ◽  
Atomic Emission ◽  
Basic Medium ◽  
Photometric Method ◽  
Colorimetric Determination ◽  
Spectrophotometric Methods ◽  
Label Claim

We proposed two simple, rapid, and convenient spectrophotometric methods are described for the determination of Amoxicillin in bulk and its pharmaceutical preparations. They are based on the measurement of the flame atomic emission of potassium ion (in first method) and colorimetric determination of the green colored solution for manganite ion at 610 nm formed after reaction of Amoxicillin with potassium permanganate as oxidant agent (in the second method) in basic medium. The working conditions of the methods were investigated and optimized. Beer's law plot showed a good correlation in the concentration range of 5-45 μg/ml. The detection limits and relative standared deviations were (2.573, 2.814 μg/ml) (2.137, 2.498) for the flame emission photometric method and (1.844, 2.016 μg/ml) (1.645,1.932) for colorimetric methods for capsules and suspensions respectively. The methods were successfully applied to the determination of Amoxicillin in capsules and suspensions, and the obtained results were in good agreement with the label claim. No interference was observed from the commonly encountered additives and expectancies.

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