scholarly journals Preparation and Characterization of Carbon Foam Derived from Fine Coal and Phenolic Resin

2018 ◽  
Vol 16 (3) ◽  
pp. 243
Author(s):  
Dodi Irwandi ◽  
Zainal Alim Mas’ud ◽  
Komar Sutriah ◽  
Muhammad Khotib

Carbon foam from fine coal and phenolic resin mixture had been prepared by heating in nitrogen atmosphere. The composition of fine coal in a mixture was 30, 35, 40, 45 and 50%. Physical and mechanical characters of carbon foam that were determined from each of these compositions were density, porosity, compressive strength, and oxidation resistance and thermal insulation. Microstructure was observed by scanning electron microscope (SEM). Thermal insulation was tested using an insulation index approach with Styrofoam for comparison. The result showed that the density and compressive strength were proportional to the composition, otherwise, the porosity. Oxidation resistance that was up to 45% composition still showed proportional value. Microstructure observations showed an irregular distribution of pore and uninform diameter. Insulation index of 34 to 50 °C showed almost the same values of all compositions and greater than styrofoam up to 50-150% which mean carbon foam had a better thermal insulation properties than styrofoam.

2009 ◽  
Vol 21 ◽  
pp. S121-S123 ◽  
Author(s):  
Xuefei ZHAO ◽  
Shiquan LAI ◽  
Hongzha LIU ◽  
Lijuan GAO

2010 ◽  
Vol 96 ◽  
pp. 141-144 ◽  
Author(s):  
Ming Xing Ai ◽  
Li Qiang Cao ◽  
Xiao Long Zhao ◽  
Zhen Yu Xiang ◽  
Xiang Yong Guo

The polyurethane rigid foam/expanded perlite thermal insulation composites (PPC) have been prepared by mixing the two-component polyurethane and expanded perlite. The effects of proportioning of constituents on the mechanical and thermal properties of PPC were investigated. The results showed the compressive strength of PPC was improved and good heat-insulating was achieved, which would promote the application of polyurethane rigid foam and expanded perlite in buildings.


Materials ◽  
2019 ◽  
Vol 12 (8) ◽  
pp. 1213 ◽  
Author(s):  
Alei Dang ◽  
Zhao Zhao ◽  
Chen Tang ◽  
Chenglin Fang ◽  
Siyuan Kong ◽  
...  

A novel high-performance carbon foam (CF) was fabricated through the addition of phenolic resin (PR) into a coal tar pitch (CTP) based precursor. The effects of mass fraction of a PR additive on the crystalline structures, morphologies, compressive strength (σ) and thermal conductivity (λ) of resultant CF material were investigated systematically. Characterization showed a strong dependence of CF’s performance from the composition and optical texture of the precursor, which were mainly depending on the polycondensation and polymerization reactions between PR and raw CTP. Comparing with the strength of pristine CF at 6.5 MPa, the σ of mCF-9 (13.1 MPa) was remarkably enhanced by 100.1%. However, the λ of mCF-9 substantially reduced to 0.9 m−1K−1 compared with 18.2 W m−1K−1 of pristine CF. Thus, this modification strategy to produce microporous CF materials from raw CTP provides a new protocol for the fabrication of high-performance carbon based materials.


2010 ◽  
Vol 38 (1) ◽  
pp. 72-76
Author(s):  
Wen-Biao WU ◽  
Ke-Qiang QIU ◽  
Cheng-Long LI ◽  
Xiao-Qun XU

2017 ◽  
Vol 68 (8) ◽  
pp. 1895-1902
Author(s):  
Ioana Cristina Tita ◽  
Eleonora Marian ◽  
Bogdan Tita ◽  
Claudia Crina Toma ◽  
Laura Vicas

Thermal analysis is one of the most frequently used instrumental techniques in the pharmaceutical research, for the thermal characterization of different materials from solids to semi-solids, which are of pharmaceutical relevance. In this paper, simultaneous thermogravimetry/derivative thermogravimetry (TG/DTG) and differential scanning calorimetry (DSC) were used for characterization of the thermal behaviour of candesartan cilexetil � active substance (C-AS) under dynamic nitrogen atmosphere and nonisothermal conditions, in comparison with pharmaceutical product containing the corresponding active substance. It was observed that the commercial samples showed a different thermal profile than the standard sample, caused by the presence of excipients in the pharmaceutical product and to possible interaction of these with the active substance. The Fourier transformed infrared spectroscopy (FT-IR) and X-ray powder diffraction (XRPD) were used as complementary techniques adequately implement and assist in interpretation of the thermal results. The main conclusion of this comparative study was that the TG/DTG and DSC curves, together with the FT-IR spectra, respectively X-ray difractograms constitute believe data for the discrimination between the pure substance and pharmaceutical forms.


Materials ◽  
2021 ◽  
Vol 14 (11) ◽  
pp. 2911
Author(s):  
Margarida Gonçalves ◽  
Inês Silveirinha Vilarinho ◽  
Marinélia Capela ◽  
Ana Caetano ◽  
Rui Miguel Novais ◽  
...  

Ordinary Portland Cement is the most widely used binder in the construction sector; however, a very high carbon footprint is associated with its production process. Consequently, more sustainable alternative construction materials are being investigated, namely, one-part alkali activated materials (AAMs). In this work, waste-based one-part AAMs binders were developed using only a blast furnace slag, as the solid precursor, and sodium metasilicate, as the solid activator. For the first time, mortars in which the commercial sand was replaced by two exhausted sands from biomass boilers (CA and CT) were developed. Firstly, the characterization of the slag and sands (aggregates) was performed. After, the AAMs fresh and hardened state properties were evaluated, being the characterization complemented by FTIR and microstructural analysis. The binder and the mortars prepared with commercial sand presented high compressive strength values after 28 days of curing-56 MPa and 79 MPa, respectively. The mortars developed with exhausted sands exhibit outstanding compressive strength values, 86 and 70 MPa for CT and CA, respectively, and the other material’s properties were not affected. Consequently, this work proved that high compressive strength waste-based one-part AAMs mortars can be produced and that it is feasible to use another waste as aggregate in the mortar’s formulations: the exhausted sands from biomass boilers.


2021 ◽  
Vol 11 (8) ◽  
pp. 3540
Author(s):  
Numfor Linda Bih ◽  
Assia Aboubakar Mahamat ◽  
Jechonias Bidossèssi Hounkpè ◽  
Peter Azikiwe Onwualu ◽  
Emmanuel E. Boakye

The quantity of polymer waste in our communities is increasing significantly. It is therefore necessary to consider reuse or recycling waste to avoid an increase in the risk to public health. This project is aimed at using pulverized low-density polyethylene (LDPE) waste as a source to reinforce and improve compressive strength, and to reduce the water absorption of geopolymer ceramics (GC). Clay:LDPE composition consisting of 5%, 10%, and 15% LDPE was geopolymerized with an NaOH/Na2SiO3 solution and cured at 30 °C and 50 °C. Characterization of the geopolymer samples was carried out using XRF and XRD. The microstructure was analyzed by SEM and chemical bonding by FTIR. The SEM micrographs showed LDPE particle pull-out on the geopolymer ceramics’ fracture surface. The result showed that the compressive strength increases with the addition of pulverized polymer waste compared to the controlled without LDPE addition. Water absorption decreased with an increase in LDPE addition in the geopolymer ceramics composite.


2011 ◽  
Vol 402 ◽  
pp. 215-220 ◽  
Author(s):  
Ru Fei Wei ◽  
Jia Xin Li ◽  
Guang Wu Tang

The effects of four inorganic binders and four organic binders on strength of green pellet containing carbon were studied. The results show that phenolic resin is the best binder, compressive strength and drop strength of preheated pellet are 312.5 N and 15.1 times, respectively, when the matching was 2%. The reason is that chemical adsorption effect occurs in pellet. Strength of wet pellet is mainly maintained by capillary force. However, preheated pellet is mainly maintained by chemical adsorption effect and viscous force. Chemical adsorption effect is better than viscous force.


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