scholarly journals Synthesis of Silicon Nitride Ceramic Material using Direct Nitridation Process

Author(s):  
Cuong Van Tran ◽  
Duong Duc La
2020 ◽  
Vol 40 (10) ◽  
pp. 3541-3554 ◽  
Author(s):  
Iyas Khader ◽  
Christof Koplin ◽  
Christian Schröder ◽  
Jens Stockmann ◽  
Wieland Beckert ◽  
...  

Author(s):  
Yanhui Li ◽  
Li Wang ◽  
Shaowu Yin ◽  
Fuming Yang ◽  
Chuanping Liu ◽  
...  

The direct nitridation process of silicon added with amorphous silicon nitride powder at atmospheric pressure was investigated and the product was analyzed by XRD and SEM. Based on the relationship between the conversion ratio of silicon and the reaction time at different temperatures, a physical and mathematical model was derived to describe the nitridation process of silicon particles. The results showed that the conversion ratio of silicon increased rapidly at the early stage of reaction. And the reaction would be accelerated by reducing the size of silicon particle and increasing the pressure of N2. At the range of experimental temperature, the conversion ratio of silicon increases with improving temperature.


2011 ◽  
Vol 130-134 ◽  
pp. 14-18
Author(s):  
Shao Wu Yin ◽  
Li Wang ◽  
Li Ge Tong ◽  
Fu Ming Yang ◽  
Yan Hui Li

Ultrafine e grain amorphous silicon nitride (Si3N4) powders were produced via direct nitridation process of silicon powders in transport bed. The properties of the nitridation products, such as morphology, phase composition, chemical composition and structure, were examined using standard characterization techniques (SEM, XRD, FTIR, etc). The experimental results showed, in the case of silicon powders with particle size of 2.7μm, the conversion rate of silicon was 53.4% at reaction temperature of 1380°C and reaction time of 2.7minutes, and the products mainly comprised amorphous silicon nitride powders.


Author(s):  
Hiro Yoshida ◽  
Takashi Nakashima ◽  
Makoto Yoshida ◽  
Yasushi Hara ◽  
Toru Shimamori

A new high quality turbine system using monolithic silicon-nitride ceramic is under development. In this study particle impact tests of the silicon-nitride have been tried at room and elevated temperatures with and without tensile load, which simulates centrifugal force of blade rotation. In the experiment 1 mm diameter particle is impacted at velocities up to 900 m s−1. In this paper, critical velocities for bending fracture and Hertzian cracks are examined. Moreover, strength degradation at elevated temperature and spall fracture of the blade are discussed. The main results are: 1) The bending fracture mode critical impact velocity for soft particles is higher than that for hard particles. 2)The impact parameter ϕ for initiation of Hertzian cracks ranges 1.08×10−5 – 1.56×10−5 for the materials tested. 3)Strength degradation at elevated temperature was clearly observed. 4) In the impact tests on blades spall fracture, which was caused by interaction of stress waves, appeared.


1997 ◽  
Vol 17 (1) ◽  
pp. 25-31 ◽  
Author(s):  
E. Heikinheimo ◽  
I. Isomäki ◽  
A.A. Kodentsov ◽  
F.J.J. van Loo

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