Application of X-ray tomography method for estimation of drilling agents influence on sedimentary rocks in the process of borehole drilling and completion

2020 ◽  
Vol 6 ◽  
pp. 40-44
Author(s):  
О.V. Garshina ◽  
◽  
D.А. Кazakov ◽  
I.L. Nekrasova ◽  
P.А. Khvoshchin ◽  
...  
Author(s):  
Thomas R. McKee ◽  
Peter R. Buseck

Sediments commonly contain organic material which appears as refractory carbonaceous material in metamorphosed sedimentary rocks. Grew and others have shown that relative carbon content, crystallite size, X-ray crystallinity and development of well-ordered graphite crystal structure of the carbonaceous material increases with increasing metamorphic grade. The graphitization process is irreversible and appears to be continous from the amorphous to the completely graphitized stage. The most dramatic chemical and crystallographic changes take place within the chlorite metamorphic zone.The detailed X-ray investigation of crystallite size and crystalline ordering is complex and can best be investigated by other means such as high resolution transmission electron microscopy (HRTEM). The natural graphitization series is similar to that for heat-treated commercial carbon blacks, which have been successfully studied by HRTEM (Ban and others).


Clay Minerals ◽  
2005 ◽  
Vol 40 (2) ◽  
pp. 191-203 ◽  
Author(s):  
F. Khormali ◽  
A. Abtahi ◽  
H. R. Owliaie

AbstractClay minerals of calcareous sedimentary rocks of southern Iran, part of the old Tethys area, were investigated in order to determine their origin and distribution, and to reconstruct the palaeoclimate of the area. Chemical analysis, X-ray diffraction, transmission electron microscopy, scanning electron microscopy, and thin-section studies were performed on the 16 major sedimentary rocks of the Fars and Kuhgiluyeh Boyerahmad Provinces.Kaolinite, smectite, chlorite, illite, palygorskite and illite-smectite interstratified minerals were detected in the rocks studied. The results revealed that detrital input is possibly the main source of kaolinite, smectite, chlorite and illite, whilein situneoformation during the Tertiary shallow saline and alkaline environment could be the dominant cause of palygorskite occurrences in the sedimentary rocks.The presence of a large amount of kaolinite in the Lower Cretaceous sediments and the absence or rare occurrence of chlorite, smectite, palygorskite and illite are in accordance with the warm and humid climate of that period. Smaller amounts of kaolinite and the occurrence of smectite in Upper Cretaceous sediments indicate the gradual shift from warm and humid to more seasonal climate. The occurrence of palygorskite and smectite and the disappearance of kaolinite in the late Palaeocene sediments indicate the increase in aridity which has probably continued to the present time.


1985 ◽  
Vol 49 (352) ◽  
pp. 393-400 ◽  
Author(s):  
P. H. Nadeau ◽  
M. J. Wilson ◽  
W. J. McHardy ◽  
J. M. Tait

AbstractDiagenetic illitic clays from seven North American bentonites of Ordovician, Devonian, and Cretaceous ages and from three subsurface North Sea sandstones of Permian and Jurassic ages have been examined by X-ray diffraction (XRD) and transmission and scanning electron microscopy (TEM and SEM). XRD indicates that the clays from the bentonites are randomly and regularly interstratified illite/smectites (I/S) with 30–90% illite layers, whereas the clays from the Jurassic and Permian sandstones are regularly interstratified I/S, with 80–90% illite layers, and illite respectively. TEM of shadowed materials shows that randomly interstratified I/S consists primarily of mixtures of elementary smectite and ‘illite’ particles (10 and 20Å thick respectively) and that regularly interstratified I/S and illite consist mainly of ‘illite’ particles 20–50 Å thick and > 50 Å thick respectively. Regularly interstratified I/S from bentonites and sandstones are similar with regard to XRD character and particle thickness distribution. These observations can be rationalized if the interstratified XRD character arises from an interparticle diffraction effect, where the smectite interlayers perceived by XRD, result from adsorption of exchangeable cations and water or organic molecules at the interfaces of particles generally < 50Å thick. A neoformation mechanism is proposed by which smectite is converted to illite with increasing depth of burial in sedimentary rocks, based on dissolution of smectite particles and the precipitation/growth of ‘illite’ particles occurring within a population of thin phyllosilicate crystals.


2010 ◽  
Vol 77 (1-2) ◽  
pp. 58-70 ◽  
Author(s):  
Heather J.H. Johnstone ◽  
Michael Schulz ◽  
Stephen Barker ◽  
Henry Elderfield

Author(s):  
L Suárez del Río ◽  
C Celorio ◽  
A Rodríguez-Rey ◽  
J Descheirder ◽  
L Calleja ◽  
...  

2019 ◽  
Vol 55 (8) ◽  
pp. 3347-3353
Author(s):  
Pierre-Louis Valdenaire ◽  
Jonathan Perrin ◽  
Olivier Grauby ◽  
Franz-Josef Ulm ◽  
Roland J. M. Pellenq

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