Creating a developed surface of copper electrolytic coatings via mechanical activation of the cathode with subsequent thermal treatment

2015 ◽  
Vol 79 (9) ◽  
pp. 1093-1097 ◽  
Author(s):  
N. N. Gryzunova ◽  
A. A. Vikarchuk ◽  
V. V. Bekin ◽  
A. E. Romanov
2016 ◽  
Vol 61 (2) ◽  
pp. 869-874 ◽  
Author(s):  
E. Jartych ◽  
T. Pikula ◽  
M. Mazurek ◽  
W. Franus ◽  
A. Lisinska-Czekaj ◽  
...  

Abstract Three different methods were used to obtain Bi5Ti3FeO15 ceramics, i.e. solid-state sintering, mechanical activation (MA) with subsequent thermal treatment, and electrical discharge assisted mechanical milling (EDAMM). The structure and magnetic properties of produced Bi5Ti3FeO15 samples were characterized using X-ray diffraction and Mössbauer spectroscopy. The purest Bi5Ti3FeO15 ceramics was obtained by standard solid-state sintering method. Mechanical milling methods are attractive because the Bi5Ti3FeO15 compound may be formed at lower temperature or without subsequent thermal treatment. In the case of EDAMM process also the time of processing is significantly shorter in comparison with solid-state sintering method. As revealed by Mössbauer spectroscopy, at room temperature the Bi5Ti3FeO15 ceramics produced by various methods is in paramagnetic state.


2015 ◽  
Vol 51 (70) ◽  
pp. 13462-13465 ◽  
Author(s):  
Yutaka Maeda ◽  
Yuya Takehana ◽  
Michio Yamada ◽  
Mitsuaki Suzuki ◽  
Tatsuya Murakami

Alkylation and subsequent thermal treatment of SWNTs induces a new bright PL peak in the NIR region.


2018 ◽  
Vol 6 (24) ◽  
pp. 11496-11506 ◽  
Author(s):  
Paul Pistor ◽  
Thomas Burwig ◽  
Carlo Brzuska ◽  
Björn Weber ◽  
Wolfgang Fränzel

We present the identification of crystalline phases by in situ X-ray diffraction during growth and monitor the phase evolution during subsequent thermal treatment of CH3NH3PbX3 (X = I, Br, Cl) perovskite thin films.


2019 ◽  
Vol 55 (1) ◽  
pp. 85-93 ◽  
Author(s):  
M.M. Vasic ◽  
A.S. Kalezic-Glisovic ◽  
R. Milincic ◽  
Lj. Radovic ◽  
D.M. Minic ◽  
...  

The mechanical activation of the Ni85.8Fe10.6Cu2.2W1.4 powder mixture in the time intervals of 30-210 min in combination with thermal treatment at 393-873 K resulted in microstructural changes, forming the nanostructured mixture of the same composition but improved magnetic properties. The best result were achieved for mechanical activation during 120 min and thermal treatment at temperatures close to the Curie temperature (693K), enhancing the mass magnetization of the starting powder mixture by about 57%. The microstructural changes, which include the structural relaxation, decrease in free volume, density of dislocation and microstrain, improve structural characteristics of material, enabling better mobility of walls of magnetic domains and their better orientation in applied magnetic field and consequently enabling better mass magnetization of the material. With longer time of milling, the growing stress introduced in the sample undergoes easier relief, relocating stress-relieving processes toward lower temperatures.


1989 ◽  
Vol 163 ◽  
Author(s):  
A. Ourmazd ◽  
Y. Kim ◽  
M. Bode

AbstractWe apply quantitative chemical mapping techniques to study thermal interdiffusion and ion-implantation induced intermixing at single heterointerfaces at the atomic level. Our results show thermal interdiffusion to be strongly depth dependent. This is related to the need for the presence of native point defects (interstitials and vacancies) to bring about interdiffusion. Since their initial concentration in the bulk is negligible, the point defects must be injected at the surface and transported to the interface for interdiffusion to occur. In the case of ion-implanted samples, we find the passage of a single energetic ion through a sample at 77 K causes significant intermixing, even when the sample receives no subsequent thermal treatment.


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