Methods of temperature measurement in microwave heating technologies

2021 ◽  
pp. 20-28
Author(s):  
Boris A. Lapshinov

In industrial technological processes associated with the heating of the processed material by microwave radiation, it is necessary to measure the temperatures of objects. Methods for measuring temperatures in the fields of technology using microwave heating systems are considered. The main possibilities, disadvantages and limitations of the used contact and non-contact (optical) measurement methods are determined. The requirements for temperature measurement systems under conditions of exposure to strong electromagnetic fields are listed. The possibilities of the spectral pyrometry method are especially noted.

Catalysts ◽  
2020 ◽  
Vol 10 (2) ◽  
pp. 246 ◽  
Author(s):  
Vincenzo Palma ◽  
Daniela Barba ◽  
Marta Cortese ◽  
Marco Martino ◽  
Simona Renda ◽  
...  

Since the late 1980s, the scientific community has been attracted to microwave energy as an alternative method of heating, due to the advantages that this technology offers over conventional heating technologies. In fact, differently from these, the microwave heating mechanism is a volumetric process in which heat is generated within the material itself, and, consequently, it can be very rapid and selective. In this way, the microwave-susceptible material can absorb the energy embodied in the microwaves. Application of the microwave heating technique to a chemical process can lead to both a reduction in processing time as well as an increase in the production rate, which is obtained by enhancing the chemical reactions and results in energy saving. The synthesis and sintering of materials by means of microwave radiation has been used for more than 20 years, while, future challenges will be, among others, the development of processes that achieve lower greenhouse gas (e.g., CO2) emissions and discover novel energy-saving catalyzed reactions. A natural choice in such efforts would be the combination of catalysis and microwave radiation. The main aim of this review is to give an overview of microwave applications in the heterogeneous catalysis, including the preparation of catalysts, as well as explore some selected microwave assisted catalytic reactions. The review is divided into three principal topics: (i) introduction to microwave chemistry and microwave materials processing; (ii) description of the loss mechanisms and microwave-specific effects in heterogeneous catalysis; and (iii) applications of microwaves in some selected chemical processes, including the preparation of heterogeneous catalysts.


Author(s):  
Julian Wüster ◽  
Yannick Bourgin ◽  
Patrick Feßer ◽  
Arne Behrens ◽  
Stefan Sinzinger

AbstractPolarizing beamsplitters have numerous applications in optical systems, such as systems for freeform surface metrology. They are classically manufactured from birefringent materials or with stacks of dielectric coatings. We present a binary subwavelength-structured form-birefringent diffraction grating, which acts as a polarizing beamsplitter for a wide range of incidence angles −30∘…+30∘. We refine the general design method for such hybrid gratings. We furthermore demonstrate the manufacturing steps with Soft-UV-Nanoimprint-Lithography, as well as the experimental verification, that the structure reliably acts as a polarizing beamsplitter. The experimental results show a contrast in efficiency for TE- and TM-polarization of up to 1:18 in the first order, and 34:1 in the zeroth order. The grating potentially enables us to realize integrated compact optical measurement systems, such as common-path interferometers.


2021 ◽  
pp. 110419
Author(s):  
Jasper Reenalda ◽  
Marit A. Zandbergen ◽  
Jelle D. Harbers ◽  
Max R. Paquette ◽  
Clare E. Milner

1997 ◽  
Vol 119 (2) ◽  
pp. 236-242 ◽  
Author(s):  
K. Peleg

The classical calibration problem is primarily concerned with comparing an approximate measurement method with a very precise one. Frequently, both measurement methods are very noisy, so we cannot regard either method as giving the true value of the quantity being measured. Sometimes, it is desired to replace a destructive or slow measurement method, by a noninvasive, faster or less expensive one. The simplest solution is to cross calibrate one measurement method in terms of the other. The common practice is to use regression models, as cross calibration formulas. However, such models do not attempt to discriminate between the clutter and the true functional relationship between the cross calibrated measurement methods. A new approach is proposed, based on minimizing the sum of squares of the differences between the absolute values of the Fast Fourier Transform (FFT) series, derived from the readings of the cross calibrated measurement methods. The line taken is illustrated by cross calibration examples of simulated linear and nonlinear measurement systems, with various levels of additive noise, wherein the new method is compared to the classical regression techniques. It is shown, that the new method can discover better the true functional relationship between two measurement systems, which is occluded by the noise.


2007 ◽  
Author(s):  
Guojun Yang ◽  
Zhuo Zhang ◽  
Sifu Chen

Author(s):  
Ethan M. Moon ◽  
Vadim V. Yakovlev

PurposeThis paper aims to introduce and illustrate a computational technique capable of determining the geometry and complex permittivity of a supplementary dielectric insert making distributions of microwave-induced dissipated power within the processed material as uniform as possible.Design/methodology/approachThe proposed technique is based on a 3D electromagnetic model of the cavity containing both the processed material and the insert. Optimization problem is formulated for design variables (geometrical and material parameters of the insert) identified from computational tests and an objective function (the relative standard deviation [RSD]) introduced as a metric of the field uniformity. Numerical inversion is performed with the method of sequential quadratic programming.FindingsFunctionality of the procedure is illustrated by synthesis of a dielectric insert in an applicator for microwave fixation. Optimization is completed for four design variables (two geometrical parameters, dielectric constant and the loss factor of the insert) with 1,000 points in the database. The best three optimal solutions provide RSD approximately 20 per cent, whereas for the patterns corresponding to all 1,000 non-optimized (randomly chosen) sets of design variables this metric is in the interval from 27 to 136 per cent with the average of 78 per cent.Research limitations/implicationsAs microwave thermal processing is intrinsically inhomogeneous and the heating time is not a part of the underlying model, the procedure is able to lead only to a certain degree of closeness to uniformity and is intended for applications with high heating rates. The initial phase of computational identification of design variables and their bounds is therefore very important and may pre-condition the “quality” of the optimal solution. The technique may work more efficiently in combination with advanced optimization techniques dealing with “smart” (rather than random) generation of the data; for the use with more general microwave heating processes characterized by lower heating rates, the technique has to use the metric of non-uniformity involving temperature and heating time.Practical implicationsWhile the procedure can be used for computer-aided design (CAD) of microwave applicators, a related practical limitation may emerge from the fact that the material with particular complex permittivity (determined in the course of optimization) may not exist. In such cases, the procedure can be rerun for the constant values of material parameters of the available medium mostly close to the optimal ones to tune geometrical parameters of the insert. Special manufacturing techniques capable of producing a material with required complex permittivity also may be a practical option here.Originality/valueNon-uniformity of microwave heating remains a key challenge in the design of many practical applicators. This paper suggests a concept of a practical CAD and outlines corresponding computational procedure that could be used for designing a range of applied systems with high heating rates.


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