scholarly journals Siloranes–Suitability of a Novel Adhesive for Orthodontic Bracket Bonding

2021 ◽  
Vol 9 (11) ◽  
pp. 135
Author(s):  
Lorenz Brauchli ◽  
Markus Steineck
Keyword(s):  
Phosphoric Acid ◽  
Bond Strength ◽  
Shear Bond Strength ◽  
The Self ◽  
Control Group ◽  
The Novel ◽  
Shear Testing ◽  
Orthodontic Bracket ◽  
Adhesive Interface

Recently, an epoxy-based resin-Filtek Silorane-has been proposed for restorative fillings. It was the aim of the investigation to evaluate the suitability of this novel resin for orthodontic bracket bonding on unground enamel. Shear bond strength was measured for two adhesives-Filtek Silorane, Transbond XT-in combination with steel, ceramic and polymer brackets. For Filtek Silorane etching was performed with the Silorane self-etching primer, as well as phosphoric acid. The Transbond XT samples were etched with phosphoric acid only and served as the control group. All samples were thermo-cycled (1000×, 5–55 °C). Shear testing was carried out with an Instron 3344. In addition, ARI scores were evaluated. The Shear bond strength showed a weak adhesion of Filtek Silorane to unprepared enamel, either with the self-etching primer or the conventional etching (0.87–4.28 MPa). The Shear bond strength of the control group was significantly higher (7.6–16.5 MPa). The ARI scores showed a clear failure at the enamel-adhesive interface for all Filtek Silorane samples. For the combination of Transbond XT and different brackets the failure was found at the adhesive–bracket interface. The novel epoxy-based resin Filtek Silorane is not appropriate for bracket bonding to unprepared enamel.

scholarly journals Reinforcement of bond strength of self-etching orthodontic adhesive

2011 ◽  
Vol 82 (1) ◽  
pp. 30-35
Author(s):  
Shinya Horiuchi ◽  
Shingo Kuroda ◽  
Masahiro Hiasa ◽  
Toshiyuki Suge ◽  
Seitaro Saku ◽  
...  
Keyword(s):  
Citric Acid ◽  
Phosphoric Acid ◽  
Bond Strength ◽  
Polyacrylic Acid ◽  
Shear Bond Strength ◽  
Adhesive System ◽  
Control Group ◽  
Bonding System ◽  
Adhesive Remnant Index ◽  
Debonding Process

Abstract Objective: To determine the reinforcement of bond strength of a self-etching system by applying a pretreatment agent. Materials and Methods: Sixty extracted human premolars were used in this study. The enamel surfaces were treated with four pretreatment agents—phosphoric acid, polyacrylic acid, citric acid, and ammonium hexafluorosilicate (SiF)—and were examined under a scanning electron microscope. Afterward, orthodontic brackets were bonded with a self-etching adhesive system (n  =  10 for each agent), and shear bond strength was measured through a debonding process. The adhesive remnant index (ARI) was also assessed. Results: Enamel surfaces treated with polyacrylic acid seemed almost the same as intact enamel. Treatment with SiF induced slight shallow depressions compared with the intact enamel. On the other hand, enamel surfaces treated with citric acid and phosphoric acid showed severe etching patterns. All pretreatments increased the bond strength, but SiF-treated specimens revealed the greatest strength (12.201 ± 1.048 MPa), followed by polyacrylic acid (12.030 ± 2.103 MPa). The control group with no pretreatment showed the least strength (9.078 ± 1.678 MPa). All pretreatments increased ARI score compared with the control group. Conclusions: Surface conditioning before bracket adhesion could reinforce the bond strength of the self-etching adhesive system, resulting in a more reliable bonding system.

scholarly journals Influence of previous acid etching on interface morphology and bond strength of self-etching adhesive to cavosurface enamel

2012 ◽  
Vol 06 (01) ◽  
pp. 056-062 ◽  
Author(s):  
Adriano Fonseca Lima ◽  
Vinícius Brito da Silva ◽  
Giulliana Panfiglio Soares ◽  
Giselle Maria Marchi ◽  
Flávio Henrique Baggio Aguiar ◽  
...  
Keyword(s):  
Phosphoric Acid ◽  
Bond Strength ◽  
Adhesive System ◽  
The Self ◽  
The Other ◽  
Acid Etching ◽  
Control Group ◽  
System Control ◽  
Etch And Rinse ◽  
Group 3

ABSTRACTObjectives: The aim of this study was to evaluate the (1) bond strength of a etch-and-rinse and self-etching adhesive systems to cavosurface enamel, (2) influence of the previous acid etching with phosphoric acid 35% to the self-etching adhesive application on bond strength values, and (3) analysis of the cavosurface enamel morphology submitted to different types of conditioning, with the use of a scanning electronic microscope (SEM).Methods: Twenty four human third molars were sectioned on mesio-distal direction, resulting in two slices. The specimens were ground flat with 600-grit aluminum oxide papers, and were randomly divided into three groups: Group 1 (etch-and-rinse adhesive system (control group)), Group 2 (selfetching adhesive), and Group 3 (self-etching adhesive with previous 35% phosphoric acid-etching for 15 s). Four cylinders (0.75 mm of diameter, 1 mm height) were confectioned prior to the microshear test. Four samples for each group were prepared according the cavosurface enamel treatment and were analyzed in an SEM.Results: Group 3 had the highest values on bond strength to cavosurface enamel compared to the other two groups, which presented statistically similar values. The performance of acid etching before the application of the self-etching adhesive results in an etching pattern that is different than the other groups, favoring the adhesion to the cavosurface enamel.Conclusions: Acid etching increases the bond strength values of the self-etching adhesive to cavosurface enamel, promoting a conditioning pattern that favors the adhesion to this substrate. (Eur J Dent 2012;6:56-62)

Shear Bond Strength of Porcelain Veneers Rebonded to Enamel

2015 ◽  
Vol 40 (3) ◽  
pp. E112-E121 ◽  
Author(s):  
HA St Germain ◽  
TH St Germain
Keyword(s):  
Phosphoric Acid ◽  
Bond Strength ◽  
Aluminum Oxide ◽  
Shear Bond Strength ◽  
Resin Cement ◽  
Enamel Surface ◽  
Control Group ◽  
Significant Difference ◽  
Mode Of Failure ◽  
Group A

SUMMARY In this laboratory research, shear bond strength (SBS) and mode of failure of veneers rebonded to enamel in shear compression were determined. Three groups (A, B, and C; n=10 each) of mounted molar teeth were finished flat using wet 600-grit silicon carbide paper, and 30 leucite-reinforced porcelain veneers (5.0 × 0.75 mm) were air abraded on the internal surface with 50 μm aluminum oxide, etched with 9.5% hydrofluoric acid, and silanated. The control group (A) veneer specimens were bonded to enamel after etching with 37% phosphoric acid using bonding resin and a dual cure resin composite cement. Groups B and C were prepared similarly to group A with the exception that a release agent was placed before the veneer was positioned on the prepared enamel surface and the resin cement was subsequently light activated. The debonded veneers from groups B and C were placed in a casting burnout oven and heated to 454°C/850°F for 10 minutes to completely carbonize the resin cement and stay below the glass transition temperature (Tg) of the leucite-reinforced porcelain. The recovered veneers were then prepared for bonding. The previously bonded enamel surfaces in group B were air abraded using 50 μm aluminum oxide followed by 37% phosphoric acid etching, while group C enamel specimens were acid etched only. All specimens were thermocycled between 5°C and 55°C for 2000 cycles using a 30-second dwell time and stored in 37°C deionized water for 2 weeks. SBS was determined at a crosshead speed of 1.0 mm/min. SBS results in MPa for the groups were (A) = 20.6±5.1, (B) = 18.1±5.5, and (C) = 17.2±6.1. One-way analysis of variance indicated that there were no significant interactions (α=0.05), and Tukey-Kramer post hoc comparisons (α=0.05) detected no significant pairwise differences. An adhesive mode of failure at the enamel interface was observed to occur more often in the experimental groups (B = 40%, C = 50%). Rebonding the veneers produced SBS values that were not significantly different from the control group. Also, no significant difference in SBS values were observed whether the debonded enamel surface was air abraded and acid etched or acid etched only.

scholarly journals Shear bond strength of resin composite to enamel treated with Er:Y AG laser and phosphoric acid

2010 ◽  
Vol 10 (4) ◽  
Author(s):  
Nádia R. Svizero ◽  
Renato S. Carvalho ◽  
Lucirene A. Domingues ◽  
Carolina N. Pegorado ◽  
Carlos Henrique Francischone ◽  
...  
Keyword(s):  
Phosphoric Acid ◽  
Bond Strength ◽  
Shear Bond Strength ◽  
Er:Yag Laser ◽  
Resin Composite ◽  
Control Group ◽  
Third Molars ◽  
Dental Crowns ◽  
Acid Control ◽  
Composite Cylinders

The purpose of this work was to evaluate the shear bond strength of resin composite to enamel treated with Er:YAG laser. It was used 33 human third molars. After the dental crowns cutting, the mesial and distal surfaces were embedded perpendicularly to the PVC cylinders long axis. Enamel was ground and the samples were randomly divided into 6 groups: G1- phosphoric acid (control), G2- Er:YAG laser (60mJ/10Hz), G3- Er:YAG (100mJ/10Hz), G4- Er:YAG (60mJ/10Hz + acid), G5- Er:YAG (100mJ/ 10Hz + acid), G6- Er:YAG (80mJ/2Hz). In all groups, Single Bond was used and resin composite cylinders (Z100) were prepared. The samples were stored in distilled water at 37oC for 24 hours and submitted to shearing test. G1 presented bond strength values significantly higher than G2, G3 and G6. The groups irradiated only with Er:YAG laser, in different intensities and frequencies, were equivalent as for the bond strength values. The groups treated with laser + acid presented strength values statistically equal to those of the control group. The enamel treatment with phosphoric acid, or its association with laser, is important to obtain good bond. The use of Er: YAG laser alone is not recommended, considering the conditions tested in this study.

Shear Bond Strength of Two Resin Cements to Human Root Dentin Using Three Dentin Bonding Agents

10.2341/06-3 ◽  
2007 ◽  
Vol 32 (1) ◽  
pp. 31-36 ◽  
Author(s):  
C. Gogos ◽  
C. Stavrianos ◽  
I. Kolokouris ◽  
N. Economides ◽  
I. Papadoyannis
Keyword(s):  
Phosphoric Acid ◽  
Bond Strength ◽  
Clinical Relevance ◽  
Shear Bond Strength ◽  
The Self ◽  
Resin Cements ◽  
Bonding Agents ◽  
Dentin Bonding ◽  
Edta Solution ◽  
Root Dentin

Clinical Relevance The application of 15% EDTA solution was shown to be an alternative to the commonly used 37% phosphoric acid in the bonding procedures of resin cements. The self-etching adhesive tested was found to improve bond strength more than one-bottle adhesives.

scholarly journals Influence of Primekote® polymer in orthodontic bonding

2017 ◽  
Vol 46 (2) ◽  
pp. 61-65
Author(s):  
Eduardo Otero Amaral VARGAS ◽  
Cinthia Candemil NUERNBERG ◽  
José Vinicius Bolognesi MACIEL ◽  
Ana Maria BOLOGNESE
Keyword(s):  
Bond Strength ◽  
Shear Bond Strength ◽  
Clinical Performance ◽  
Testing Machine ◽  
Adhesive System ◽  
Test Sample ◽  
Wilcoxon Test ◽  
Tooth Surface ◽  
Control Group ◽  
Orthodontic Bracket

Abstract Objective The Primekote® (TP) polymer was incorporated to the of Orthodontic Bracket mesh base to improve bond strength and make it more efficient. The purpose of this study was to assess the shear bond strength and adhesive remnant index (ARI) of these brackets. Material and method The test sample consisted of thirty bovine incisors divided into 2 groups: with a group with TP® brackets (n=15), and a control group with Morelli® brackets (n=15) without Primekote® technology. The TransbondTM XT was used as adhesive system in both groups, following the same protocol and manufacturer’s instructions. Specimens were stored in distilled water for 24 hours and then submitted to shear bond strength test in a universal testing machine (EMIC DL2000). The assessment of ARI was performed under stereomicroscope by two calibrated examiners. Result No significant differences (p>0.05) in shear bond strength were found between the two groups according to the independent t-test. The Wilcoxon test was used to assess ARI data and statistical difference was found between Morelli® and TP® Nu-Edge brackets; the last one left less remaining adhesive on tooth surface. Conclusion TP® brackets had higher adherence to the adhesive system as shown by lower ARI scores, but this does not improve its clinical performance.

scholarly journals SHEAR BOND STRENGTH OF BISPHENOL A-GLYCIDYL METHACRYLATE ADHESIVE RESIN AFTER APPLICATION OF EUCALYPTUS OIL BEFORE DEBONDING METALLIC ORTHODONTIC BRACKET

2019 ◽  
pp. 187-189
Author(s):  
ARISTY RIYANTI ◽  
ERWIN SIREGAR ◽  
HARU SETYO ANGGANI
Keyword(s):  
Bisphenol A ◽  
Bond Strength ◽  
Glycidyl Methacrylate ◽  
Shear Bond Strength ◽  
Control Group ◽  
Adhesive Resin ◽  
Orthodontic Bracket ◽  
Eucalyptus Oil ◽  
Significant Difference ◽  
Group 2

Objective: Debonding of orthodontic braces could lead to enamel fracture and moderate discomfort for the patients. This study was conducted toexamine whether eucalyptus oil and eucalyptol were effective in decreasing the shear bond strength and facilitate the debonding of metallic bracketsbonded with bisphenol A-glycidyl methacrylate (bis-GMA) adhesive resin.Methods: Thirty upper premolar teeth were randomly divided into the following three groups: Group 1 (75% eucalyptus oil), Group 2 (100%eucalyptol), and Group 3 (aquades; controls). Gemini brackets (3M Unitek, Monrovia) were bonded to the teeth using Transbond XT (3M Unitek,Monrovia). The areas around the brackets were lubricated with 75% eucalyptus oil, 100% eucalyptol, and aquades for 10 min before debonding.Results: A significant difference in shear bond strength between Group 2 and the control group was noted (p<0.05).Conclusion: The findings of this study indicated that eucalyptol can decrease the shear bond strength of bis-GMA-based adhesive resin after 10 minof application.

scholarly journals Effect of Lactic Acid Etching on Bonding Effectiveness of Orthodontic Bracket after Water Storage

2014 ◽  
Vol 2014 ◽  
pp. 1-6 ◽  
Author(s):  
Fahad F. Alsulaimani
Keyword(s):  
Lactic Acid ◽  
Phosphoric Acid ◽  
Bond Strength ◽  
Shear Bond Strength ◽  
Water Storage ◽  
Adhesive System ◽  
Orthodontic Brackets ◽  
Orthodontic Bracket ◽  
Significant Difference ◽  
Before And After

Objective. To determine the effect of lactic acid at various concentrations on the shear bond strength of orthodontic brackets bonded with the resin adhesive system before and after water storage. Materials and Methods. Hundred extracted human premolars were divided into 5 treatment groups and etched for 30 seconds with one of the following agents: lactic acid solution with (A) 10%, (B) 20%, (C) 30%, and (D) 50%; group E, 37% phosphoric acid (control). Metal brackets were bonded using a Transbond XT. Bonding effectiveness was assessed by shear bond strength after 24 hours and 6 months of water storage at 37°C. The data were analyzed with 2-way analysis of variance and Tukey’s Honestly Significant Difference (HSD) test (α=.001). Results. Lactic acid concentration and water storage resulted in significant differences for brackets bond strength (P<.001). 20% lactic acid had significantly higher mean bond strength values (SD) for all conditions: 24 hours [12.2 (.7) MPa] and 6 months [10.1 (.6) MPa] of water storage. 37% phosphoric acid had intermediate bond strength values for all conditions: 24 hours [8.2 (.6) MPa] and 6 months [6.2 (.6) MPa] of water storage. Also, there were differences in bond strength between storage time, with a reduction in values from 24 hours and 6 months for all experimental groups (P<.001). Conclusion. Lactic acid could be used in place of phosphoric acid as an enamel etchant for bonding of orthodontic brackets.

scholarly journals Application Modes Affect Two Universal Adhesive Systems’ Nanoleakage Expression and Shear Bond Strength

2021 ◽  
Vol 2021 ◽  
pp. 1-8
Author(s):  
A. S. Bakry ◽  
M. A. Abbassy
Keyword(s):  
Bond Strength ◽  
Silver Nitrate ◽  
Shear Bond Strength ◽  
The Self ◽  
Bonding Layer ◽  
Adhesive Systems ◽  
Hybrid Layer ◽  
Adhesive Interface ◽  
Bonding Systems ◽  
Self Etch

Objectives. The aim of this study was to evaluate the shear bond strength and the nanoleakage expression of CLEARFIL Universal Bond Quick and Tetric N-Bond adhesive systems bonded to dentin. Materials and Methods. 100 freshly extracted human premolar teeth were utilized. The teeth were sectioned to expose dentin. All dentin specimens were assigned into 4 experimental groups; 2 groups had Universal Bond Quick (Universalself group) and Tetric N-Bond (Tetricself group) applied in the self-etch mode, while 2 groups had Universal Bond Quick (Universaltotal group) and Tetric N-Bond (Tetrictotal group) applied in the total-etch mode. n = 15 for shear bond strength and n = 10 for nanoleakage experiment. One-way ANOVA and Kruskal-Wallis test were utilized to analyze the shear bond strength test and the nanoleakage expression, respectively. Results. The highest significant bond strength value was recorded by the Tetricself specimens ( p < 0.05 ) when compared to the remaining three groups. There were no statistically significant differences between the shear bond strength values recorded in the Tetrictotal, Universalself, and Universaltotal groups ( p < 0.05 ). Both bonding systems applied in the self-etch mode (Universalself, Tetricself) had no silver nitrate deposits in the hybrid layer and the hybrid layer-adhesive interface ( p < 0.001 ); however, both bonding systems applied in the total-etch mode (Universaltotal, Tetrictotal) had silver nitrate deposits in the hybrid layer, the hybrid layer-adhesive interface, and the bonding layer ( p < 0.001 ). Conclusion. Applying the Universal Bond Quick and Tetric N-Bond in the self-etch mode exhibited better results in terms of nanoleakage expression. Universal Bond Quick showed the stability of the shear bond strength to dentin when applied using the total-etch or self-etch modes. Tetric N-Bond showed significant deterioration in bond strength when applied in the total-etch mode and exhibited the highest bond strength when applied in the self-etch mode.

scholarly journals Effects of Self-Etching Primer on Shear Bond Strength of Orthodontic Brackets at Different Debond Times

2007 ◽  
Vol 77 (1) ◽  
pp. 108-112 ◽  
Author(s):  
Tamer Turk ◽  
Selma Elekdag-Turk ◽  
Devrim Isci
Keyword(s):  
Phosphoric Acid ◽  
Bond Strength ◽  
Conventional Method ◽  
Shear Bond Strength ◽  
Orthodontic Brackets ◽  
Control Group ◽  
Study Group ◽  
Group A ◽  
Bond Strengths

Abstract Objective: To evaluate the effect of a self-etching primer on shear bond strengths (SBS) at the different debond times of 5, 15, 30, and 60 minutes and 24 hours. Materials and Methods: Brackets were bonded to human premolars with different etching protocols. In the control group (conventional method [CM]) teeth were etched with 37% phosphoric acid. In the study group, a self-etching primer (SEP; Transbond Plus Self Etching Primer; 3M Unitek, Monrovia, Calif) was applied as recommended by the manufacturer. Brackets were bonded with light-cure adhesive paste (Transbond XT; 3M Unitek) and light-cured for 20 seconds in both groups. The shear bond test was performed at the different debond times of 5, 15, 30 and 60 minutes and 24 hours. Results: Lowest SBS was attained with a debond time of 5 minutes for the CM group (9.51 MPa) and the SEP group (8.97 MPa). Highest SBS was obtained with a debond time of 24 hours for the CM group (16.82 MPa) and the SEP group (19.11 MPa). Statistically significant differences between the two groups were not observed for debond times of 5, 15, 30, or 60 minutes. However, the SBS values obtained at 24 hours were significantly different (P &lt; .001). Conclusions: Adequate SBS was obtained with self-etching primer during the first 60 minutes (5, 15, 30 and 60 minutes) when compared with the conventional method. It is reliable to load the bracket 5 minutes after bonding using self-etching primer (Transbond Plus) with the light-cure adhesive (Transbond XT).

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