scholarly journals Optimisation of Heat Treatment Process for Damping Properties of Mg-13Gd-4Y-2Zn-0.5Zr Magnesium Alloy Using Box–Behnken Design Method

Metals ◽  
2019 ◽  
Vol 9 (2) ◽  
pp. 157 ◽  
Author(s):  
Jun Zhang ◽  
Ziming Kou ◽  
Yaqin Yang ◽  
Baocheng Li ◽  
Xiaowen Li ◽  
...  
Keyword(s):  
Heat Treatment ◽  
Magnesium Alloy ◽  
Treatment Process ◽  
High Strength ◽  
Damping Capacity ◽  
Heat Treatment Process ◽  
Damping Properties ◽  
Heat Treated ◽  
Second Phases ◽  
Imagej Software

High damping magnesium alloys have poor mechanical properties, so it is necessary to investigate the damping properties of high-strength wrought magnesium alloys to effectively reduce vibration and noise in mechanical engineering. The aim of this work is to improve the mechanical damping performance of a novel high-strength Mg-13Gd-4Y-2Zn-0.5Zr magnesium alloy by optimising the heat treatment process. The mechanical damping coefficient, considering not only damping capacity but also the yield strength, is selected as one of the evaluation indexes. The other evaluation index is the tensile strength. The solid solution and ageing treatment were optimised by Box-Behnken method, an efficient experimental design technique. Heat treatment experiments based on the optimal parameters verified that the best process is a solution at 520 °C for 10 h followed by ageing at 239 °C for 22 h. The damping coefficient reaches 0.296, which is 73.1% higher than that before heat treatment. There was a good agreement between the experimental and Box-Behnken predicted results. The microstructure, morphology and composition of the second phases after heat treatment were analysed by SEM, XRD and EDS. Due to the high content of alloying elements in Mg-13Gd-4Y-2Zn-0.5Zr alloy, there are a large number of second phases after heat treated. They mainly include layer, short rod-shaped, bulk long period stacking order (LPSO) Mg12YZn and granular Mg5Gd phases. It was found that the area fraction of the second phases has an extreme effect on the damping capacity and short rod-shaped LPSO can effectively improve the damping capacity of heat-treated Mg-13Gd-4Y-2Zn-0.5Zr alloy. The volume fraction of the second phases was analysed by ImageJ software. It was concluded that the smaller the area occupied by the second phases, the better the mobility of the dislocation, and the better the damping performance of the alloy. The statistical analysis results obtained using ImageJ software are consistent with the experimental results damping capacity.

Optimization of Heat Treatment Process of ZE41A Magnesium Alloy Using Grey- Based Taguchi Method

2008 ◽  
Vol 3 (2) ◽  
pp. 63-69
Author(s):  
M. Sivapragash ◽  
◽  
V. Sateeshkumar ◽  
P.R. Lakshminarayanan ◽  
R. Karthikeyan ◽  
...  
Keyword(s):  
Heat Treatment ◽  
Magnesium Alloy ◽  
Taguchi Method ◽  
Treatment Process ◽  
Heat Treatment Process

High Tensile Strength of Drawn Gold

2005 ◽  
Vol 495-497 ◽  
pp. 907-912 ◽  
Author(s):  
Suk Hoon Kang ◽  
Hee Suk Jung ◽  
Woong Ho Bang ◽  
Jae Hyung Cho ◽  
Kyu Hwan Oh ◽  
...  
Keyword(s):  
Heat Treatment ◽  
Grain Size ◽  
Tensile Strength ◽  
Treatment Process ◽  
Gold Wire ◽  
Equivalent Strain ◽  
Heat Treatment Process ◽  
High Tensile Strength ◽  
Heat Treated ◽  
Gold Wires

This paper studies the microstructure of drawn gold wires to equivalent strain of 10 and to equivalent strain of 8.5 then heat-treated. The texture of gold wire drawn to strain of 10 is mainly composed of <100> and <111> fibers. Tensile strength of the gold wire increases with <111> fiber fraction, while the grain size does not appear to affect the tensile property. With an exception at heat treatment at 600oC, the texture of gold wire drawn the strain of 8.5 is replaced with <100> fiber component by heat treatment process at 400~700oC. Heat treatment at 600oC produces <110> fiber or <112> fiber, depending upon annealing time.

scholarly journals Heat Treated AZ61 Magnesium Alloy Obtained by Direct Extrusion and Continuous Rotary Extrusion Process

2016 ◽  
Vol 61 (1) ◽  
pp. 405-410
Author(s):  
M. Bigaj ◽  
S. Boczkal ◽  
J. Żelechowski ◽  
M. Gawlik ◽  
M. Mitka
Keyword(s):  
Heat Treatment ◽  
Magnesium Alloy ◽  
Treatment Process ◽  
Extrusion Process ◽  
Direct Extrusion ◽  
Preferred Direction ◽  
Decomposition Of Solid Solution ◽  
Az61 Magnesium Alloy ◽  
Heat Treated ◽  
Low Degree

The results of studies carried out on the heat treated AZ61 magnesium alloy extruded by two methods, i.e. direct extrusion and continuous rotary extrusion, were presented. As part of the work, parameters of the T6 heat treatment were proposed and aging curves were plotted. The solution heat treatment process was accompanied by the grain growth. During artificial aging, due to the decomposition of solid solution, the β-Mg17Al12 phase was precipitated from the supersaturated α solution. It precipitated in a coagulated form at the grain boundaries and in the form of fine-dispersed plates arranged in a preferred direction relative to the grain orientation. Rods obtained by continuous rotary extrusion, unlike those made by the direct process, exhibited a low degree of texturing and lack of anisotropic properties.

Microstructure of Silicon Nitride Fibers at Elevated Temperatures

2017 ◽  
Vol 898 ◽  
pp. 1705-1711 ◽  
Author(s):  
Jun Zhe Li ◽  
Xun Sun ◽  
Hai Tao Liu ◽  
Hai Feng Cheng ◽  
Xiao Shan Zhang
Keyword(s):  
Heat Treatment ◽  
Silicon Nitride ◽  
Amorphous Silicon ◽  
Treatment Process ◽  
Elevated Temperatures ◽  
Heat Treatment Process ◽  
Amorphous Silicon Nitride ◽  
Heat Treated ◽  
Strength Retention ◽  
Heat Treated Temperature

The composition and microstructure of silicon nitride fibers after heat-treatment at elevated temperatures were investigated by XRD, NMR, XPS, SEM and TEM analyses. The results show that as-received fibers consisted of amorphous silicon nitride, and a little Si-C-O structure. During heat-treatment process, α-Si3N4 and β-Si3N4 formed resulting from the crystallization of amorphous silicon nitride, and the formation of β-SiC derived from the decomposition of Si-C-O structure. As heat-treated temperature increased from 1400oC to 1600oC, the above phenomenon become obvious, indicating that the fiber would possess high serving life with serving temperature lower than 1400oC. The tensile strength of fibers stays stable when heat-treated temperature was below 1200oC, while the strength retention of fibers sharply decreased to 50% after heat-treatment at 1400°C.

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