scholarly journals Green Synthesis of Silver Nanoparticles Using Extract of Cilembu Sweet Potatoes (Ipomoea batatas L var. Rancing) as Potential Filler for 3D Printed Electroactive and Anti-Infection Scaffolds

Molecules ◽  
2021 ◽  
Vol 26 (7) ◽  
pp. 2042
Author(s):  
Arie Wibowo ◽  
Gusti U. N. Tajalla ◽  
Maradhana A. Marsudi ◽  
Glen Cooper ◽  
Lia A. T. W. Asri ◽  
...  
Keyword(s):  
Silver Nanoparticles ◽  
Green Synthesis ◽  
Ipomoea Batatas ◽  
Conductive Filler ◽  
Biological Assessment ◽  
Sweet Potatoes ◽  
Transmission Electron ◽  
3D Printed ◽  
Toxic Organic Solvents ◽  
Synthesis Approach

Electroactive biomaterials are fascinating for tissue engineering applications because of their ability to deliver electrical stimulation directly to cells, tissue, and organs. One particularly attractive conductive filler for electroactive biomaterials is silver nanoparticles (AgNPs) because of their high conductivity, antibacterial activity, and ability to promote bone healing. However, production of AgNPs involves a toxic reducing agent which would inhibit biological scaffold performance. This work explores facile and green synthesis of AgNPs using extract of Cilembu sweet potato and studies the effect of baking and precursor concentrations (1, 10 and 100 mM) on AgNPs’ properties. Transmission electron microscope (TEM) results revealed that the smallest particle size of AgNPs (9.95 ± 3.69 nm) with nodular morphology was obtained by utilization of baked extract and ten mM AgNO3. Polycaprolactone (PCL)/AgNPs scaffolds exhibited several enhancements compared to PCL scaffolds. Compressive strength was six times greater (3.88 ± 0.42 MPa), more hydrophilic (contact angle of 76.8 ± 1.7°), conductive (2.3 ± 0.5 × 10−3 S/cm) and exhibited anti-bacterial properties against Staphylococcus aureus ATCC3658 (99.5% reduction of surviving bacteria). Despite the promising results, further investigation on biological assessment is required to obtain comprehensive study of this scaffold. This green synthesis approach together with the use of 3D printing opens a new route to manufacture AgNPs-based electroactive with improved anti-bacterial properties without utilization of any toxic organic solvents.

Optimization of Green Synthesis Approach of Silver Nanoparticles Using Indonesian Wild Honey

2021 ◽  
Vol 891 ◽  
pp. 111-115
Author(s):  
Maradhana Agung Marsudi ◽  
Farah Fitria Sari ◽  
Pandu Mauliddin Wicaksono ◽  
Adinda Asmoro ◽  
Arif Basuki ◽  
...  
Keyword(s):  
Electron Microscopy ◽  
Silver Nanoparticles ◽  
Green Synthesis ◽  
Synthesis Method ◽  
X Ray Diffraction ◽  
X Ray ◽  
Particle Count ◽  
Transmission Electron ◽  
Nitrate Precursor ◽  
Synthesis Approach

In this work, silver nanoparticles have been successfully synthesized using simple and environmentally friendly ‘green synthesis’ method using Indonesian wild honey as mediator. Particle count and size can be optimized by varying the silver nitrate precursor and honey concentration, with the help of sodium hydroxide as pH regulator. Based on X-ray diffraction (XRD) result, crystalline structure of Ag has been confirmed in sample with impurities from AgCl. Based on dynamic light scattering (DLS) and transmission electron microscopy (TEM) results, it was found that the smallest average particles size of AgNPs (117.5 nm from DLS and 11.1 nm from TEM) was obtained at sample with 5% w/v of honey and 0.5 mM of AgNO3.

Stability Enhancement of Silver Nanoparticles Through Surface Encapsulation via a Facile Green Synthesis Approach and Toxicity Reduction

2019 ◽  
Vol 30 (6) ◽  
pp. 1956-1965 ◽  
Author(s):  
Mahmuda Akter ◽  
A. K. M. Atique Ullah ◽  
Md. Shiblur Rahaman ◽  
Md. Mostafizur Rahman ◽  
Md. Tajuddin Sikder ◽  
...  
Keyword(s):  
Silver Nanoparticles ◽  
Green Synthesis ◽  
Toxicity Reduction ◽  
Stability Enhancement ◽  
Synthesis Approach

scholarly journals Microwave Assisted Rapid and Green Synthesis of Silver Nanoparticles Using a Pigment Produced byStreptomyces coelicolorklmp33

2013 ◽  
Vol 2013 ◽  
pp. 1-5 ◽  
Author(s):  
Deene Manikprabhu ◽  
K. Lingappa
Keyword(s):  
Silver Nanoparticles ◽  
Green Synthesis ◽  
Streptomyces Coelicolor ◽  
Biological Synthesis ◽  
Toxic Substances ◽  
X Ray Diffraction ◽  
Chemical Methods ◽  
Major Drawback ◽  
Transmission Electron ◽  
Uv Visible

Traditional synthesis of silver nanoparticles using chemical methods produces toxic substances. In contrast biological synthesis is regarded as a safe and nontoxic process but the major drawback of biological synthesis is, this process is slow. In the present investigation, we developed a rapid and green synthesis of silver nanoparticles employing a pigment produced byStreptomyces coelicolorklmp33 in just 90 s. The silver nanoparticles were characterized by UV-visible spectroscopy, transmission electron microscopy (TEM), X-ray diffraction (XRD), and Fourier transform infrared spectroscopy (FTIR). The biobased synthesis developed in this method is a safe, rapid, and appropriate way for bulky synthesis of silver nanoparticles.

A novel green synthesis approach for polymer nanocomposites decorated with silver nanoparticles and their antibacterial activity

The Analyst ◽  
2014 ◽  
Vol 139 (22) ◽  
pp. 5793-5799 ◽  
Author(s):  
Guofang Chen ◽  
Jingran Lu ◽  
Clarissa Lam ◽  
Yong Yu
Keyword(s):  
Silver Nanoparticles ◽  
Antibacterial Activity ◽  
Green Synthesis ◽  
Polymer Nanocomposites ◽  
Polymer Composite ◽  
High Purity ◽  
Synthesis Strategy ◽  
Polymer Colloid ◽  
Synthesis Approach

A novel green synthesis strategy was developed for polymer composite spheres decorated with silver nanoparticles, mediated by a polymer colloid support itself, which are very stable and of high purity with excellent antibacterial activity.

scholarly journals Green Synthesis of Hydroxyethyl Cellulose-Stabilized Silver Nanoparticles

2013 ◽  
Vol 2013 ◽  
pp. 1-11 ◽  
Author(s):  
M. A. El-Sheikh ◽  
S. M. El-Rafie ◽  
E. S. Abdel-Halim ◽  
M. H. El-Rafie
Keyword(s):  
Silver Nanoparticles ◽  
Green Synthesis ◽  
Colloidal Solution ◽  
Hydroxyethyl Cellulose ◽  
Synthesis Process ◽  
Reaction Conditions ◽  
Oh Groups ◽  
Stabilizing Agents ◽  
Transmission Electron ◽  
Optimum Reaction

Green synthesis aims to minimize the use of unsafe reactants and maximize the efficiency of synthesis process. These could be achieved by using environmentally compassionate polymers and nontoxic chemicals. Hydroxyethyl cellulose (HEC), an ecofriendly polymer, was used as both reducing and stabilizing agents in the synthesis of stable silver nanoparticles, while silver nitrate was used as a precursor and water as a solvent. The formation of silver nanoparticles was assessed by monitoring UV-vis spectra of the silver colloidal solution. The size of the nanoparticles was measured using transmission electron microscope (TEM). Reaction kinetics was followed by measuring the absorbance of silver colloidal solution at different time intervals. Optimum reaction conditions revealed that the highest absorbance was obtained using HEC : AgNO3 of 1.5 : 0.17 (g/100 cm3) at 70°C for 120 min at pH 12. The Ag0 nanoparticles colloidal solution so obtained (1000 ppm) were found stable in aqueous solution over a period of six months at room temperature (°C). The sizes of these nanoparticles were found in the range of 11–60 nm after six months of storing. FTIR spectra confirmed the interaction of both the aldehyde and OH groups in the synthesis and stabilization of silver nanoparticles.

scholarly journals Antiplasmodial activity of silver nanoparticles: A novel green synthesis approach

2018 ◽  
Vol 8 (5) ◽  
pp. 268 ◽  
Author(s):  
Sanjay Kumar ◽  
Madhur Sardana ◽  
Varnika Agarwal ◽  
Akansha Pant ◽  
Vinita Kapoor ◽  
...  
Keyword(s):  
Silver Nanoparticles ◽  
Green Synthesis ◽  
Antiplasmodial Activity ◽  
Synthesis Approach

scholarly journals Cottonseed Oilcake Extract Mediated Green Synthesis of Silver Nanoparticles and Its Antibacterial and Cytotoxic Activity

2016 ◽  
Vol 2016 ◽  
pp. 1-6 ◽  
Author(s):  
Muthusamy Govarthanan ◽  
Min Cho ◽  
Jung-Hee Park ◽  
Jum-Suk Jang ◽  
Young-Joo Yi ◽  
...  
Keyword(s):  
Electron Microscopy ◽  
Transmission Electron Microscopy ◽  
Silver Nanoparticles ◽  
Fourier Transform ◽  
Green Synthesis ◽  
Pseudomonas Syringae ◽  
X Ray Diffraction ◽  
X Ray ◽  
Transmission Electron ◽  
Xrd Techniques

Agroindustrial byproduct mediated green synthesis of silver nanoparticles was carried out using cottonseed oilcake (CSOC) extract. The aqueous silver nitrate formed stable silver nanoparticles with CSOC extract as a reducing agent for Ag+to Ag0. The synthesized nanoparticles were characterized using energy dispersive X-ray spectroscopy (EDS), transmission electron microscopy (TEM), Fourier transform infrared (FTIR) spectroscopy, and X-ray diffraction (XRD) techniques. The synthesized silver nanoparticles (AgNPs) (4 mM) significantly inhibited the growth of phytopathogens,Pseudomonas syringaepv.actinidiaeandRalstonia solanacearum. Further, cytotoxicity of AgNPs was evaluated using rat splenocyte cells. The splenocyte viability was decreased according to the increasing concentration of AgNPs and 90% of cell death was observed at 100 μg/mL.

scholarly journals Green Synthesis of Silver Nanoparticles using Polyalthia longifolia Stem Bark Extract and its Catalytic Reduction of 4-Nitrophenol

2019 ◽  
Vol 31 (11) ◽  
pp. 2439-2442
Author(s):  
Karuppiah Muthu ◽  
B. Akilandaeaswari ◽  
S. Mangala Nagasundari
Keyword(s):  
Silver Nanoparticles ◽  
Green Synthesis ◽  
Catalytic Reduction ◽  
Stem Bark ◽  
Bark Extract ◽  
Visible Spectroscopy ◽  
Transmission Electron ◽  
Stem Bark Extract ◽  
Uv Visible ◽  
Polyalthia Longifolia

In this present study, green synthesis of silver nanoparticles (AgNPs) was synthesized from silver nitrate using the reducing agents of Polyalthia longifolia bark extract and applied the catalyst in the reduction/degradation of environmental polluted organic compound in the presence of NaBH4. Initially, the colourless reaction mixture was slowly changed to yellowish brown, UV-visible spectroscopy of surface plasmon resonance centre at 447 nm confirmed the formation of AgNPs. High resolution transmission electron microscopy (HRTEM) clearly identified the spherical shapes nanoparticles with diameters sizes 5-25 nm. This AgNPs has excellent catalyst in the catalytic reduction of 4-nitrophenol (4-NP) to 4-aminophenol (4-AP) as compared to the reducing agent of NaBH4 (chemical) and plant extract (natural).

scholarly journals Green Synthesis of Silver Nanoparticles Using Astragalus tribuloides Delile. Root Extract: Characterization, Antioxidant, Antibacterial, and Anti-Inflammatory Activities

Nanomaterials ◽  
2020 ◽  
Vol 10 (12) ◽  
pp. 2383
Author(s):  
Majid Sharifi-Rad ◽  
Pawel Pohl ◽  
Francesco Epifano ◽  
José M. Álvarez-Suarez
Keyword(s):  
Silver Nanoparticles ◽  
Green Synthesis ◽  
Total Phenolics ◽  
Cost Effective ◽  
Root Extract ◽  
Transmission Electron ◽  
Vis Spectroscopy ◽  
High Efficient ◽  
Anti Inflammatory ◽  
Average Size

Today, the green synthesis of metal nanoparticles is a promising strategy in material science and nanotechnology. In this research, silver nanoparticles (AgNPs) were synthesized through the high-efficient, cost-effective green and facile process, using the Astragalus tribuloides Delile. root extract as a bioreduction and capping agent at room temperature. UV–Vis spectroscopy was applied for the investigation of the reaction proceedings. To characterize the greenly synthesized AgNPs, Fourier-transform infrared spectroscopy (FTIR), X-ray diffraction spectroscopy (XRD), and transmission electron microscopy (TEM) analyses were utilized. In addition, the total phenolics and flavonoids contents, antioxidant, antibacterial, and anti-inflammatory activities of the greenly synthesized AgNPs and the A. tribuloides root extract were evaluated. The results indicated that the AgNPs had spherical morphology and crystalline structure with the average size of 34.2 ± 8.0 nm. The total phenolics and flavonoids contents of the greenly synthesized AgNPs were lower than those for the A. tribuloides root extract. The resultant AgNPs exhibited the appropriate antioxidant activity (64%) as compared to that for the A. tribuloides root extract (47%). The antibacterial test approved the higher bactericidal activity of the resulting AgNPs on the Gram-positive and Gram-negative bacteria in comparison to the A. tribuloides root extract. Considering the anti-inflammatory activity, the greenly synthesized AgNPs showed a stranger effect than the A. tribuloides root extract (82% versus 69% at 500 μg/mL). Generally, the AgNPs that were fabricated by using the A. tribuloides root extract had appropriate antioxidant, antibacterial, and anti-inflammatory activities and, therefore, can be considered as a promising candidate for various biomedical applications.

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