Performance Evaluation of Agarwood Distillation Waste as Retarder for High Strength Oilwell Cement

2014 ◽  
Vol 548-549 ◽  
pp. 101-105
Author(s):  
A. Sauki ◽  
A. Azizi ◽  
Nur Hashimah Alias ◽  
Nurul Aimi Ghazali ◽  
T.A.T. Mohd ◽  
...  

Cement strength must be carefully maintained so that the cement is able to sustain formation stresses without failing. Such a mechanical failure in a cement sheath can cause a loss of annular isolation. A synthetic polymer cement retarder has been designed to provide extended pumping times for cement slurries, while having minimal effect on compressive strength development. However, it is difficult to select a retarder that can suit a wide range of field conditions. Fluid loss control can also be affected by the addition of a retarder, especially at high temperatures. Addition of retarder sometimes may increase the viscosity and pumping pressure of the slurry and may result in fracturing of the hydrocarbon bearing zone and costly job failure. The main idea for this study is to determine whether Agarwood waste from distillation process (AGW) can be used as a retarder in oil well cement with excellent compressive strength development. The compressive strength developments were evaluated at different curing time and particle sizes of AGW which are 90 μm, 150μm and 250μm. The performance of AGW slurries were compared with commercial retarder slurry. Apart from that, chemical analysis on AGW was conducted by using X-ray Fluorescent (XRF) to determine the presence of cementations component in this material. All cement testing procedures should follow API recommended specification 10B standard. From the results obtained, the performance of 250 μm of AGW is better than commercial retarder by 10% increment in the development of cement strength.

2015 ◽  
Vol 2015 ◽  
pp. 1-12 ◽  
Author(s):  
Keun-Hyeok Yang ◽  
Jae-Sung Mun ◽  
Myung-Sug Cho

This study examined the relative strength-maturity relationship of high-strength concrete (HSC) specifically developed for nuclear facility structures while considering the economic efficiency and durability of the concrete. Two types of mixture proportions with water-to-binder ratios of 0.4 and 0.28 were tested under different temperature histories including (1) isothermal curing conditions of 5°C, 20°C, and 40°C and (2) terraced temperature histories of 20°C for an initial age of individual 1, 3, or 7 days and a constant temperature of 5°C for the subsequent ages. On the basis of the test results, the traditional maturity function of an equivalent age was modified to consider the offset maturity and the insignificance of subsequent curing temperature after an age of 3 days on later strength of concrete. To determine the key parameters in the maturity function, the setting behavior, apparent activation energy, and rate constant of the prepared mixtures were also measured. This study reveals that the compressive strength development of HSC cured at the reference temperature for an early age of 3 days is insignificantly affected by the subsequent curing temperature histories. The proposed maturity approach with the modified equivalent age accurately predicts the strength development of HSC.


2021 ◽  
Author(s):  
Hasmukh Patel ◽  
Kenneth Johnson ◽  
Roland Martinez

Abstract The oil well cement placed in the annulus between casings and the formations experience high stresses under downhole conditions. These frequent stresses deteriorate the mechanical properties of cement and lead to the formation of micro-cracks and fractures, which affect production and increases the cost of operation. Although several polymeric materials have been employed to improve tensile properties of the cement, these additives have also adversely affected the compressive strength of the cement. A highly stable polymeric additive, triazine-based polymers, is designed, synthesized, and compounded with the cement to improve the tensile properties of the well-cement. Triazine polymer was characterized by fourier transform infrared spectroscopy and thermogravimetric analysis. The triazine polymer was mixed with cement and the cement slurries were cured at 180 °F under 3000 psi for 3 days. The set-cement samples were subjected to mechanical testing under high temperature and high pressure to study the elastic properties of the cement. The introduction of this polymer into the cement has improved the elastic properties of the cement with minimum reduction in compressive strength. The thickening time, dynamic compressive strength development, rheology, fluid loss properties, and brazilian tensile strength of the control and cement with triazine polymers were studied to understand the effect of this newly developed polymeric additive. The molecular interaction of the triazine polymer with cement particles has shown formation of covalent linkage between the polymer and cement particle. We have observed a 15 % decrease in Young's modulus for cement compounded with 2%wt. of triazine polymer, indicating the introduction of elastic properties in wellbore cement.


2014 ◽  
Vol 905 ◽  
pp. 195-198 ◽  
Author(s):  
Keun Hyeok Yang ◽  
Jae Sung Mun ◽  
Jae Eun Jeong

The present study examined the in-place strength of high-strength concrete based on the relative strength-maturity relationship. The measured strength gain of high-strength concrete was compared with the predictions obtained from the modified maturity function to consider the offset maturity and the insignificance of subsequent curing temperature after an age of 3 days on later strength of concrete. This study demonstrates that the compressive strength gain of concrete cured at the reference temperature (20°C) for an early age of 3 days is little affected by the subsequent curing temperature histories.


2015 ◽  
Vol 802 ◽  
pp. 214-219 ◽  
Author(s):  
Aktham Hatem Alani ◽  
Megat Azmi Megat Johari

The influence of silica fume (SF) inclusion on the compressive strength development of high strength concrete (HSC) containing high volume of palm oil fuel ash (POFA) has been investigated. A HSC containing 100% ordinary Portland cement (OPC) and another HSC mix with 50% POFA as part of the binder were prepared. Due to the reduction in early strength of the HSC with the inclusion of high volume of POFA in the binary blended binder HSC, attempt was made to partially replace the OPC with SF at 5, 10, 15 and 20%, thus creating a ternary blended binder HSC. The results show that the compressive strength development of the HSC containing high volume of POFA was significantly improved with the inclusion of SF. The ternary blended binder HSC with 15% SF exhibited the highest increase in early age strength, even though it did not surpass the OPC-HSC, and it provided the highest strength at 7 and 28 days in comparison to other HSC mixes. Thus, ternary blended binder containing more than 60% supplementary cementitious material (POFA and SF) could be utilized to produce HSC.


2016 ◽  
Vol 872 ◽  
pp. 271-275 ◽  
Author(s):  
Mochamad Solikin

This paper presents a research to produce high strength concrete incorporated with fly ash as cement replacement up to 50% (high volume fly ash concrete) by using local material. The research is conducted by testing the strength development of high volume fly ash concrete at the age of 14 days, 28 days and 56 days. As a control mix, the compressive strength of Ordinary Portland Cement (OPC) concrete without fly ash is used. Both concrete mixtures use low w/c. consequently, they lead to the use of 1 % superplasticizer to reach sufficient workability in the process of casting. The specimens are concrete cubes with the dimension of 15 cm x15 cm x 15 cm. The totals of 24 cubes of HVFA concrete and OPC concrete are used as specimens of testing. The compressive strength design of concrete is 45 MPa and the slump design is ± 10 cm. The result shows that the compressive strengths of OPC concrete at the age of 14 days, 28 days, and 56 days are 38 MPa, 40 MPa, and 42 MPa. Whereas the compressive strength of HVFA concrete in the same age of immersing sequence are 29 MPa, 39 MPa, and 42 MPa. The result indicates that HVFA concrete can reach the similar compressive strength as that of normal concrete especially at the age of 56 days by deploying low water cement ratio.


2021 ◽  
Author(s):  
Mahamat Habib Abdelkerim Doutoum ◽  
Romulo Francisco Bermudez Alvarado ◽  
Ahmed Rashed Alaleeli ◽  
Thein Zaw Phyoe ◽  
Jose Salazar ◽  
...  

Abstract Lost circulation while drilling across vugular or naturally fractured limestone formations is a costly challenge and has financial impacts including nonproductive time and remedial operational expenses. Many fields in the UAE are encountering notorious lost circulation complications, which are difficult to control with conventional lost circulation solutions while drilling surface sections. Novel lightweight thixotropic cement has proven beneficial to take control of severe losses in these vugular and naturally fractured limestone formations. The main challenge while drilling across the surface section in UAE offshore field is the heavy or total loss of returns. Drilling performance is affected due to poor hole cleaning, a risk of stuck pipe, surface fluid handling problems, and well control risks. Conventional extended cement slurries have been widely used to cure losses while drilling but with limited success. A new lost circulation solution combines lightweight (10.5- lbm/galUS) high solids fraction cement (trimodal system) and a thixotropic agent, which develop fast gels with high compressive strength. Thus, it enables plugging of large voids and fractures to deliver the wellbore integrity required to continue drilling with enhanced performance and efficiency. Intensive laboratory qualification tests focusing on static gel strength and compressive strength development was performed to tailor the new solution. The results were promising with more than 100 lbf/100 ft2 of static gel strength in 10 minutes and compressive strength development of 1,000 psi within 24 hours at low surface temperature. In addition, a transition time (TT) on-off-on test demonstrated more rapid gel strength development when the shear is reduced and regained fluidity with reapplication of shear. In one of the wells, heavy losses were encountered while drilling across surface section. The lightweight thixotropic solution was pumped for the first time worldwide and it was shown that the innovative lost circulation solution was effective in significantly reducing the losses and enabled the operator to continue drilling to section TD. This case study demonstrates that this advanced system is effective in curing losses and reducing nonproductive time. The unique properties of faster rapid gel strength and high compressive strength make this solution effective for treating a wide range of lost circulation events while drilling. Furthermore, the advanced lightweight thixotropic cement lost circulation solution exhibits strong performance in curing heavy losses and establishing well integrity with reliability.


1983 ◽  
Vol 10 (4) ◽  
pp. 600-613 ◽  
Author(s):  
Claude Bedard ◽  
Pierre-Claude Aitcin

It is possible to make in 1983 a field concrete in the Montreal area having a 28-day compressive strength of 120 MPa, using locally available materials.To obtain such a high compressive-strength concrete, it has been necessary to study the overall performances of 8 different cements, 3 types of sand, 16 types of aggregates, 3 types of superplasticizers, 9 grain-size distributions of the coarse aggregate, and 5 different ways of batching. An ultra high strength concrete is not obtained by chance, but through a long research effort planned in a laboratory as well as in the field.Such a concrete is feasible using: (1) high cement dosage of type 10, 20, or 30, according to the desired rate of compressive strength development; (2) a cubical coarse aggregate having a high compressive strength and an elastic modulus as near as possible as that of the mortar; (3) a manufactured sand having a high fineness modulus made from the same rock as the coarse aggregate; (4) a very high dosage of superplasticizer; and (5) 5 to 8% of condensed silica fume. The limited efficiency of the present industrial mixers (tilt mixers) for the very special mixes of this study is actually the main limitation for reaching a strength of 150 MPa. Keywords: high compressive strength concrete, superplasticizer, condensed silica fumes, manufactured sand, grain-sizes, aggregates, retarder, ready-mix concrete, precast plants.


2020 ◽  
Vol 1 ◽  
Author(s):  
Mohammed A. Hefni

Abstract The use of natural pozzolans in concrete applications is gaining more attention because of the associated environmental, economic, and technical benefits. In this study, reference cemented mine backfill samples were prepared using Portland cement, and experimental samples were prepared by partially replacing Portland cement with 10 or 20 wt.% fly ash as a byproduct (artificial) pozzolan or pumice as a natural pozzolan. Samples were cured for 7, 14, and 28 days to investigate uniaxial compressive strength development. Backfill samples containing 10 wt.% pumice had almost a similar compressive strength as reference samples. There is strong potential for pumice to be used in cemented backfill to minimize costs, improve backfill properties, and promote the sustainability of the mining industry.


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