A New Method in Producing Ni Deposited Hydroxyapatite Composite by Modification of Electroless Deposition Technique

2014 ◽  
Vol 699 ◽  
pp. 99-104
Author(s):  
M.A. Sri Asliza ◽  
K. Mohd Zaheruddin ◽  
Azmi Rahmat ◽  
Shamsul Baharin Jamaludin ◽  
Rafezi Ahmad Khairel
Keyword(s):  
Electroless Deposition ◽  
Deposition Technique ◽  
X Ray Diffraction ◽  
Tetracalcium Phosphate ◽  
X Ray ◽  
Hydroxyapatite Powder ◽  
Hydroxyapatite Composite ◽  
Before And After ◽  
Surface Morphologies ◽  
Scanning Electron

Ni deposited Hydroxyapatite powder was prepared by electroless deposition technique without sensitization and activation treatments. The composition and phase of deposition were studied. The surface morphologies and composition of initial pure HA powder, as received Ni deposited HA powder and compacted Ni deposited HA powder after sintering were characterized by scanning electron microscopy (SEM) and energy dispersive spectroscopy (EDS) respectively. The phases in the powder before and after sintering were investigated by x-ray diffraction (XRD). From the experiment, with the increase of reduction agent, the plating time becomes shorter and optimal concentration of reduction agent and powder ratio is 3:1. The result shows that Ni succesfully deposited on HA powder and confirmed by EDX result. The Ni grain size distribution of 75nm to 250nm can be clearly observed on the HA surface from the micrograph after sintering. Decomposition of hydroxyapatite into α-TCP (α tricalcium phosphate) and TTCP (tetracalcium phosphate) did not occur in nickel deposited HA before and after sintering. On the other hand, a sharp Ni peak were detected

Development of Dense Hydroxyapatite-Ni by Modified Electroless Deposition Technique

2013 ◽  
Vol 594-595 ◽  
pp. 306-310 ◽  
Author(s):  
Sri Asliza Md Amin ◽  
Kasmuin Mohd Zaheruddin ◽  
Azmi Rahmat ◽  
Shamsul Baharin Jamaludin ◽  
R.A. Khairel
Keyword(s):  
Electron Microscopy ◽  
Scanning Electron Microscopy ◽  
Electroless Deposition ◽  
Deposition Technique ◽  
X Ray Diffraction ◽  
X Ray ◽  
Average Hardness ◽  
Sintered Powder ◽  
Diffraction Peaks ◽  
Scanning Electron

Ni deposited on HA powder was prepared by electroless plating process without sensitization and activation treatment. The deposited powder obtained was characterized by energy dispersive spectroscopy (EDX) and x-ray diffraction (XRD). The microstructure and hardness of the sintered powder were examined by scanning electron microscopy (SEM) and Vickers hardness respectively. From the result, the nickel existence in the deposition was confirmed by the EDX analysis. The diffraction peaks at 44.5 and 64.7o (2θ) of planes (111) and (211) respectively were belong to nickel. Nickel are homogeneously dispersed in HA matrix with grain size between 0.25-2μm after sintered at 1250°C. The improvement of 93% and 180% in average hardness and flexural strength respectively were achieved with nickel presence in HA compared to pure HA.

Synthesis and Comparison of Boron Nitride Nanostructure Prepared on Silicon and Molybdenum Substrates by Laser Plasma Deposition Technique

2011 ◽  
Vol 1307 ◽  
Author(s):  
M. Sajjad ◽  
H. X. Zhang ◽  
P. X. Feng
Keyword(s):  
Electron Microscopy ◽  
Boron Nitride ◽  
Plasma Deposition ◽  
Nitrogen Concentration ◽  
Deposition Technique ◽  
X Ray Diffraction ◽  
Experimental Conditions ◽  
X Ray ◽  
Si Substrates ◽  
Scanning Electron

ABSTRACTThe synthesis of boron nitride nanowires on silicon (Si) and nanorods on molybdenum (Mo) substrates at the same experimental conditions was composed. Fine tip nanowires with diameters around 50 nm were produced on Si substrates, whereas, nanorods with diameter around 100 nm were formed on Mo substrates. The change in length from 5 μm to 100 μm for nanowires and 0.2 μm to 0.8μm for nanorods following variation of substrate temperature were studied systematically.Scanning Electron Microscopy was used to analyze the surface images of BN nanowires and nanorods. Energy Dispersive X-Ray spectroscopy (EDS) was used to analyze boron and nitrogen concentration in the samples. The crystal structures of BN samples were investigated using Raman spectroscopy and x-ray diffraction. The experimental results showed that the nanorods are hexagonal mixed with cubic, whereas the nanowires are hexagonal.

Microstructure of In Situ Reaction TiB2/Zn-30Al-1Cu Composites Prepared by Spray Deposition Process

2015 ◽  
Vol 1120-1121 ◽  
pp. 572-575
Author(s):  
Hong Wei Liu ◽  
Feng Wang ◽  
Qiang Zhang ◽  
Xi Wu Li ◽  
Zhi Hui Li ◽  
...  
Keyword(s):  
Electron Microscopy ◽  
Scanning Electron Microscopy ◽  
Spray Deposition ◽  
Deposition Process ◽  
Deposition Technique ◽  
X Ray Diffraction ◽  
X Ray ◽  
Α Phase ◽  
Scanning Electron

An innovative spray deposition technique has been applied to produce in situ TiB2/Zn-30Al-1Cu composites. The microstructures of the spray-deposited composite were studied using optical microscopy, scanning electron microscopy, and X-ray diffraction. Both theoretical and experimental results have shown that the TiB2particulates are formed in the microstructure. It was found that the TiB2particles were distributed in Zn-30Al-1Cu matrix uniformly, and the TiB2particles are about 2 μm in size. Moreover, the presence of the TiB2particles was led to increasing of α’ phase with less 2 μm size in the composites which have a tendency to decompose to α+η structure.

The Effects of Ternary Elemental Additions on the Structure and Magnetic Properties of Nanocrystalline Feco Powders

2002 ◽  
Vol 753 ◽  
Author(s):  
I. Baker ◽  
R. G. Quiller ◽  
M. Robson ◽  
D. Wu
Keyword(s):  
Magnetic Properties ◽  
Vibrating Sample Magnetometer ◽  
X Ray Diffraction ◽  
X Ray ◽  
Grain Sizes ◽  
Before And After ◽  
Diffraction Peaks ◽  
Computer Controlled ◽  
Steel Balls ◽  
Scanning Electron

ABSTRACTPowders of near-equiatomic Fe and Co were mechanically milled with additions of Zr, C, Ni, Cu and/or B for 60 hr using stainless steel balls in a Svegari attritor operated at 1300 r.p.m. under argon. The milled powders were examined before and after annealing at 600 °C. The morphologies and sizes of the powders were examined using a scanning electron microscope. The grain sizes were characterized from the widths of X-ray diffraction peaks obtained using a computer-controlled x-ray diffractometer and the lattice parameters were determined. The resulting magnetic properties were measured using a vibrating sample magnetometer.

Biocompatibility Research of Medicine Titanium Alloy Coating by Microarc Oxidation

2011 ◽  
Vol 189-193 ◽  
pp. 222-226
Author(s):  
Feng Biao Wang ◽  
Shi Chun Di ◽  
Jie Yu
Keyword(s):  
Titanium Alloy ◽  
Body Fluid ◽  
Oxidation Process ◽  
Microarc Oxidation ◽  
Alloy Coating ◽  
P Value ◽  
X Ray Diffraction ◽  
X Ray ◽  
Surface Morphologies ◽  
Scanning Electron

A medicinal titanium alloy hydroxyapatite coating was fabricated by microarc oxidation process, and a kind standard of simulated body fluid was configured, after that the biocompatibility experiment was carried out. The soaked coatings surface morphologies were observed and analysed by scanning electron microscopy,and the coating spectra were simultaneityly researched by X-ray diffraction. The instance of degradation and precipitate were investigated,and the transformation of Ca/P value were measured.

scholarly journals Hydroxyapatite Extracted from Waste Fish Bones and Scales via Calcination Method

2015 ◽  
Vol 773-774 ◽  
pp. 287-290 ◽  
Author(s):  
N. Mustafa ◽  
Mohd Halim Irwan Ibrahim ◽  
Rosli Asmawi ◽  
Azriszul Mohd Amin
Keyword(s):  
Chemical Reaction ◽  
Fish Bone ◽  
Powder Size ◽  
X Ray Diffraction ◽  
Calcination Process ◽  
X Ray ◽  
Calcination Temperatures ◽  
Hydroxyapatite Powder ◽  
Before And After ◽  
Calcination Method

A hydroxyapatite is known as one of vital materials and common use in biomedical field and concentrated in clinical area. In relation to the above, the development of hydroxyapatite powder becomes an attractive research lines due to simplify in produce it. Thus in this paper the researcher stress out about Hydroxyapatite powder gained from the natural sources or so called as the waste of Tilapia bone and scales. The raw bones of and scale were undergo to crushing process to form in powder size (0.2 mm) then analysed by X-ray Diffraction (XRD) to identified the mineralogy of raw bone. Moreover the powder of fish bone and scales also go through to Scanning Electron Microscope (SEM) machine to analyse the microstructure of the powder while EDS act as device to determine the chemical composition of the sample powder. Sample powder then forward calcination process at selected temperature range to as a cheaper method in obtained hydroxyapatite raw sources. The range of calcination temperatures are between 800°C to 1000 °C. The sample preparation were analysed in both condition before and after calcination process by using XRD, SEM and EDS. The HAP crystalline composition of tilapia bones for raw powder and at 800 °C are similar with HAP pattern (JDS 00-009-0432) and the chemical reaction is Ca5(PO4)3(OH) then at temperature 900 and 1000 similar to HAP pattern (JDS 00-055-0592) with chemical reaction equal to Ca10(PO4)6(OH)2.

The Effect of Regeneration Conditions on the Properties of CeO2 Desulfurization Sorbent in SO2 Atmosphere

2017 ◽  
Vol 896 ◽  
pp. 155-161
Author(s):  
Lei Yang ◽  
Shang Guan Ju ◽  
Hui Qing Wang ◽  
Jia An ◽  
Jun Ming Yu ◽  
...  
Keyword(s):  
Electron Microscope ◽  
Elemental Sulfur ◽  
Fixed Bed ◽  
Fixed Bed Reactor ◽  
X Ray Diffraction ◽  
X Ray ◽  
Before And After ◽  
Regeneration Condition ◽  
Main Components ◽  
Scanning Electron

CeO2 desulfurization sorbent was prepared by calcination of Ce(NO3)3 ● 6H2O and the effect of regeneration conditions on its properties in SO2 atmosphere was investigated in a fixed bed reactor. The regeneration conversion and the yield of elemental sulfur for CeO2 desulfurization sorbent were tested and calculated. And the composition and the morphology of CeO2 desulfurization sorbent before and after regeneration were obtained by X-ray diffraction and scanning electron microscope. It was found that the main components of the regeneration products of Ce2O desulfurization sorbent were solid CeO2 and gaseous elemental S in SO2 atmosphere. The optimum regeneration condition of CeO2 desulfurization sorbent is that the regeneration temperature of 750 °C and the SO2 concentration of 4.25 %, under which the CeO2 desulfurization sorbent shows the higher regeneration conversion of 96 % and the yield of elemental sulfur of 68.95 wt. %.

Microstructural Characterization of In Situ Reaction TiB2/Zn-30Al-1Cu Composites Prepared by Spray Deposition Process

2014 ◽  
Vol 1015 ◽  
pp. 688-691 ◽  
Author(s):  
Feng Wang ◽  
Qiang Zhang ◽  
Bai Qing Xiong ◽  
Yong An Zhang ◽  
Hong Wei Liu ◽  
...  
Keyword(s):  
Spray Deposition ◽  
Microstructural Characterization ◽  
Deposition Process ◽  
Deposition Technique ◽  
X Ray Diffraction ◽  
X Ray ◽  
Transmission Electron ◽  
Scanning Electron

An innovative spray deposition technique has been applied to produce in situ TiB2/Zn-30Al-1Cu composites. The microstructures of the spray-deposited composite were studied using scanning electron microscopy, transmission electron microscope and X-ray diffraction. The results have shown that the TiB2particulates are formed in the microstructure. It was found that the TiB2particles were distributed in Zn-30Al-1Cu matrix uniformly, and the TiB2particles are about 2μm in size.

Anodization of Sputtered Titanium Films

2007 ◽  
Vol 1023 ◽  
Author(s):  
Deepak Dhawan ◽  
Suresh K. Bhargava ◽  
Wojtek Wlodarski ◽  
Kourosh Kalantar-zadeh
Keyword(s):  
Thin Films ◽  
Ammonium Fluoride ◽  
X Ray Diffraction ◽  
X Ray ◽  
Anodization Process ◽  
Titanium Thin Films ◽  
Anodized Titanium ◽  
Surface Morphologies ◽  
Micro Structures ◽  
Scanning Electron

AbstractNanoporous Ti (and TiOx) has been formed by anodization of RF sputtered titanium thin films. A solution of 1M (NH4)2SO4 (ammonium sulphate) electrolytes containing 0.5wt% (NH4)F (ammonium fluoride) was used in the anodization process. Different nano and micro structures were obtained. Voltage in a rage of 2 to 10V was employed in the process. It was observed that the magnitude of applied voltage have a significant impact in the formation of different surface morphologies with various nano/micro structures. The anodized titanium thin films were characterised using scanning electron microscopy and X-ray diffraction techniques.

Study on Spheroidization of Niobium Powders by RF Plasma Processing

2013 ◽  
Vol 442 ◽  
pp. 22-26
Author(s):  
Jian Jun Wang ◽  
Jun Jie Hao ◽  
Zhi Meng Guo
Keyword(s):  
Electron Microscopy ◽  
Scanning Electron Microscopy ◽  
Feeding Rate ◽  
Plasma Processing ◽  
Argon Plasma ◽  
Rf Plasma ◽  
X Ray Diffraction ◽  
X Ray ◽  
Before And After ◽  
Scanning Electron

Spherical niobium powders were synthesized by (RF) argon plasma with irregular niobium powders in this paper. The objective of the present work was to investigate how the feeding rate influence the spheroidization efficiency. The phase composition, morphology and particle size distribution of the powders before and after spheroidization were characterized by X-ray diffraction (XRD), scanning electron microscopy (SEM) and laser micron sizer (LMS). The results show that niobium powders after plasma processing have good dispersity and smooth surfaces, and their spheroidization ratio is almost 100%. The apparent density and flowability of the powder with the spheroidization efficiency 100% is 4.35 g/cm3 and 12.51 s/(50g), respectively. With the increasing of the feeding rate, the spheroidization ratio of niobium powders drops gradually.

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