Preparation of α High-Strength Gypsum from FGD Gypsum by Autoclaved Semi-Dry Process

2014 ◽  
Vol 1051 ◽  
pp. 230-236
Author(s):  
Ying Li ◽  
Peng Xuan Duan ◽  
Yuan Chao Miao ◽  
Qing Li

This paper introduced the characteristics of α high-strength gypsum preparation from FGD gypsum by autoclaved semi-dry process. The compositions of the product in different stages of the reaction and the effects of crystal modifiers on the morphology of the α-HH crystals were examined and compared. The properties of α-HH and the feature of hydration products of α-HH were investigated. The results indicated that the α-HH crystals were well-shaped with the aspect ratio of 1 and the compressive strength of the α-HH could reach or exceed 60MPa. In the new process, the reaction time could be significantly shortened to 2.5hrs, which was much shorter than the conventional process. This process could be widely applied to prepare α high-strength gypsum with phosphogypsum, citric acid gypsum, etc.

2010 ◽  
Vol 150-151 ◽  
pp. 1754-1757 ◽  
Author(s):  
Peng Liu ◽  
Zhi Wu Yu ◽  
Ling Kun Chen ◽  
Zhu Ding

The influence of curing time on the mechanical property of the phosphoaluminate cement (PAC) was investigated, and the mechanism was discussed as well. The phase composition and morphology of hydration products, electrical properties, porosity and pore size distribution of PAC cured different age were analyzed with XRD, EIS and MIP. The results showed PAC has the property of early-high strength, and the compressive strength of PAC cured for 1 day was about 70% of 28 days’. The main hydration products of PAC are micro-crystal phase and gel of phosphate and phosphoaluminate which formed compacter microstructure. In addition, there are no calcium hydroxide (CH) and ettringite (AFt) produced during the process of hydration. The compressive strength of PAC increased with age, which was due to more products continuously produced. The ac resistance analysis manifested as the change of the nyquist pattern and resistance value.


2010 ◽  
Vol 150-151 ◽  
pp. 1750-1753
Author(s):  
Ya Ping Wu ◽  
Yin Hui Wang ◽  
Li Xia Wang ◽  
Zu Guang Bian

The influence of curing time on the mechanical property of the phosphoaluminate cement (PAC) was investigated, and the mechanism was discussed as well. The phase composition and morphology of hydration products, electrical properties, porosity and pore size distribution of PAC cured different age were analyzed with XRD, EIS and MIP. The results showed PAC has the property of early-high strength, and the compressive strength of PAC cured for 1 day was about 70% of 28 days’. The main hydration products of PAC are micro-crystal phase and gel of phosphate and phosphoaluminate which formed compacter microstructure. In addition, there are no calcium hydroxide (CH) and ettringite (AFt) produced during the process of hydration. The compressive strength of PAC increased with age, which was due to more products continuously produced. The ac resistance analysis manifested as the change of the nyquist pattern and resistance value.


2020 ◽  
Vol 1012 ◽  
pp. 284-288
Author(s):  
Beatryz Cardoso Mendes ◽  
Rita de Cássia Silva Sant’Ana Alvarenga ◽  
Délio Porto Fassoni ◽  
Leonardo Gonçalves Pedroti ◽  
Afonso Rangel Garcez de Azevedo ◽  
...  

The influence of citric acid in the properties of high strength Portland cement pastes and mortars, both in fresh and hardened condition, was evaluated. The content of citric acid varied from 0 to 0.8 wt%. Tests were carried out in cement pastes to determine the water required for normal consistency and initial and final setting times. Mortars cements were tested to define bulk density, consistency index, air content in the fresh condition and compressive strength after 7, 14, and 28 days. Analysis by XRD was also performed. The results showed that the use of citric acid as a retardant additive is a viable procedure, because it increased the mechanical strength after 14 days and improved the mortar workability.


2014 ◽  
Vol 602-603 ◽  
pp. 262-265
Author(s):  
Lei Ning ◽  
Jin Hong Li ◽  
Qi Zhang ◽  
Ting Ting Qian

In this research, high strength and lightweight wall materials were made from oil shale ash (OSA) by grinding, mixing, casting molding, autoclave curing processes, et al. Factors influencing the bulk density and compressive strength of the wall materials were discussed in detail. X-ray diffraction (XRD) analysis and scanning electron microscopy (SEM) analysis were used to characterize the samples. The results indicated that the compressive strength can reach up to 13.42 MPa when the bulk density reduced to 1.11g/cm3 introduced 72.00 % of OSA, the wall materials showed thermal conductivity of 0.12~0.14 W/m k. The main hydration products of the wall materials were calcium hydroxide [Ca (OH)2], C-S-H gelation and hydrogrossular [Ca3Al2(SiO4)(OH)8]. These hydration products are prodominently C-S-H gelation bonded the solid raw materials together tightly and play a great contribution to the compressive strength of wall materials.


Alloy Digest ◽  
2015 ◽  
Vol 64 (4) ◽  

Abstract This producer has pioneered the development of the -T77 temper, a high strength corrosion resistant temper for Alloy 7150 plate and extrusions. Alloy 7150-T77 provides weight savings opportunities in structure governed by static strength requirements but where "overaged" condition corrosion resistance is required. This datasheet provides information on composition, tensile properties, and compressive strength. It also includes information on corrosion resistance as well as forming. Filing Code: Al-442. Producer or source: Alcoa Mill Products Inc..


Alloy Digest ◽  
2010 ◽  
Vol 59 (1) ◽  

Abstract Kubota KNC-03 is a grade with a combination of high strength and excellent resistance to oxidation. These properties make this alloy suitable for long-term service at temperature up to 1250 deg C (2282 deg F). This datasheet provides information on physical properties, hardness, elasticity, tensile properties, and compressive strength as well as creep. It also includes information on high temperature performance as well as casting and joining. Filing Code: Ni-676. Producer or source: Kubota Metal Corporation, Fahramet Division. See also Alloy Digest Ni-662, April 2008.


Alloy Digest ◽  
1965 ◽  
Vol 14 (9) ◽  

Abstract MALLORY 53B is an economical copper alloy combining high strength with high heat and electrical conductivity and excellent corrosion resistance. It is heat treatable. This datasheet provides information on composition, physical properties, hardness, elasticity, tensile properties, and compressive strength. It also includes information on corrosion resistance as well as forming, heat treating, and machining. Filing Code: Cu-155. Producer or source: P. R. Mallory & Company Inc..


Alloy Digest ◽  
1960 ◽  
Vol 9 (3) ◽  

Abstract ELEKTRON AZM is a magnesium extrusion alloy having a high strength level. This datasheet provides information on composition, physical properties, hardness, elasticity, tensile properties, and compressive strength as well as fracture toughness and fatigue. It also includes information on corrosion resistance as well as forming, heat treating, machining, joining, and surface treatment. Filing Code: Mg-45. Producer or source: Magnesium Elektron Ltd.


Alloy Digest ◽  
2020 ◽  
Vol 69 (11) ◽  

Abstract Meehanite GB300 is a pearlitic gray cast iron that has a minimum tensile strength of 300 MPa (44 ksi), when determined on test pieces machined from separately cast, 30 mm (1.2 in.) diameter test bars. This grade exhibits high strength while still maintaining good thermal conductivity and good machinability. It is generally used for applications where the thermal conductivity requirements preclude the use of other higher-strength materials, such as spheroidal graphite cast irons, which have inferior thermal properties. This datasheet provides information on physical properties, hardness, tensile properties, and compressive strength as well as fatigue. It also includes information on low and high temperature performance as well as heat treating, machining, and joining. Filing Code: CI-75. Producer or source: Meehanite Metal Corporation.


Alloy Digest ◽  
1970 ◽  
Vol 19 (2) ◽  

Abstract ALLEGHENY ALMAR-362 is an age-hardenable martensitic stainless steel recommended for applications requiring high strength and good corrosion resistance, such as aircraft and missile structures, hydraulic and pneumatic equipment components, and in the chemical processing industry. This datasheet provides information on composition, physical properties, hardness, elasticity, tensile properties, and compressive strength as well as fracture toughness. It also includes information on corrosion resistance as well as casting, forming, heat treating, machining, joining, and surface treatment. Filing Code: SS-234. Producer or source: Allegheny Ludlum Corporation.


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