Reaction Sintering of NiTi-Ti2Ni-TiC under Cubic High Pressure

2010 ◽  
Vol 143-144 ◽  
pp. 703-706
Author(s):  
Rui Song Yang ◽  
Ming Tian Li ◽  
Fang Wei Luo

In this paper, NiTi-Ti2Ni-TiC composite powders were first prepared by in-situ reaction in molten salt and then sintered by a cubic high pressure apparatus under 8 GPa to produce bulk composite material at a short time. It was found that the composite was composed of TiC particles embedded in NiTi-Ti2Ni matrix, in which the Ti2Ni encapsulated TiC particles. The martensitic transformation of the NiTi matrix was evidenced by differential scanning calorimetry analysis. The research on the sintering mechanism shows that there may be a reaction like TiC +Ti2Ni 􀃆 Ti2C + NiTi existing under the pressure up to 8 GPa

2000 ◽  
Vol 644 ◽  
Author(s):  
Y.X. Zhuang ◽  
L. Gerward ◽  
J.Z. Jiang ◽  
J.S. Olsen ◽  
Y. Zhang ◽  
...  

AbstractThe crystallization of bulk Zr48Nb8Cu14Ni12Be18metallic glass has been investigated by differential scanning calorimetry (DSC) and X-ray powder diffraction. The activation energies of glass transition and crystallization for the glass obtained using Kissinger analysis from the shift of the peak temperature in the DSC curve are 470 and 235 kJ/mol, respectively. The effect of applied pressure on crystallization is studied by in situ high-pressure and high-temperature X-ray powder diffraction using synchrotron radiation. It is found that the crystallization temperature increases with pressure having a slope of 9.5 K/GPa in the range of 0-4.4 GPa.


CrystEngComm ◽  
2017 ◽  
Vol 19 (34) ◽  
pp. 4992-5000 ◽  
Author(s):  
C. Bartha ◽  
C. E. Secu ◽  
E. Matei ◽  
M. Secu

The crystallization mechanism of sol–gel-derived NaYF4:(Yb,Er) up-converting phosphors has been studied by differential scanning calorimetry analysis using both model-free and model fitting approaches.


2016 ◽  
Vol 643 ◽  
pp. 65-72 ◽  
Author(s):  
Dmitry R. Streltsov ◽  
Alexander I. Buzin ◽  
Petr V. Dmitryakov ◽  
Pawel Kamasa ◽  
Dimitri A. Ivanov ◽  
...  

2018 ◽  
Vol 24 (02) ◽  
pp. 22-25
Author(s):  
Dovchinvanchig M ◽  
Chunwang Zhao

The nanocrystal, phase transformation and microstructure behavior of Ni50Ti50 shape memory alloy was investigated by scanning electronic microscope, X-ray diffraction and differential scanning calorimetry. The results showed that the microstructure of Ni-Ti binary alloy consists of the NiTi2 phase and the NiTi matrix phase. One-step phase transformation was observed alloy.


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