Preparation and Characterization of Ag, Au and Ti Metal Nanoparticles Colloids by Pulsed Laser Ablation in Liquids

2011 ◽  
Vol 415-417 ◽  
pp. 648-651 ◽  
Author(s):  
Bing Xu ◽  
Ren Guo Song ◽  
Chao Wang
Keyword(s):  
Particle Size ◽  
Laser Ablation ◽  
Metal Nanoparticles ◽  
Pulsed Laser ◽  
Pulsed Laser Ablation ◽  
Average Diameter ◽  
Transmission Electron ◽  
Particle Size And Morphology ◽  
Size And Morphology

Ag, Au and Ti metal nanoparticles colloids have been prepared by pulsed laser ablation in various liquids. The particle size and morphology of the obtained nanoparticles colloids were characterized by transmission electron microscopy (TEM), the average diameter and its distribution were analyzed by Image-ProPlus software. The results showed that the Au nanoparticles were of the best characterization, the average diameter was the smallest (D=8.79 nm), and also, the distribution of particle size was the narrowest (=17.5 nm) and the morphologies were more homogeneous.

Effect of Laser Fluence on Siliver Nanoparticles Colloid

2011 ◽  
Vol 415-417 ◽  
pp. 747-750
Author(s):  
Bing Xu ◽  
Ren Guo Song ◽  
Chao Wang
Keyword(s):  
Electron Microscopy ◽  
Silver Nanoparticles ◽  
Laser Ablation ◽  
Laser Fluence ◽  
Pulsed Laser ◽  
Pulsed Laser Ablation ◽  
Average Diameter ◽  
Distilled Water ◽  
Transmission Electron ◽  
Silver Target

In order to study the effects of laser fluence on silver nanoparticles colloid, the silver nanoparticles colloid was prepared by pulsed laser ablation of silver target for 10min in distilled water at different laser fluence. The particles size，morphologies and absorption spectroscopy of the obtained nanoparticles colloid were characterized by ultraviolet to visible (UV-Vis) spectrometer and transmission electron microscopy (TEM), the average diameter and its distribution were analyzed by Image-ProPlus software. The results shown that the average diameter of the silver nanoparticles prepared at the laser fluence of 4.2J/cm2 was the smallest (D=17.54nm), also, the distribution of particle size was narrowest (=36.86nm) and the morphologies were more homogeneous. It was confirmed that the nanoparticles size and shape could be controlled by pulsed laser ablation parameters.

Preparation of Ag Nanoparticles Colloid by Pulsed Laser Ablation in Distilled Water

2008 ◽  
Vol 373-374 ◽  
pp. 346-349 ◽  
Author(s):  
Bing Xu ◽  
Ren Guo Song ◽  
P.H. Tang ◽  
J. Wang ◽  
Guo Zhong Chai ◽  
...  
Keyword(s):  
Laser Ablation ◽  
Ag Nanoparticles ◽  
Surface Active Agent ◽  
Active Agent ◽  
Pulsed Laser ◽  
Pulsed Laser Ablation ◽  
Average Diameter ◽  
Distilled Water ◽  
Ablation Efficiency ◽  
Transmission Electron

The Ag nanoparticles colloid was prepared by pulsed laser ablation for different time in 10 ml distilled water without any surface active agent, and it was analysed by means of UV-visible spectrophotometer and transmission electron microscopy (TEM). The results showed that the ablation efficiency and absorbance increased fast and shift to higher energies with increasing ablation time from 5 to 10 min, then increased slowly from 10 to 20 min, and increased fast again from 20 to 25 min. The morphologies of most Ag nanoparticles were nearly spherical. The average diameter and its distribution decreased from 5 to 7.5 min, then increased from 7.5 to 15 min, and decreased from 15 to 25 min.

Characterization of deposits produced by TEA CO2 pulsed laser ablation of silicon mono- and dioxide

2005 ◽  
Vol 351 (2) ◽  
pp. 116-123 ◽  
Author(s):  
Vladislav Dřínek ◽  
Karel Vacek ◽  
Josef Pola ◽  
Gleb Yuzhakov ◽  
Olga Šolcová ◽  
...  
Keyword(s):  
Laser Ablation ◽  
Pulsed Laser ◽  
Pulsed Laser Ablation

Laser assisted synthesis of WS2 nanorods by pulsed laser ablation in liquid environment

2021 ◽  
pp. 2140007
Author(s):  
Pankaj Koinkar ◽  
Kohei Sasaki ◽  
Tetsuro Katayama ◽  
Akihiro Furube ◽  
Satoshi Sugano
Keyword(s):  
Electron Microscopy ◽  
Laser Ablation ◽  
2D Materials ◽  
Pulsed Laser ◽  
Pulsed Laser Ablation ◽  
Laser Ablation In Liquid ◽  
Simple Method ◽  
Liquid Environment ◽  
Transmission Electron ◽  
Specific Morphology

Two dimensional (2D) materials are widely attracting the interest of researchers due to their unique crystal structure and diverse properties. In the present work, tungsten disulfide (WS[Formula: see text] nanorods were synthesized by a simple method of pulsed laser ablation in liquid (PLAL) environment. The prepared WS2 are analyzed by field emission scanning electron microscopy (FESEM), transmission electron microscopy (TEM), UV-visible spectroscopy (UV-vis) and Raman spectroscopy to confirm the surface morphology, phase and structure. A possible growth mechanism of WS2 is proposed. This study indicates new door for the preparation of 2D materials with specific morphology.

Synthesis and Characterization of Calcium Tartrate Dihydrate Nanoparticles

2015 ◽  
Vol 14 (04) ◽  
pp. 1550013 ◽  
Author(s):  
Urvisha Tarpara ◽  
Poorvesh Vyas ◽  
Mihir J. Joshi
Keyword(s):  
Average Crystallite Size ◽  
Powder Xrd ◽  
Xrd Pattern ◽  
Crystalline Materials ◽  
Transmission Electron ◽  
Calcium Tartrate ◽  
Particle Size And Morphology ◽  
Wet Chemical ◽  
Size And Morphology

Calcium tartrate finds various applications. In the present study, calcium tartrate nanoparticles were synthesized by wet chemical method using surfactant mediated approach. The powder XRD pattern revealed the typical broadening of peaks indicating the nanostructured nature. The average crystallite size was calculated by applying the Scherrer's formula to powder XRD pattern and was found in the range of 22.8–23.9 nm. The particle size and morphology of the synthesized nanoparticles was confirmed by using transmission electron microscopy (TEM). FTIR spectroscopy was used to confirm the presence of various functional groups. From TGA, it was found that calcium tartrate nanoparticles remained stable up to 120°C and were having two water molecules associated with them. The results are compared with the bulk crystalline materials available in the literature.

scholarly journals Synthesis, structural and magnetic characterization of lead-metaniobate/cobalt-ferrite nanocomposite films deposited by pulsed laser ablation

2014 ◽  
Vol 118 (1) ◽  
pp. 275-281 ◽  
Author(s):  
Pedro Sá ◽  
José Barbosa ◽  
Isabel T. Gomes ◽  
Jorge A. Mendes ◽  
João Ventura ◽  
...  
Keyword(s):  
Laser Ablation ◽  
Cobalt Ferrite ◽  
Pulsed Laser ◽  
Pulsed Laser Ablation ◽  
Nanocomposite Films ◽  
Magnetic Characterization ◽  
Lead Metaniobate

Growth and characterization of epitaxial Ba2Bi4Ti5O18 films deposited by pulsed laser ablation

2000 ◽  
Vol 114 (5) ◽  
pp. 249-253 ◽  
Author(s):  
A.R James ◽  
A Pignolet ◽  
S Senz ◽  
N.D Zakharov ◽  
D Hesse
Keyword(s):  
Laser Ablation ◽  
Pulsed Laser ◽  
Pulsed Laser Ablation

Characterization of Hastelloy thin films deposited by pulsed laser ablation

2002 ◽  
Vol 197-198 ◽  
pp. 343-347 ◽  
Author(s):  
M.F Vignolo ◽  
I Avram ◽  
S Duhalde ◽  
C Morales ◽  
T Pérez ◽  
...  
Keyword(s):  
Thin Films ◽  
Laser Ablation ◽  
Pulsed Laser ◽  
Pulsed Laser Ablation

Preparation of ZnO Nanoparticles by 1064/532nm Laser Ablation and Studying the Effect of the Ablation Wavelength

2021 ◽  
Vol 1021 ◽  
pp. 171-180
Author(s):  
Munaf S. Majeed ◽  
Rabea Q. Nafil ◽  
Marwa F. Abdul Jabbar ◽  
Kadhim H. Suffer
Keyword(s):  
Zinc Oxide ◽  
Laser Ablation ◽  
Pure Water ◽  
Pulsed Laser ◽  
Pulsed Laser Ablation ◽  
Ultra Pure Water ◽  
Hexagonal Shape ◽  
532 Nm ◽  
Laser Ablation Technique

We prepared Zinc oxide nanomaterial employing PLA (pulsed laser ablation) technique. A pure Zn target was immersed in ultra-pure water (UPW) and it was subjected to several pulses (1st. and 2nd. harmonic) of the pumping Nd: YAG laser. The influence of changing laser’s wavelength (1064, 532) nm on the characterization of the produced nanoparticles was studied. The results obtained from studying the structure, topography, and morphology of the product showed that the particles have a hexagonal shape. Also, changing the wavelength of the laser from 532nm to 1064nm leads to size reduction and density increasing of the nanoparticles.

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