Synthesis, Characterization, and Electrochemical Properties of Mn3O4/Cr2O3 Composite

2012 ◽  
Vol 463-464 ◽  
pp. 555-559
Author(s):  
Fen Ran ◽  
Ling Ren Wang ◽  
Lei Zhao ◽  
Yong Tao Tan ◽  
Ling Bin Kong ◽  
...  
Keyword(s):  
Cyclic Voltammetry ◽  
Composite Materials ◽  
Electrochemical Properties ◽  
Specific Capacitance ◽  
Surface Area ◽  
Coprecipitation Method ◽  
Chemical Coprecipitation ◽  
Charge Discharge ◽  
Chemical Coprecipitation Method

Mn3O4/Cr2O3composite materials were prepared by a chemical coprecipitation method. The structures were characterized by using SEM and XRD, and the supercapacitive behaviors of these composite materials were investigated with cyclic voltammetry (CV) and charge–discharge tests. Morphology of Mn3O4/Cr2O3composite materials showed that the Mn3O4/Cr2O3composite materials containning a small amount of Cr2O3has a better dispersion compared with that containning a lage amount of it. Owing to the higher surface area and poor crystallization, the Mn3O4/Cr2O3composite materials containning a small amount of Cr2O3show much higher specific capacitance (The highest specific capacitance value of 494 F/g was obtained), and were more promising for applications in supercapacitors.

Synthesis of BCN Nanoparticles Sandwiched between Carbon Nanosheets and Performance in Electrochemical Capacitors

2015 ◽  
Vol 719-720 ◽  
pp. 137-140
Author(s):  
Ren Li Yang ◽  
Jun Shuang Zhou ◽  
Li Hou ◽  
Yu Feng Zhao ◽  
Fa Ming Gao
Keyword(s):  
Cyclic Voltammetry ◽  
Electrochemical Properties ◽  
Specific Capacitance ◽  
Current Density ◽  
Nitrogen Atmosphere ◽  
Galvanostatic Charge ◽  
Carbon Nanosheets ◽  
And Performance ◽  
Discharge Measurements ◽  
Charge Discharge

BCN nanoparticles sandwiched between carbon nanosheets were synthesized with the P123 and borate ammonium under nitrogen atmosphere. The samples were characterized by SEM, TEM, and EELS. The SEM and TEM images show BCN nanoparticles are attached on the carbon nanosheets. Cyclic voltammetry (CV) and galvanostatic charge-discharge measurements are used to evaluate electrochemical properties of the composites. The samples show the specific capacitance of 102 F/g at current density of 200mA/g and good durability.

Preparation and Microstructure of (La0.5Sm0.5)2(Zr0.7Ce0.3)2O7 Ceramics Prepared by Chemical Coprecipitation Method

2016 ◽  
Vol 697 ◽  
pp. 89-92 ◽  
Author(s):  
Xian Kai Sun ◽  
Guang Hai Wang ◽  
Shi Chao Zhang ◽  
Hao Ran Sun ◽  
Kai Fang ◽  
...  
Keyword(s):  
Specific Surface ◽  
Surface Area ◽  
Specific Surface Area ◽  
Ph Value ◽  
Raw Materials ◽  
Ceramic Materials ◽  
Coprecipitation Method ◽  
Chemical Coprecipitation ◽  
The Impact ◽  
Chemical Coprecipitation Method

Ceramic materials of (La0.5Sm0.5)2(Zr0.7Ce0.3)2O7 composition powder was synthesized by chemical coprecipitation method using Sm2O3, La2O3, Ce (NO3)3·6H2O and ZrOCl2·8H2O powders as raw materials. Microstructure and phases of (La0.5Sm0.5)2(Zr0.7Ce0.3)2O7 (LSZCO) powder was examined by Transmission Electron Microscope (TEM) and X-ray diffraction (XRD). The specific surface area of powders were determined by BET specific surface area test. The structure of LSZCO powder remained in pyrochlore with the increase of temperature more than 1200 °C. According to the impact on the specific surface area of LSZCO powder, the factors of the process is ordered in descending sequence as follows: pH value, dispersant content, concentration of reactants, the reaction temperature.

Preparation and Electrochemical Properties of VO2(B) Nano-Belts

2011 ◽  
Vol 694 ◽  
pp. 91-97
Author(s):  
Yu Long Qiao ◽  
Yong Jun Ma ◽  
Qing Ping Luo ◽  
Chong Hua Pei
Keyword(s):  
Cyclic Voltammetry ◽  
Energy Loss ◽  
Electrochemical Properties ◽  
Specific Capacitance ◽  
Hydrothermal Method ◽  
Monoclinic Phase ◽  
Galvanostatic Charge ◽  
Crystal Direction ◽  
Electron Energy Loss ◽  
Charge Discharge

The VO2(B) nanobelts with monoclinic phase were synthesized by a hydrothermal method at 220°C for 48 h in the absence of any surfactants. The electron energy loss spectrum (EELS) demonstrates that vanadium exists only in the 4+ oxidation state. The SEM and TEM images reveal a belt-like structure of the VO2(B) with the length of several micrometers, the width of 140 nm and the thickness of around 20nm and growth along the [110] crystal direction. Cyclic voltammetry (CV) and galvanostatic charge/discharge demonstrate that VO2(B) nano-belts electrode exhibits desirable electrochemical properties and the specific capacitance reaches up to 632.6F•g-1.

Preparation and Electrochemical Properties of LaMnO3 Powder as a Supercapacitor Electrode Material

2017 ◽  
Vol 727 ◽  
pp. 698-704 ◽  
Author(s):  
Xian Wei Wang ◽  
Xiao Er Wang ◽  
Hui Chao Zhang ◽  
Qian Qian Zhu ◽  
Dong Li Zheng ◽  
...  
Keyword(s):  
Cyclic Voltammetry ◽  
Electrochemical Properties ◽  
Electrode Material ◽  
Raw Materials ◽  
Sol Gel ◽  
Galvanostatic Charge ◽  
Supercapacitor Electrode ◽  
Lanthanum Manganate ◽  
Pure Phase ◽  
Charge Discharge

The structural and electrochemical properties of lanthanum manganate (LaMnO3) powder prepared by the sol-gel method are researched in this article. The powder calcined at 600 °C showed amorphous, and the powder calcined at 700-800 °C showed the pure phase of the LaMnO3. The grains with the size of about 80-120 nm were agglomerating together. Cyclic voltammetry and galvanostatic charge-discharge were used to characterize the electrochemical properties in alkaline environment. The electrochemical properties calcined at 700 °C showed a specific capacitance of 73 F/g at the current density of 0.5 A/g. The raw materials for preparing the LaMnO3 powder are cheap, and the operation method is simple.

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