The Research on Preparation of Modified Bentonite and Adsorption of Crystal Violet in Dyeing Wastewater

2012 ◽  
Vol 610-613 ◽  
pp. 1731-1734
Author(s):  
Yu Chen ◽  
Shun Sheng Yang ◽  
Zheng Jun Gong ◽  
Dong Mei Wang
Keyword(s):  
Crystal Violet ◽  
Ph Value ◽  
Mixing Time ◽  
Dyeing Wastewater ◽  
Preparation Temperature ◽  
Modified Bentonite ◽  
Preparation Conditions ◽  
Dodecyltrimethylammonium Chloride ◽  
Decoloration Rate

Dodecyltrimethylammonium chloride was used to modify na-bentonite in Sichuan Yanting. It was studied that the optimal modification conditions of bentonite and its optimum decoloration conditions of crystal violet in dyeing wastewater. The optimum preparation conditions were that the concentration of dodecyltrimethylammonium chloride was 1000mg /L, the preparation temperature was 70°C and the mixing time was 20 minutes. The optimum adsorption conditions for crystal violet were that the pH value was 8, the mixing time was 20 minutes and the dosing quantity of modified bentonite was 15 g/L. The decoloration rate was 85.4% under aforesaid conditions.

Preparation and Adsorption Properties of PDMDAAC Modified Bentonite

2011 ◽  
Vol 399-401 ◽  
pp. 1226-1229
Author(s):  
Hong Shao ◽  
Ning Cao ◽  
Da Wei Wang
Keyword(s):  
Adsorption Properties ◽  
Dyeing Wastewater ◽  
X Ray Diffraction ◽  
Modified Bentonite ◽  
Preparation Conditions ◽  
Treatment Agent ◽  
Optimized Conditions ◽  
Decoloration Rate ◽  
Interplanar Space

A novel environmentally friendly water treatment agent was prepared by the natural bentonite and PDMDAAC. The treatment effect of direct black G dyeing wastewater on different preparation conditions was studied. The decoloration rate reached 98.57% under the optimized conditions (cross-linker concentration of 40g/L, M-V of 12 g/L, contact time of 75min, particle size of 0.124mm). The performance characterization of the modified bentonite was observed by means of X-ray diffraction, scanning electron microscopy. The PDMDAAC has entered into the bentonite interplanar space. The adsorption properties of bentonite were improved, which was suitable for the treatment of dyeing wastewater.

Adsorption Properties of Dyeing Wastewater on 8-Hydroxyquinoline Modified Bentonite

2011 ◽  
Vol 71-78 ◽  
pp. 1118-1122
Author(s):  
Hong Shao ◽  
Ning Cao ◽  
Hong Kang Xiao
Keyword(s):  
Blue Dye ◽  
Dyeing Wastewater ◽  
X Ray Diffraction ◽  
Reaction Conditions ◽  
Modified Bentonite ◽  
X Ray ◽  
Direct Light ◽  
Effects Of Ph ◽  
Optimum Reaction ◽  
Decoloration Rate

A novel adsorption material was synthesized and characterized by the methods of X-ray diffraction and scanning electron microscopy. The optimum reaction conditions of the 8-hydroxyquinoline modified bentonites were studied. And the modified bentonite was applied into the treatment of dyeing wastewater. The decoloration rate was invested as index. The effects of pH, adsorbent dosage, stirring speed, sedimentation time on adsorption have also been studied. The result showed that the decoloration rate of direct light turquoise blue dye on modified bentonites reached 94.12%, and the decoloration rate of acid orange dyeing wastewater reached 74.46%. So this type of modified bentonite was suitable for the treatment of dyeing wastewater.

Superior Adsorption Properties of Dyeing Wastewater on PDMDAAC Modified Bentonite

2011 ◽  
Vol 356-360 ◽  
pp. 386-390
Author(s):  
Hong Shao ◽  
Ning Cao
Keyword(s):  
Industrial Wastewater ◽  
Treatment Process ◽  
Orthogonal Experiment ◽  
Adsorption Properties ◽  
Dyeing Wastewater ◽  
Reaction Conditions ◽  
Complex Composition ◽  
Modified Bentonite ◽  
Optimized Conditions ◽  
Decoloration Rate

With the development of printing and dyeing industry, the nation has become the world's largest dye production and use country. With the complex composition and high color, the dyeing wastewater was currently recognized as one of the more difficult industrial wastewater to deal with. The bentonites was modified by PDMDAAC and applied into the treatment of dyeing wastewater. The treatment process was optimized with the index of decoloration rate. The decoloration rate reached 99.76% under the optimized conditions of adsorbent dosage=2g/L, pH=11, adsorption time=80min, stirring speed=350r/min, solution concentrate=500mg/L. The orthogonal experiment was designed to investigate the interaction between various reaction conditions. The superiority of PDMDAAC modified bentonite was confirmed by the comparing experiment.

scholarly journals Aluminum oxide carrier for a catalyst for low-temperature isomerization of hydrocarbons

2020 ◽  
Vol 15 (3) ◽  
pp. 58-69
Author(s):  
N. Tagandurdyyeva ◽  
N. V. Maltseva ◽  
T. A. Vishnevskaya ◽  
V. N. Narayev ◽  
A. Yu. Postnov
Keyword(s):  
Low Temperature ◽  
Polyvinyl Alcohol ◽  
Aluminum Oxide ◽  
High Selectivity ◽  
Ph Value ◽  
Strength Properties ◽  
Isomerization Reaction ◽  
Preparation Conditions ◽  
Constant Ph ◽  
Extrusion Method

Objectives. Determine the necessary conditions for obtaining a granulated η-Al2O3 carrier, investigate its structural and strength properties, and evaluate its activity for the model n-butane isomerization reaction.Methods. Samples containing bayerite structure aluminum trihydroxide were synthesized by precipitation from aqueous solutions of aluminum nitrate with ammonia under isothermal conditions at a constant pH value. The samples of the granulated carrier were obtained using an extrusion method when the composition of molding pastes was varied by tuning the ratio of bayerite- and η-Al2O3 -containing components and introducing polyvinyl alcohol.Results. The influence of the preparation conditions on the structural and strength properties of the active Al2O3 granules is evaluated. Samples of the aluminum oxide carrier were tested for a model reaction of low-temperature isomerization of n-butane, demonstrating a sufficiently high selectivity and reasonable prospects for use as catalysts for low-temperature isomerization of hydrocarbons.Conclusions. Increasing the content of the polyvinyl alcohol in the molding paste from 0.4 to 1.8 wt % is accompanied by an increase in the predominant sizes of the mesopores in the range of 10–50 nm and pores in the range of 50–80 nm, explaining the high values of all recorded parameters for the process of isomerization of n-butane.

SYNTHESIS AND OPTICAL PROPERTIES OF WATER SOLUBLE ZnSe NANOCRYSTALS

2001 ◽  
Vol 15 (28n30) ◽  
pp. 3881-3884 ◽  
Author(s):  
N. Murase ◽  
M. Y. Gao ◽  
N. Gaponik ◽  
T. Yazawa ◽  
J. Feldmann
Keyword(s):  
Ph Value ◽  
Water Soluble ◽  
Final Solution ◽  
Blue Fluorescence ◽  
Wet Chemistry ◽  
Preparation Conditions ◽  
Transmission Electron ◽  
Mean Size ◽  
Surface Capping ◽  
Znse Nanocrystals

ZnSe nanocrystals are prepared in water by a wet chemistry method. By selecting an appropriate pH value and surface-capping agents, a whitish blue fluorescence peaking at 470 nm is observed under ZV irradiation. The intensity of this fluorescence increases dramatically under reflux and saturates after ~ 40 hrs. The final mean size of the ZnSe nanocrystals measured by transmission electron microscopy is aboyt 2 nm in diameter. The quantum efficiency of the fluorescence form the final solution is estimated to be ~1%, although the preparation conditions have not yet been completely optimized. These properties are discussed in comparison with those of similarly prepared CdTe and differently prepared ZnSe nanocrystals.

Hydrothermal Synthesis of GdVO4:Eu 3+ Phosphors by Optimizing its Preparation Conditions

2011 ◽  
Vol 287-290 ◽  
pp. 1360-1364
Author(s):  
Ying Lin Yan ◽  
Yun Hua Xu ◽  
Juan Wang ◽  
Zhen Xing Luan
Keyword(s):  
Ph Value ◽  
Photo Luminescence ◽  
Luminescence Spectroscopy ◽  
Temperature Reaction ◽  
Hydrothermal Temperature ◽  
Red Emission ◽  
X Ray ◽  
Preparation Conditions ◽  
Optimal Reaction Condition ◽  
Optimal Reaction

Eu3+ -doped GdVO4 powders have been synthesized via a novel hydrothermal method using commercially available Gd2O3, NH4VO3 and Eu2O3 as the reacting precursors. The influences of several important parameters, such as hydrothermal temperature, reaction time and pH value, of the experiment were investigated. The obtained samples were characterized by X-ray powder diffraction (XRD), field emission scanning electron microscopy (FESEM), and photo-luminescence spectroscopy (PL). The experimental results showed that the optimal reaction condition was processed at 180°C for 12 h and adjusted pH value to 4. The morphology of products was uniform pseudo-octahedron with a little conglomeration. All the phosphors exhibit the characteristic dominant red emission of Eu3+ ion (5D0 → 7F2) at 618nm.

scholarly journals The nanostructure of barium dititanate prepared by hydrothermal method

2019 ◽  
Vol 09 (02) ◽  
pp. 1950011
Author(s):  
Sarah L. Rasheed ◽  
Emad K. Al-Shakarchi
Keyword(s):  
Electron Microscopy ◽  
Reaction Time ◽  
Hydrothermal Method ◽  
Ph Value ◽  
Hydrothermal Process ◽  
Dielectric Ceramic ◽  
Lattice Constants ◽  
Preparation Conditions ◽  
Transmission Electron ◽  
Lcr Meter

The dielectric ceramic of barium dititanate compound BaTi2O5 had been prepared through the hydrothermal process by applying different parameters, such as pH-value, reaction time, temperature and pressure. The prepared powders were examined by X-ray diffraction (XRD). The predominant phase was a monoclinic phase with lattice constants ([Formula: see text], [Formula: see text], [Formula: see text] Å), ([Formula: see text], [Formula: see text]), and the unit cell volume (527 Å3). The surface morphology was demonstrated by Scanning Electron Microscopy (SEM). It exhibited the grains in spherical and elliptical shapes with high homogeneity. The shapes of nanostructure were analyzed by Transmission Electron Microscopy (TEM). The appearance of nanostructures like the nanoparticles and nano rods were found. The size of nanoparticles was in the range of 9–31[Formula: see text]nm, and size of nanorods was 32–37[Formula: see text]nm. The dielectric measurements were done by using LCR meter at different temperature and frequencies (10, 50 and 100[Formula: see text]kHz). It was clear that the Curie temperature had a high value up to (485∘C). The relative permittivity was partially changed for two prepared samples regarding high pressure and long reaction time, which were the main preparation conditions of hydrothermal method.

Study on Dyeing of Lyocell Knitted Fabric with Grape Seed Extract Dyes

2012 ◽  
Vol 550-553 ◽  
pp. 1633-1636 ◽  
Author(s):  
De Ling Chi ◽  
Hu Sheng Yu ◽  
Shan Shan Zhao
Keyword(s):  
Ph Value ◽  
Grape Seed Extract ◽  
Grape Seed ◽  
Seed Extract ◽  
Knitted Fabric ◽  
Light Fastness ◽  
Preparation Temperature ◽  
Dyeing Method ◽  
Dyed Fabric ◽  
Better Than

The natural vegetable dye grape seed extract (GSE) was applied on the direct dyeing of lyocell knitted fabric. By changing the dyeing condition, the modified process was derived after evaluating various fastnesses of the dyed fabric. The direct dyeing method should be under the condition of GSE’s concentration 5g/L, bath preparation temperature 80°C, pH value 3, bath ratio 1:30, dyeing time 60min. The color is very sensitive to pH and GSE’s concentration. The rubbing fastness, washing fastness and light fastness is good, the acid perspiration fastness is better than the alkaline perspiration fastness.

Foam Glass for Soilless Cultivation Matrix Prepared by Using Boron Mud

2013 ◽  
Vol 455 ◽  
pp. 106-111
Author(s):  
Yan Yan Jiang ◽  
Ya Nan Li ◽  
Ji Wen Zhang ◽  
Qiao Yu ◽  
Zhi Qiang Hu ◽  
...  
Keyword(s):  
Immersion Time ◽  
Absorption Rate ◽  
Ph Value ◽  
Foam Glass ◽  
Foaming Agents ◽  
Preparation Conditions ◽  
Soilless Cultivation ◽  
Foaming Temperature ◽  
Boron Mud ◽  
Foaming Time

Foam glass was prepared by boron mud, broken glass, foaming agents and fluxes. The appropriate foaming temperature and foaming time were got by sintering parameter optimization. The effects of preparation conditions on propertis of the foam glass for soilless cultivation matrix were investigated. The results show that under the optimum preparation conditions (the foaming temperature is 800 °C and foaming time is 40 min), the formula for boron mud/broken glass: Borax: Sodium nitrate: Calcium carbonate is 35/50: 5:7:3, the bulk density is 247 kg/m3, the open porosity is 70%, the water absorption rate is 202.3%, the pH value of soak solution keeps at about 6.5 with the increase of immersion time. All of these will meet the application requirement of soilless cultivation.

Sign in / Sign up

Export Citation Format

Share Document