Synthesis and Characterization of a New Amino-Functionalized PMO Material
2013 ◽
Vol 712-715
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pp. 271-279
Keyword(s):
X Ray
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A new organic silicane which is bridged by a long amino-functionalized alkyl chain was prepared and used as the precursor in the synthesis of a series of PMO materials. The organic silicane was added into the reaction system in CH2Cl2and the PMO materials were prepared by a simple stirring method under acidic condition, with a nonionic surfactantBrij 76 as template. To find the proper synthesis condition, the time of stirring and the proportion of organic silicane and TEOS were varied. Liquid and solid state NMR, X-ray diffraction (XRD) patterns, thermogravimetric analysis (TGA), transmission electron microscopy (TEM) and N2-physisorption properties were used to characterize the structures.
2012 ◽
Vol 174-177
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pp. 508-511
2000 ◽
Vol 55
(9)
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pp. 882-886
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2013 ◽
Vol 32
(2)
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pp. 157-162
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1990 ◽
Vol 73
(8)
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pp. 2281-2286
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2014 ◽
Vol 602-603
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pp. 19-22
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2010 ◽
Vol 160-162
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pp. 1301-1308
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2012 ◽
Vol 624
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pp. 59-62
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