Logging Evaluation Method and its Application for Measuring the Total Organic Carbon Content in Shale

2014 ◽  
Vol 962-965 ◽  
pp. 51-54
Author(s):  
Zhi Feng Wang ◽  
Yuan Fu Zhang ◽  
Hai Bo Zhang ◽  
Qing Zhai Meng

The acquisition of the total organic carbon (TOC) content mainly relies on the geochemical analysis and logging data. Due to geochemical analysis is restricted by coring and experimental analysis, so it is difficult to get the continuous TOC data. Logging evaluation method for measuring TOC is very important for shale gas exploration. This paper presents a logging evaluation method that the shale is segmented according to sedimentary structures. Sedimentary structures were recognized by core, thin section and scanning electron microscope. Taking Wufeng-Longmaxi Formation, Silurian, Muai Syncline Belt, south of Sichuan Basin as research object, the shale is divided into three kinds: massive mudstone, unobvious laminated mudstone, and laminated mudstone. TOC within each mudstone are calculated using GR, resistivity and AC logging data, and an ideal result is achieved. This method is more efficient, faster and the vertical resolution is higher than △logR method.

2017 ◽  
Vol 36 (5) ◽  
pp. 1295-1309 ◽  
Author(s):  
Wei Guo ◽  
Weijun Shen ◽  
Shangwen Zhou ◽  
Huaqing Xue ◽  
Dexun Liu ◽  
...  

Shales in the Well district of Yu 106 of the Shanxi Formation in the Eastern Ordos Basin is deposited in the swamp between delta plains, distributary river channels, natural levee, the far end of crevasse splay, and depression environments. According to organic geochemistry, reservoir physical property, gas bearing capacity, lithology experimental analysis, combined with the data of drilling, logging, testing and sedimentary facies, the reservoir conditions of shale gas and the distribution of an advantageous area in Shanxi Formation have been conducted. The results show that the total organic carbon content of the Shanxi Formation is relatively high, with an average content value of 5.28% in the segment 2 and 3.02% in segment 1, and the organic matter is mainly kerogen type II2 and III. The maturity of organic matter is high with 1.89% as the average value of Ro which indicates the superior condition for gas generation of this reservoir. The porosity of shales is 1.7% on average, and the average permeability is 0.0415 × 10−3 µm2. The cumulative thickness is relatively large, with an average of 75 m. Brittle mineral and clay content in shales are 49.9% and 50.1%, respectively, but the burial depth of shale is less than 3000 m. The testing gas content is relatively high (0.64 × 104 m3/d), which shows a great potential in commercial development. The total organic carbon of the segment 2 is higher than that of the segment 1, and it is also better than segment 1 in terms of gas content. Based on the thickness of shale and the distribution of sedimentary facies, it is predicted that the advantageous area of shale gas in the segment 2 is distributed in a striped zone along the northeast and the northsouth direction, which is controlled by the swamp microfacies between distributary river channels.


2021 ◽  
pp. 1-64
Author(s):  
Guangzhao Zhou ◽  
Zhiming Hu ◽  
Xiangui Liu ◽  
Xianggang Duan ◽  
Jin Chang

Recent observations of shale gas breakthroughs have in the Weiyuan marine shale gas play in the Sichuan Basin have attracted great interest. To better understand these breakthroughs, we use core description, FIB-SEM data, XRD data, organic geochemistry, and well logging data, to better understand the reservoir characteristics carbonaceous shale, calcareous shale, and siliceous shale lithology, with a focus on the organic-rich shale units. We find conventional well log methods are effective in mapping the spatial distribution of the organic-rich shale in the Weiyuan area where the. total organic carbon content in the Longmaxi Formation ranges from 1.35%-6.95%, averaging 4.42%. The kerogen is Type I-II and the vitrinite reflectance (Ro) is greater than 2.57%, which indicates that the formation is susceptible to shale gas accumulation. The clay mineral content ranges from 48 wt.% to 63 wt.% (avg. 51 wt.%).with illite and chlorite averaging 73.8% and 25.7%, respectively. The brittle mineral quartz and plagioclase content ranges from 32 wt.% to 61 wt.% (avg. 47 wt.%). Compared to the surrounding litholgic units, the marine shale exhibits relatively high GR, CNL, AC, RT, K, and U values and relatively low DEN, PE and Th/U values, allowing us to construct. Cross-plots to define the units of interest. Using the same process, we quantify the TOC content providing a spatial distribution of organic-rich shale using conventional well logging.


2019 ◽  
Vol 7 (2) ◽  
pp. T283-T292 ◽  
Author(s):  
Huang Yanran ◽  
Xiao Zhenhui ◽  
Dong Li ◽  
Yu Ye ◽  
Cao Taotao

The lower Cambrian Niutitang Formation in northwestern Hunan, South China, has already reached its high or over matured stage and is formed with hydrothermal activity and deposition. Thus, it is extremely difficult to predict the total organic carbon (TOC) content accurately by common methods with well-logging data. To solve this problem, we use artificial neural networks for predicting the TOC of the black shales in our study case. We got the input vectors through principal component analysis and based on the relationships and the logging response mechanism between TOC and logging data. In the back-propagation algorithm, some important parameters including the sample databases, the number of hidden layer nodes, transfer function, and weight value adjustment were all optimized correctly in the networks. Then, we built the mathematical model through a large number of learning sample datum and the error function between the actual and expected outputs, and we found that the results are good according to many performance indicators. In testing samples, mean absolute and relative errors are all reduced probably due to the datum ranges and features being focused, but the accuracy also drops when the numbers of participating samples are reduced. Through redefining the [Formula: see text] sample database, we gained more accurate values for the high-TOC source rock. Finally, we think that the results suggest that the method is suitable for shale gas resource exploration under similar geologic conditions and data characteristics.


2017 ◽  
Vol 113 (9/10) ◽  
Author(s):  
Michiel de Kock ◽  
Nicolas Beukes ◽  
Elijah Adeniyi ◽  
Doug Cole ◽  
Annette Götz ◽  
...  

The Main Karoo basin has been identified as a potential source of shale gas (i.e. natural gas that can be extracted via the process of hydraulic stimulation or ‘fracking’). Current resource estimates of 0.4–11x109 m3 (13–390 Tcf) are speculatively based on carbonaceous shale thickness, area, depth, thermal maturity and, most of all, the total organic carbon content of specifically the Ecca Group’s Whitehill Formation with a thickness of more than 30 m. These estimates were made without any measurements on the actual available gas content of the shale. Such measurements were recently conducted on samples from two boreholes and are reported here. These measurements indicate that there is little to no desorbed and residual gas, despite high total organic carbon values. In addition, vitrinite reflectance and illite crystallinity of unweathered shale material reveal the Ecca Group to be metamorphosed and overmature. Organic carbon in the shale is largely unbound to hydrogen, and little hydrocarbon generation potential remains. These findings led to the conclusion that the lowest of the existing resource estimates, namely 0.4x109 m3 (13 Tcf), may be the most realistic. However, such low estimates still represent a large resource with developmental potential for the South African petroleum industry. To be economically viable, the resource would be required to be confined to a small, well-delineated ‘sweet spot’ area in the vast southern area of the basin. It is acknowledged that the drill cores we investigated fall outside of currently identified sweet spots and these areas should be targets for further scientific drilling projects.


2016 ◽  
Vol 4 (2) ◽  
pp. T123-T140 ◽  
Author(s):  
Julius Kwame Borkloe ◽  
Renfang Pan ◽  
Jineng Jin ◽  
Emmanuel Kwesi Nyantakyi ◽  
Jianghui Meng

The Cambrian Jiulaodong Formation of the Wei-201 well block in the Sichuan Basin was investigated for shale gas potential. In the subsurface, the thermally mature formation attained a stable thickness of 234 m encompassing an area of approximately [Formula: see text] and representing a potential gas resource. The total gas content measurements from canistered samples was more than the estimated total gas storage capacity of the free gas, absorbed gas, and gas dissolved in water and in oil. The canister gas content ranged between 0.971 and [Formula: see text] and averaged [Formula: see text]. The average estimated gas in place was 2.5 billion cubic meters for the formation in the Weiyuan area. Reflectance measurements for thermal maturity range between 2.60% and 3.06% and average 2.84%. The results of our total organic carbon content (TOC) content analysis conducted on the core shale samples indicate that the TOC content of the formation ranges from 0.87% to 3.57% and averages 2.2%. The mineral composition of marine mudstone formation of the Jiulaodong shale is relatively consistent. Brittle mineral content increases with organic carbon content and is approximately 32%–43%, of which quartz content is 29%–40% with a very low amount of clay mineral as the mixed layer. The amount of illite-smectite ranges from 0% to 1% and the brittleness index range from 37% to 62% and average 57.1%. The Cambrian Jiulaodong Formation ha very good petroleum-source rock potential due to its average TOC content of greater than 2%, average canister gas content of [Formula: see text], good type I kerogen, high maturity with average 2.84% of source rocks that are characterized by a fairly high abundance of organic matter increasing from top to bottom and a large thickness of 234 m. Natural fractures, cracks, and pores developed in the Jiulaodong Formation also provide space for shale gas storage, and its average brittleness index is greater than 57%, which is good for fracability.


Geofluids ◽  
2020 ◽  
Vol 2020 ◽  
pp. 1-11
Author(s):  
Chao Luo ◽  
Nanxin Yin ◽  
Hun Lin ◽  
Xuanbo Gao ◽  
Junlei Wang ◽  
...  

The lower Silurian Longmaxi Formation hosts a highly productive shale gas play in the Zhaotong region of southern China. According to core observation, X-ray diffraction analyses, and scanning electron microscopy (SEM) observations, the shale comprises primarily quartz, carbonate minerals, and clay minerals, with minor amounts of plagioclase, K-feldspar, and pyrite. The clay mineral content ranges from 15.0% to 46.1%, with an average of 29.3% in the Zhaotong region. Organic geochemical analyses show that the Longmaxi Formation has good potential for shale gas resources by calculating total organic carbon, vitrinite reflectance, and gas content. Scanning electron microscope images demonstrate that reservoir pore types in the Longmaxi shale include organic pores, interparticle pores, intercrystalline pores, intraparticle pores, and fractures. Reservoir distribution is controlled by lithofacies, mineral composition, and geochemical factors. In addition, we investigated the relationships between reservoir parameters and production from 15 individual wells in the Zhaotong region by correlation coefficients. As a result, the brittleness index, total organic carbon (TOC), porosity, and gas content were used to define high-quality reservoirs in the Longmaxi shale. Based on these criteria, we mapped the thickness and distribution of high-quality reservoirs in the Longmaxi Formation and selected highlighted several key sites for future exploration and development.


2017 ◽  
Vol 5 (3) ◽  
pp. T387-T398 ◽  
Author(s):  
Jingling Xu ◽  
Yangyang Li ◽  
Baoying Zhang ◽  
Lei Xu ◽  
Yuxing Qin

Quantitative estimation of total-organic-carbon (TOC) content using well logs is very important for shale-gas reservoir evaluation, especially when core data are limited. Even though many techniques have been developed to calculate TOC from well logs, they all have their limitations and accurate assessment of TOC in organic-rich tight shales is still challenging. We have used an improved log-overlay method for evaluating TOC content in organic-rich tight shale reservoirs by overlying the properly scaled gamma-ray, sonic transit time, and bulk density curves on top of the compensated neutron log (CNL) curve based on the same concept to the original [Formula: see text] technique. These logging curves are overlapped with the CNL in nonsource intervals, and they are separated in organic-rich shale reservoirs. The separation magnitude increases along with the increase in TOC content of the shale, and this relationship is transformed to calculate TOC. This method was tested and verified by doing a case study using well-log data from the Jiaoshiba tight shale-gas play in the Sichuan Basin. The results illustrated that the new TOC evaluation method is more practical and effective compared with existing TOC evaluation methods.


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