Multiple Shear Bands in Zr-Based Bulk Metallic Glass Processed by Severe Plastic Deformation

2018 ◽  
Vol 385 ◽  
pp. 319-324 ◽  
Author(s):  
Evgeniy Boltynjuk ◽  
Evgeniy Ubyivovk ◽  
Dmitriy Gunderov ◽  
Vladimir Mikhalovskii ◽  
Ruslan Z. Valiev

The Zr62Cu22Al10Fe5Dy1 bulk metallic glass was subjected to high pressure torsion (HPT) processing at temperatures of 20 and 150°C. Structural studies were carried out by TEM on the lamella-sample prepared from the HPT-specimens in transversal direction to the specimen plane. TEM studies revealed formation of multiple shear bands with spacings in a 20-50 nm range for both HPT states. Shear bands could be divided in two types: primary and secondary bands. The morphology of shear bands strongly depends on the processing temperature. Shear bands are distributed homogeneously throughout the whole lamella-sample for state processed by HPT at temperature of 20°C. Regions with shear bands are divided by amorphous regions on lamella-sample cut from the sample processed by HPT at temperature of 150°C. Analysis of optical microscopy and SEM data showed that shear bands are distributed throughout the whole volume of HPT-specimens.

Author(s):  
Vasily Astanin ◽  
Dmitry Gunderov ◽  
Zhi Qiang Ren ◽  
Ruslan Valiev ◽  
Jing Tao Wang

2019 ◽  
Vol 58 (1) ◽  
pp. 304-312
Author(s):  
Ádám Révész ◽  
András Horváth ◽  
Gábor Ribárik ◽  
Erhard Schafler ◽  
David J. Browne ◽  
...  

Abstract Bulk metallic glass of Cu60Zr20Ti20 composition has been synthesized by copper mold casting. Slices of the as-cast glass has been subjected to severe plastic deformation by high-pressure torsion for different whole turns. The microstructure and the thermal behavior of the deformed disks have been investigated by X-ray diffraction and differential scanning calorimetry. It was confirmed that the initial compression preceding the high pressure torsion induces crystallized structure, which shows only minor further changes upon the severe plastic shear deformation achieved by twisting the sample. The X-ray line profiles have been evaluated by the Convolutional Whole Profile Fitting algorithm in order to determine the evolution of the microstructural parameters, such as the median and variance of the crystallite size distribution, average crystallite size and dislocation density as a function of the number of revolutions. Hardness measurements by nanoindentation have also been carried out on the as-cast alloys and the deformed disks.


2007 ◽  
Vol 22 (2) ◽  
pp. 501-507 ◽  
Author(s):  
F.F. Wu ◽  
Z.F. Zhang ◽  
S.X. Mao

The quasi-static compressive deformation behavior of a Vitreloy 1 bulk metallic glass (BMG) with an aspect ratio of 0.25 was investigated. It is found that the friction and the confinement at the specimen–loading platen interface will cause the dramatic increase in the compressive load, leading to higher compressive strength. In particular, the BMG specimens show great plastic-deformation ability, and plenty of interacted, deflected, wavy, or branched shear bands were observed on the surfaces after plastic deformation. The formation of the strongly interacted, deflected, wavy, or branched shear bands can be attributed to the triaxial stress state in the glassy specimens with a very small aspect ratio.


2009 ◽  
Vol 618-619 ◽  
pp. 437-441
Author(s):  
Hao Wen Xie ◽  
Peter D. Hodgson ◽  
Cui E Wen

Vickers and nano indentations were performed on a structurally relaxed Zr41Ti14Cu12.5Ni10Be22.5 bulk metallic glass (BMG), and the evolution of the shear bands in the relaxed BMG was investigated and compared to that in the as-cast alloy. Results indicate that the plastic deformation in the BMG with structure relaxation is accommodated by the semicircular (primary) and radial (secondary) as well as tertiary shear bands. Quantitatively, the shear band density in the relaxed alloy was much lower than that in the as-cast alloy. The annihilation of free volume caused by the annealing was responsible for the embrittlement of the sample with structure relaxation.


2009 ◽  
Vol 24 (8) ◽  
pp. 2697-2704 ◽  
Author(s):  
Alban Dubach ◽  
K. Eswar Prasad ◽  
Rejin Raghavan ◽  
Jorg F. Löffler ◽  
Johann Michler ◽  
...  

Instrumented indentation experiments on a Zr-based bulk metallic glass (BMG) in as-cast, shot-peened and structurally relaxed conditions were conducted to examine the dependence of plastic deformation on its structural state. Results show significant differences in hardness, H, with structural relaxation increasing it and shot peening markedly reducing it, and slightly changed morphology of shear bands around the indents. This effect is in contrast to uniaxial compressive yield strength, σy, which remains invariant with the change in the structural state of the alloys investigated. The plastic constraint factor, C = H/σy, of the relaxed BMG increases compared with that of the as-cast glass, indicating enhanced pressure sensitivity upon annealing. In contrast, C of the shot-peened layer was found to be similar to that observed in crystalline metals, indicating that severe plastic deformation could eliminate pressure sensitivity. Microscopic origins for this result, in terms of shear transformation zones and free volume, are discussed.


2016 ◽  
Vol 22 (3) ◽  
pp. 383-390 ◽  
Author(s):  
Soo-Hyun Joo ◽  
Dong-Hai Pi ◽  
Jing Guo ◽  
Hidemi Kato ◽  
Sunghak Lee ◽  
...  

2012 ◽  
Vol 67 (4) ◽  
pp. 332-335 ◽  
Author(s):  
D.D. Qu ◽  
Y.B. Wang ◽  
X.Z. Liao ◽  
J. Shen

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