Effect of Temperature on Structural and Optical Properties of ZnO Nanorods by Hydrothermal Method

2013 ◽  
Vol 591 ◽  
pp. 293-296 ◽  
Author(s):  
Xiao Yan Fei ◽  
Jun Luo ◽  
Shu Wang Duo ◽  
Hao Zhang ◽  
Xiang Min Xu ◽  
...  

The ZnO nanorods were prepared at 130 °C, 160 °C and 190 °C for 6 h by hydrothermal method. The structural and optical properties of ZnO nanorods were invesitigated by powder X-ray diffraction (PXRD), scanning electron microscopy (SEM) and Fourier transform infrared spectroscopy (FTIR). XRD pattern analysis showed that the ZnO nanorods are the hexagonal structure (space group P63 mc). No other crystal phases, such as Zn and Zn (OH)2 were detected. FT-IR study identified the sharp peak that appeared at 573 cm-1 is related with the ZnO stretching mode. Also, SEM images revealed that the diameter of a single ZnO crystal ranges from 100 to 300 nm and the length ranges from 1 to 3 μm.

2016 ◽  
Vol 675-676 ◽  
pp. 53-56
Author(s):  
Supawadee Pokai ◽  
Puenisara Limnonthakul ◽  
Mati Horprathum ◽  
Sukon Kalasung ◽  
Pitak Eiamchai ◽  
...  

Zinc oxide (ZnO) nanorods (NRs) promise high potentials in several applications, such as photovoltaic device, thermoelectric device, sensor and solar cell. In this research, the vertical alignment of ZnO NRs was fabricated by hydrothermal method with various precursor concentrations and growth time on different seed layers (ZnO and Au), which deposited on silicon wafer substrate (100). The crystalline structure and morphology of ZnO NRs have been characterized by x-ray diffraction (XRD) and field emission scanning electron microscopy (FE-SEM) techniques, respectively. The x-ray diffraction pattern shows that the prepared samples have a strong preferred orientation (002) plane. FE-SEM images of the ZnO NRs, it found that the density and aspect ratio were strongly influenced by the seed layer and precursor concentration. In addition, the aspect ratio of ZnO NRs was increased with increasing growth time. This study provides a cost effective method for the fabrication of well aligned ZnO NRs for nano-electronic devices.


2016 ◽  
Author(s):  
Khyati Gautam ◽  
Inderpreet Singh ◽  
Varun Singh Nirwal ◽  
Joginder Singh ◽  
Koteswara Rao Peta ◽  
...  

2012 ◽  
Vol 460 ◽  
pp. 147-150
Author(s):  
Qiu Ming Fu ◽  
Jian Peng Wu ◽  
Zhi Bin Ma ◽  
Ya Fang Tu

ZnO nanostructures were prepared on Si and AlN substrates with and without etching by hydrothermal method. The influences of substrate etching on the morphology and structure were investigated by scanning electron microscopy, X-ray diffraction, Raman microscopy, and photoluminescence spectrum. The results show that the morphology and the photoluminescence properties of ZnO nanorods are significantly influenced by substrate etching.


2014 ◽  
Vol 211 (11) ◽  
pp. 2611-2615 ◽  
Author(s):  
Chan Oeurn Chey ◽  
Hatim Alnoor ◽  
Mazhar Ali Abbasi ◽  
Omer Nur ◽  
Magnus Willander

2018 ◽  
Vol 10 (1) ◽  
pp. 01004-1-01004-4 ◽  
Author(s):  
S. Wahyuningsih ◽  
◽  
F. N. Ainiy ◽  
A. H. Ramelan ◽  
◽  
...  

2019 ◽  
Vol 33 (20) ◽  
pp. 1950227
Author(s):  
Xue Jiang ◽  
Weihong Wu ◽  
Yuqian Li ◽  
Xiaoqing Guo ◽  
Nan Wang ◽  
...  

In this study, [Formula: see text]-doped yttrium oxide nanophosphors were prepared using the hydrothermal method assisting with the polyacrylic acid (PAA), phenol formaldehyde resin precursor (PF), and gum arabic (GA), respectively and their structural and optical properties were studied. X-ray diffraction (XRD) patterns of the samples can be well indexed to the cubic structure. Additionally, scanning electron microscopy (SEM) images showed that the samples were different morphologies, via combining with different templates. The luminescence results revealed that the addition of templates have a significant influence on the luminescence properties of [Formula: see text]-doped [Formula: see text].


2019 ◽  
Vol 397 ◽  
pp. 1-7
Author(s):  
Hassene Nezzari ◽  
Riad Saidi ◽  
Adel Taabouche ◽  
Meriem Messaoudi ◽  
Mohamed Salah Aida

In this work, ZnO thin films grown on heated glass substrates in a temperature range of 300 to 500 °C with a 50°C step. The prepared solution is composed of methanol and zinc acetate Zn(CH3COO)2.2H2O. ZnO thin films are deposited by pyrolysis spray technique, our work focuses on the study of the substrate temperature influence on the structural and optical properties of these layers. Therefore, The X-ray diffraction, showed a Wurtzit hexagonal structure of elaborated films, with (002) as a preferred orientation, and a grain size of 64 to 74 nm. The optical transmission spectroscopy UV-Visible, illustrated an increase of optical band gap from 3.19 to 3.25 eV, proportionally with the substrate temperature.


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