High Temperature Micro Structural Evolution of ZrO2 Fibers Thermal Insulation Materials

2014 ◽  
Vol 602-603 ◽  
pp. 319-322 ◽  
Author(s):  
Guang Hai Wang ◽  
Hao Ran Sun ◽  
Chun Peng Wang ◽  
Jian Zhou ◽  
Yan Li Huo ◽  
...  

Yttria-stabilized zirconia fibers thermal insulation materials may be the main developmental direction of high temperature thermal protection materials, due to their high temperature resistance (above 2000 °C), high strength and toughness, low thermal conductivity ( about 2 W/m·K), oxidation resistance and other excellent properties. However, mechanical property of zirconia fibers thermal insulation materials is decrease after high temperature heat treatment. In this paper, the evolution of microscopic structure of zirconia fibers is studied by using the method of oxyacethlene ablation. The gain growth and high temperature creep are observed after 600 s heat treatment at 1800 °C. Crystal phase of zirconia fibers is not changed and still cubic. Moreover, crystallinity is more higher form XRD patterns. Controlling grain growth can improve high temperature mechanical property of zirconia fibers thermal insulation materials.

2021 ◽  
pp. 79-86
Author(s):  
V.G. Babashov ◽  
◽  
N.M. Varrik ◽  

Based on the analysis of recent publications of scientific and technical literature, data on the production of zirconium oxide fibers used for the manufacture of high-temperature thermal insulation materials are presented. Information is provided on various methods of obtaining zirconium oxide fibers (methods of impregnation of the template and molding of the mixture, sol-gel method of spinning a fiber-forming precursor solution), as well as on the technique of fiber molding (manual pulling, dry and wet spinning, blowing and electrospinning). The use of such fibers for the production of thermal insulation materials (felts, cords and blocks) instead of currently existing materials made of aluminum oxide-based fibers can significantly increase the operating temperatures of the thermal protection systems.


2018 ◽  
Vol 281 ◽  
pp. 131-136
Author(s):  
Shi Chao Zhang ◽  
Wei Wu ◽  
Yu Feng Chen ◽  
Liu Shi Tao ◽  
Kai Fang ◽  
...  

With the increase of the speed of vehicle, the thermal protection system of its powerplant requires higher insulation materials. Phase change materials can absorb large amounts of heat in short time. So the introduction of phase change materials in thermal insulation materials can achieve efficient insulation in a limited space for a short time. In this paper, a new phase change thermal insulation material was prepared by pressure molding with microporous calcium silicate as matrix and Li2CO3 as phase change material. The morphology stability, exudation and heat insulation of the materials were tested. The results show that the porous structure of microporous calcium silicate has a good encapsulation when the phase transition of Li2CO3 is changed into liquid. And the material has no leakage during use. The thermal performance test also shows that the insulation performance of the material has obvious advantages in the short term application.


Author(s):  
K.I. Nedashkovskiy ◽  
A.V. Gulshin ◽  
Yu.M. Averina ◽  
V.A. Naumkina ◽  
V.V. Menshikov ◽  
...  

The paper presents investigation results and a technology for manufacturing fastener workpieces out of the 07Kh16N6-Sh (07Х16Н6-Ш) steel using high-temperature heat treatment. The steel undergoing our testing was additionally doped with molybdenum, as reflected in the 07Kh16N6M-Sh (07Х16Н6М-Ш) designation, which facilitated grain refinement. We implemented accelerated climate testing of bolts in order to assess the corrosion cracking resistance of 07Kh16N6-Sh (07Х16Н6-Ш), 07Kh16N6M-Sh (07Х16Н6М-Ш) and 13Kh15N4AM3-Sh (13Х15Н4АМ3-Ш) steel fasteners in maritime climates.


2021 ◽  
Vol 1016 ◽  
pp. 906-910
Author(s):  
Xin Hua Min ◽  
Cheng Jin

In this paper,effect of the different forging processes on the microstructure and mechanical properties of the flat flat billets of TA15 titanium alloy was investigated.The flat billiets of 80 mm×150 mm×L sizes of TA15 titanium alloy are produced by four different forging processes.Then the different microstrure and properties of the flat billiets were obtained by heat treatment of 800 °C~850 °C×1 h~4h.The results show that, adopting the first forging temperature at T1 °C、slow cooling and the second forging temperature at T2°C 、quick cooling, the primary αphases content is just 10%, and there are lots of thin aciculate phases on the base. This microstructure has both high strength at room temperature and high temperature, while the properties between the cross and lengthwise directions are just the same. So the hot processing of the first forging temperature at T1 °C、slow cooling and the second forging temperature at T2°C 、quick cooling is choosed as the ideal processing for production of aircraft frame parts.


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