Metal Oxide Nanoparticles Obtained by Microwave Synthesis and Application in Gas Sensing by Microwave Transduction

2014 ◽  
Vol 605 ◽  
pp. 299-302 ◽  
Author(s):  
Jerome Rossignol ◽  
Didier Stuerga

In literature, many papers describe the applications of semiconductor as sensitive material in sensor field. The gas sensor using tin oxide requires a strictly controlled high operating temperature in order to detect both reducing and oxidizing gases. The semiconductor nanoparticles, with their high specific surface area, increase the gas sensing performance. The originality of this work is to valorize the nanoparticle of metal oxide like SnO2, TiO2 obtained by microwave thermohydrolysis synthesis, using a gas sensing microwave transduction. The present synthesis is to prepare metal oxide nanocrystalline powder with a high surface area by microwave-induced thermohydrolysis. We propose to study the influence of the metal oxide nanoparticle, as a sensitive layer, in gas sensing measurement. The pollutant is added into an argon flow (dynamic regim). This work highlights a specific sensor response to each ammonia concentration at room temperature. It shows a quasi-linear relationship between the set of points of the real part of the response and the ammonia concentration. The authors are currently working on these issues as well as the interaction mechanism between adsorbed gas molecules and metal oxide films.

2018 ◽  
Vol 3 (3) ◽  
pp. 244-250 ◽  
Author(s):  
Dereck N. F. Muche ◽  
Flavio L. Souza ◽  
Ricardo H. R. Castro

A non-system specific method for the synthesis of metal oxide nanoparticles with high homogeneity, spherical morphology and high surface areas is proposed based on an aqueous precipitation.


2017 ◽  
Vol 114 (35) ◽  
pp. 9279-9283 ◽  
Author(s):  
Prateek Dongare ◽  
Ian MacKenzie ◽  
Degao Wang ◽  
David A. Nicewicz ◽  
Thomas J. Meyer

We describe here a surface-bound, oxide-based procedure for the photooxidation of a family of aromatic hydrocarbons by a phosphate-bearing flavin mononucleotide (FMN) photocatalyst on high surface area metal-oxide films.


2012 ◽  
Vol 10 (3) ◽  
pp. 826-832 ◽  
Author(s):  
A. Dhayal Raj ◽  
P. Suresh Kumar ◽  
D. Mangalaraj ◽  
N. Ponpandian ◽  
A. Albert Irudayaraj ◽  
...  

2002 ◽  
Vol 110 (1288) ◽  
pp. 1097-1099 ◽  
Author(s):  
Daiji SHIN ◽  
Satoshi SATO ◽  
Ryoji TAKAHASHI ◽  
Toshiaki SODESAWA

2015 ◽  
Vol 5 (1) ◽  
Author(s):  
Hee-Young Park ◽  
Injoon Jang ◽  
Namgee Jung ◽  
Young-Hoon Chung ◽  
Jaeyune Ryu ◽  
...  

Abstract Metal and metal oxide nanoparticles (NPs) supported on high surface area carbon (NP/Cs) were prepared by the physical vapor deposition of bulk materials on an α-D-glucose (Glu) substrate, followed by the deposition of the NPs on carbon supports. Using Glu as a carrier for the transport of NPs from the bulk materials to the carbon support surfaces, ultrafine NPs were obtained, exhibiting a stabilizing effect through OH moieties on the Glu surfaces. This stabilizing effect was strong enough to stabilize the NPs, but weak enough to not significantly block the metal surfaces. As only the target materials and Glu are required in our procedure, it can be considered environmentally friendly, with the NPs being devoid of hazardous chemicals. Furthermore, the resulting NP/Cs exhibited an improvement in activity for various electrochemical reactions, mainly attributed to their high surface area.


Sign in / Sign up

Export Citation Format

Share Document