Surface Modification of Pure Magnesium and Magnesium Alloy AZ91 by Friction Stir Processing

2015 ◽  
Vol 651-653 ◽  
pp. 796-801 ◽  
Author(s):  
Andreas Hütter ◽  
Wilfried Huemer ◽  
Claudia Ramskogler ◽  
Fernando Warchomicka ◽  
Aymen Lachehab ◽  
...  
Keyword(s):  
Mechanical Properties ◽  
Grain Size ◽  
Magnesium Alloy ◽  
Magnesium Alloys ◽  
Friction Stir Processing ◽  
Phase Distribution ◽  
Intermetallic Phases ◽  
Friction Stir ◽  
Alloy Az91 ◽  
Magnesium Alloy Az91

In recent years an interest in magnesium and magnesium alloys not only for the automotive industry but also for medical applications was increasing due to the low density and good specific strength. Magnesium alloys show good castability but lower ductility and strength than wrought materials. For this reason, refinement of grains and homogenous distribution of intermetallic phases are needed to improve formability and mechanical properties. On the other hand, the degradation of the material by corrosion is influenced by the grain size and phase distribution. This work investigates the microstructure evolution of pure Mg and magnesium alloy AZ91 by friction stir processing (FSP) technique. FSP experiments are carried out by constant force, optimizing the rotation and feed rate to obtain a homogenous microstructure, free of defects stir zone, good surface finishing and stable conditions during the process. The results show that the grain size is affected by the spindle speed. Increasing the number of passes reduces also the size of the grains and the intermetallic phases in the AZ91 alloy. The overlapping of passes between overlapping ratio 0.5 to 1 determines an uniform depth of the stir zone over a larger surface area.Hardness measurements are performed to evaluate the influence of FSP parameters on the mechanical properties. The degradation rate of the studied FSP Mg alloys is determined by hydrogen evolution in corrosion immersion tests, which depend strongly on the phase distribution and grain size.

scholarly journals Friction Stir Processing of the Magnesium Alloy AZ61: Grain Size Refinement and Mechanical Properties

2012 ◽  
Vol 706-709 ◽  
pp. 1823-1828 ◽  
Author(s):  
J.A. del Valle ◽  
P. Rey ◽  
D. Gesto ◽  
D. Verdera ◽  
Oscar A. Ruano
Keyword(s):  
Mechanical Properties ◽  
Grain Size ◽  
Magnesium Alloy ◽  
Friction Stir Processing ◽  
Superplastic Forming ◽  
Important Change ◽  
Heat Extraction ◽  
Processing Temperature ◽  
Friction Stir ◽  
Size Refinement

The effect of friction stir processing (FSP), on the microstructure and mechanical properties of a magnesium alloy AZ61 has been analyzed. This is a widely used wrought magnesium alloy provided in the form of rolled and annealed sheets with a grain size of 45 μm. The FSP was performed with an adequate cooling device in order to increase the heat extraction and reduce the processing temperature. The final microstructure showed a noticeable grain size refinement down to values close to 1.8 μm and an important change in texture. The change in texture favors basal slip during tensile testing leading to an increase of ductility and a decrease in yield stress. The stability of the grain size and the creep behavior at high temperatures were investigated. The optimum conditions for superplastic forming were determined; however, the presence of a large amount of cavities precludes the achievement of high superplastic elongations. Additionally, these results are compared with those obtained by severe hot rolling.

Effects of Nd on Mechanical Properties of Magnesium Alloy AZ91

2014 ◽  
Vol 488-489 ◽  
pp. 256-259
Author(s):  
Hui Zhen Jiang ◽  
Quan An Li ◽  
Xiao Ya Chen ◽  
Lei Lei Chen
Keyword(s):  
Mechanical Properties ◽  
Grain Size ◽  
Melting Point ◽  
Magnesium Alloy ◽  
Room Temperature ◽  
High Melting ◽  
High Melting Point ◽  
Alloy Az91 ◽  
Magnesium Alloy Az91

The effect of Nd on the mechanical properties of magnesium alloy AZ91 has been studied. The results show that the addition of 1wt.%Nd can refine the grain size, cause the formation of high melting point Al2Nd phase and reduce the amount of β-Mg17Al12 phase. and enhance the mechanical properties of magnesium alloy AZ91 at room temperature and 150°C.

1044 Fatigue Behaviour of Cast Magnesium alloy AZ91 Microstructurally Modified by Friction Stir Processing

2008 ◽  
Vol 2008.6 (0) ◽  
pp. 177-178
Author(s):  
Keiro TOKAJI ◽  
Yoshihiko UEMATSU ◽  
Kazuma FUJIWARA ◽  
Yasunari TOZAKI ◽  
Hideaki SHIBATA
Keyword(s):  
Magnesium Alloy ◽  
Friction Stir Processing ◽  
Fatigue Behaviour ◽  
Friction Stir ◽  
Alloy Az91 ◽  
Magnesium Alloy Az91 ◽  
Cast Magnesium Alloy ◽  
Cast Magnesium

Enhanced mechanical properties of as-cast Mg-Al-Ca magnesium alloys by friction stir processing

2021 ◽  
Vol 296 ◽  
pp. 129880
Author(s):  
Zahra Nasiri ◽  
Mahmoud Sarkari Khorrami ◽  
Hamed Mirzadeh ◽  
Massoud Emamy
Keyword(s):  
Mechanical Properties ◽  
Magnesium Alloys ◽  
Friction Stir Processing ◽  
Friction Stir

scholarly journals Novel grain refinement of AZ91E magnesium alloy and the effect on hot tearing during solidfication

2021 ◽  
Author(s):  
Abdallah Elsayed
Keyword(s):  
Mechanical Properties ◽  
Grain Size ◽  
Magnesium Alloy ◽  
Grain Refinement ◽  
Magnesium Alloys ◽  
Hot Tearing ◽  
Grain Refining ◽  
Grain Refiner ◽  
Structural Applications ◽  
Hot Tearing Susceptibility

For the A1-5Ti-1B grain refiner, the addition of 0.1 wt.% provided a 68 % reduction in grain size as compared to the unrefined AZ91E alloy at a holding time of five minutes. Grain growth restriction by TiB₂ particles was the source of grain refinement. With the addition of A1-5Ti-1B, only a small reduction in hot tearing susceptibility ws observed because large TiA1₃ particles bonded poorly with the eutectic and blocked feeding channels.The addition of 1.0 wt.% A1-1Ti-3B provided a grain size reduction of 63% as compared to the unrefined AZ91E alloy at a holding time of five minutes. The grain refinement with A1-1Ti-3B addition was attributed to a combination of TiB₂ grain growth restriction and A1B₂ nucleating sites. A significant reduction in hot tearing susceptibility was observed with A1-1Ti-3B addition as a result of a higher cooling rate and shorter local soldification time as compared to the AZ91E alloy. The reduction in hot tearing susceptibility was attributed to the good interface between eutectic and TiB₂ particles. Both grain refiners demonstrated a good resistance to fading during the holding times investigated. In addition, the AZ91E + A1-5Ti-1B and AZ91E + A1-1Ti-3B castings showed much fewer dislocation networks as compared to the untreated AZ91E casting.The development of efficient A1-Ti-B refiners can also improve castability of magnesium alloys. In addition, the fade resistant A1-Ti-B grain refiners can reduce operating costs and maintain productivity on the foundry floor. Thus, magnesium alloy with A1-Ti-B treatment have the potential for more demanding structural applications in the automobile and aerospace industries. Vehicle weight in the aerospace and automotive industries directly impacts carbon emissions and fuel efficiency. An increase in the use of lightweight materials for structural applications will result in lighter vehicles. Low density materials, such as magnesium (1.74 g/cm³) are a potential alternative to aluminium (2.70 g/cm³), to reduce component weight in structural applications.However, current magnesium alloys still do not have adequate mechanical properties and castability to meet the performance specifications of the automotive and aerospace industries. Grain refinement can significantly improve mechanical properties and reduce hot tearing during permanent mould casting. Recently, Al-Ti-B based grain refiners have shown potential in grain refining magnesium-aluminum alloys such as AZ91E. This study investigates the grain refining efficiency and fading of A1-5Ti-1B and A1-1Ti-3B in AZ91E magnesium alloy and their subsequent effect on hot tearing.The grain refiners were added at 0.1, 0.2, 0.5 and 1.0 wt.% levels. For the grain refinement and fading experiments, the castings were prepared using graphite moulds with holding times of 5, 10 and 20 minutes. For the hot tearing experiments, castings were produced representing the optimal addition level of each grain refiner. The castings were prepared using a permanent mould with pouring and mould temperatures of 720 and 180 ºC, respectively. The castings were characterized using SEM, TEM, optical microscopy and thermal analysis.

Microstructural and Mechanical Properties of a Solid-State Additive Manufactured Magnesium Alloy

2021 ◽  
pp. 1-21
Author(s):  
Thomas Robinson ◽  
Malcolm Williams ◽  
Harish Rao ◽  
Ryan P. Kinser ◽  
Paul Allison ◽  
...  
Keyword(s):  
Mechanical Properties ◽  
Additive Manufacturing ◽  
Solid State ◽  
Magnesium Alloy ◽  
Magnesium Alloys ◽  
Process Parameters ◽  
Weight Ratio ◽  
Structural Components ◽  
Friction Stir ◽  
Magnesium Alloy Az31b

Abstract In recent years, additive manufacturing (AM) has gained prominence in rapid prototyping and production of structural components with complex geometries. Magnesium alloys, whose strength-to-weight ratio is superior compared to steel and aluminum alloys, have shown potential in lightweighting applications. However, commercial beam-based AM technologies have limited success with magnesium alloys due to vaporization and hot cracking. Therefore, as an alternative approach, we propose the use of a near net-shape solid-state additive manufacturing process, Additive Friction Stir Deposition (AFSD), to fabricate magnesium alloys in bulk. In this study, a parametric investigation was performed to quantify the effect of process parameters on AFSD build quality including volumetric defects and surface quality in magnesium alloy AZ31B. In order to understand the effect of the AFSD process on structural integrity in the magnesium alloy AZ31B, in-depth microstructure and mechanical property characterization was conducted on a bulk AFSD build fabricated with a set of acceptable process parameters. Results of the microstructure analysis of the as-deposited AFSD build revealed bulk microstructure similar to wrought magnesium alloy AZ31 plate. Additionally, similar hardness measurements were found in AFSD build compared to control wrought specimens. While tensile test results of the as-deposited AFSD build exhibited a 20 percent drop in yield strength, nearly identical ultimate strength was observed compared to the wrought control. The experimental results of this study illustrate the potential of using the AFSD process to additively manufacture Mg alloys for load bearing structural components with achieving wrought-like microstructure and mechanical properties.

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