Local Mechanical Characterization of Metal Foams by Nanoindentation

2015 ◽  
Vol 662 ◽  
pp. 59-62 ◽  
Author(s):  
Jiří Němeček ◽  
Vlastimil Kralik
Keyword(s):  
Cell Walls ◽  
Plastic Material ◽  
Spherical Indentation ◽  
Isotropic Hardening ◽  
Plastic Properties ◽  
Macro Scale ◽  
Static Indentation ◽  
Indentation Tests ◽  
Constitutive Parameters

This paper deals with microstructure and micromechanical properties of two commercially available aluminium foams (Alporas and Aluhab). Since none of the materials is available in a bulk and standard mechanical testing at macro-scale is not possible the materials need to be tested at micro-scale. To obtain both elastic and plastic properties quasi-static indentation was performed with two different indenter geometries (Berkovich and spherical tips). The material phase properties were analyzed with statistical grid indentation method and micromechanical homogenization was applied to obtain effective elastic wall properties. In addition, effective inelastic properties of cell walls were identified with spherical indentation. Constitutive parameters related to elasto-plastic material with linear isotropic hardening (the yield point and tangent modulus) were directly deduced from the load–depth curves of spherical indentation tests using formulations of the representative strain and stress introduced by Tabor.

Identification of Stress-Strain Relation of Aluminium Foam Cell Wall by Spherical Nanoindentation

2014 ◽  
Vol 606 ◽  
pp. 11-14 ◽  
Author(s):  
Vlastimil Králík ◽  
Jiří Němeček ◽  
Petr Koudelka
Keyword(s):  
Cell Walls ◽  
Foam Cell ◽  
Plastic Material ◽  
Aluminium Foam ◽  
Analytical Models ◽  
Spherical Indentation ◽  
Isotropic Hardening ◽  
Stress Strain Relation ◽  
Indentation Tests ◽  
Constitutive Parameters

The aim of this paper is to identify, in addition to elastic properties, inelastic properties of tiny aluminium foam cell walls that can be directly deduced from the loaddepth curves of spherical indentation tests using formulations of the representative strain and stress. Constitutive parameters related to plastic material with linear isotropic hardening, the yield point (122 ± 17 MPa) and tangent modulus (950 ± 377 MPa), were obtained in this work. Spherical indentation and uniaxial tension experiments have also been performed on a standard aluminium alloy EN AW 6060 to explore the accuracy of the analytical models used to predict the uniaxial stressstrain in wide strain ranges. Some deviations received from different tests arose and, therefore, their effect on the evaluation of inelastic properties was discussed.

scholarly journals Numerical verification for instrumented spherical indentation techniques in determining the plastic properties of materials

2009 ◽  
Vol 24 (12) ◽  
pp. 3653-3663 ◽  
Author(s):  
Taihua Zhang ◽  
Peng Jiang ◽  
Yihui Feng ◽  
Rong Yang
Keyword(s):  
Numerical Experiments ◽  
Spherical Indentation ◽  
Numerical Verification ◽  
Instrumented Indentation ◽  
Plastic Properties ◽  
Wide Range ◽  
Validity Range ◽  
Indentation Tests ◽  
Properties Of Materials ◽  
Indentation Methods

Instrumented indentation tests have been widely adopted for elastic modulus determination. Recently, a number of indentation-based methods for plastic properties characterization have been proposed, and rigorous verification is absolutely necessary for their wide application. In view of the advantages of spherical indentation compared with conical indentation in determining plastic properties, this study mainly concerns verification of spherical indentation methods. Five convenient and simple models were selected for this purpose, and numerical experiments for a wide range of materials are carried out to identify their accuracy and sensitivity characteristics. The verification results show that four of these five methods can give relatively accurate and stable results within a certain material domain, which is defined as their validity range and has been summarized for each method.

Small Scale Plastic Yielding of Mg Alloys Assessed with Nanoindentation

2020 ◽  
Vol 405 ◽  
pp. 339-344
Author(s):  
Jiří Němeček ◽  
Jan Maňák ◽  
Jiří Němeček
Keyword(s):  
Focused Ion Beam ◽  
Electron Backscatter Diffraction ◽  
Ion Beam ◽  
Az31 Alloy ◽  
Small Scale ◽  
Spherical Indentation ◽  
Plastic Properties ◽  
Indentation Tests ◽  
Order Of Magnitude ◽  
Volume Characteristics

The paper investigates deformations and plastic properties received from different material volumes and tests of magnesium samples. Small volume characteristics gained on single Mg crystals are compared to polycrystalline AZ31 alloy. Results of tests employing nanoindentation, focused ion beam milling and electron backscatter diffraction techniques are presented. Large differences were found between micro-beam testing and spherical indentation tests having the volume one order of magnitude apart. The plastic strength scaling factor was found 1.7 for the studied grain configurations and volumes.

Instrumented Indentation Contact with Sharp Probes of Varying Acuity

2007 ◽  
Vol 1049 ◽  
Author(s):  
Dylan J. Morris
Keyword(s):  
Plastic Material ◽  
Instrumented Indentation ◽  
Nano Scale ◽  
Indentation Toughness ◽  
Preliminary Model ◽  
Initiation And Propagation ◽  
Cube Corner ◽  
Macro Scale ◽  
Indentation Tests ◽  
Toughness Measurement

AbstractWhile elastic and plastic material property extraction from instrumented indentation tests has been well-studied, similarly-based fracture property measurement remains difficult. Furthermore, estimation of the fracture toughness requires measurement of the crack lengths from a micrograph, which makes nano-scale indentation toughness measurement expensive and difficult. Initiation and propagation of cracks on the nano-scale requires a more acute indenter than a Berkovich or sphere, such as the cube-corner pyramid. Experiments described here were performed on a range of elastic, plastic and brittle materials with diamond indenters of acuity varying between the Berkovich and the cube-corner. These experiments reveal some of what is changed and what remains the same, when the acuity of the probe is changed, when fracture is initiated at the contact, or both. A preliminary model for the physical origin of the extra crack-driving power of acute probes is presented in light of these, and complementary macro-scale in-situ indentation experiments. This work provides the basis for development of instrumented indentation-based nano-scale toughness measurement.

Spherical indentation of ductile power law materials

2004 ◽  
Vol 19 (9) ◽  
pp. 2641-2649 ◽  
Author(s):  
Roberta Mulford ◽  
Robert J. Asaro ◽  
Robert J. Sebring
Keyword(s):  
Power Law ◽  
Contact Surface ◽  
Indentation Test ◽  
Strain Curve ◽  
Spherical Indentation ◽  
Actual Contact ◽  
Indentation Tests ◽  
Surface Profiles ◽  
Constitutive Parameters ◽  
Versus Strain

A procedure for extracting simple constitutive parameters from microindentationtests is described. The analysis used to interpret the indentation tests is based onthe analysis of the spherical indentation test developed by Hill et al. for power law materials. Indentation tests are supplemented by scanning interference microscopyof the residual indented surface profiles and a method is suggested for using the residual surface profiles to estimate the actual contact surface. This, in turn, allowsfor the construction of the entire stress versus strain curve.

Inverse Characterization of Nonlinear Anisotropic Mechanical Properties of Engineered Cardiovascular Tissues Using a Spherical Indentation Test

2007 ◽  
Author(s):  
M. A. J. Cox ◽  
R. A. Boerboom ◽  
C. V. C. Bouten ◽  
N. J. B. Driessen ◽  
F. P. T. Baaijens
Keyword(s):  
Mechanical Properties ◽  
Soft Tissues ◽  
Indentation Test ◽  
Tensile Tests ◽  
Material Behavior ◽  
Uniaxial Tensile ◽  
Spherical Indentation ◽  
Mechanical Conditioning ◽  
Indentation Tests

Over the last few years, research interest in tissue engineering as an alternative for e.g. current treatment and replacement strategies for cardiovascular and heart valve diseaes has significantly increased. In vitro mechanical conditioning is an essential tool for engineering strong implantable tissues [1]. Detailed knowledge of the mechanical properties of the native tissue as well as the properties of the developing engineered constructs is vital for a better understanding and control of the mechanical conditioning process. The typical highly nonlinear and anisotropic behavior of soft tissues puts high demands on their mechanical characterization. Current standards in mechanical testing of soft tissues include (multiaxial) tensile testing and indentation tests. Uniaxial tensile tests do not provide sufficient information for characterizing the full anisotropic material behavior, while biaxial tensile tests are difficult to perform, and boundary effects limit the test region to a small central portion of the tissue. In addition, characterization of the local tissue properties from a tensile test is non-trivial. Indentation tests may be used to overcome some of these limitations. Indentation tests are easy to perform and when indenter size is small relative to the tissue dimensions, local characterization is possible. Therefore, we propose a spherical indentation test using finite deformations.

Prediction of the Bilinear Stress-Strain Curve of Engineering Material by Nanoindentation Test

2010 ◽  
Vol 437 ◽  
pp. 589-593
Author(s):  
Tung Sheng Yang ◽  
Te Hua Fang ◽  
C.T. Kawn ◽  
G.L. Ke ◽  
S.Y. Chang
Keyword(s):  
Plastic Material ◽  
Bulk Material ◽  
Strain Curve ◽  
Nanoindentation Test ◽  
Displacement Curve ◽  
Film Material ◽  
Stress Strain Curve ◽  
Stress Strain ◽  
Plastic Properties ◽  
Indentation Tests

Instrumented indentation is widely used to probe the elastic and plastic properties of engineering materials. Finite Element Method (FEM) has been widely used for numerical simulation of indentation tests on bulk and film material in order to analyze its deformation response. This study proposed an improved technique to determine the stress-strain curve of bulk material. FEM in conjunction with an abductive network is used to predict the stress-strain relationship of bilinear elastic-plastic material from the nanoindentation test’s force-displacement curve.

Spherical Indentation Testing on Ballistic Gelatin and Perma-Gel

2014 ◽  
Author(s):  
Amélie Caron-Laramée ◽  
Martin Brouillette
Keyword(s):  
Viscoelastic Properties ◽  
Loss Modulus ◽  
Indentation Test ◽  
Spherical Indentation ◽  
Strain Rates ◽  
Dynamic Indentation ◽  
Hertz Theory ◽  
Static Indentation ◽  
Indentation Tests ◽  
Ballistic Gelatin

This paper reports on a series of indentation tests performed on ballistic gelatin (10%) and Perma-Gel. In these experiments, both gels were submitted to strain rates varying from 0.1 and 2.7 s−1 in quasi-static indentation. Two methods were used to evaluate the Young’s modulus from quasi-static indentation test: the Hertz theory and the Oliver-Pharr model. The dependence of strain rate was also analyzed. Finally, dynamic indentation tests were performed on both gels at frequencies of 0.1 and 1.0 Hz to evaluate the gel’s viscoelastic properties characterized by the storage modulus, the loss modulus and the phase angle.

Characterization of machined polystyrene foam

1989 ◽  
Vol 47 ◽  
pp. 372-373
Author(s):  
C. W. Price ◽  
E. F. Lindsey ◽  
R. M. Franks ◽  
M. A. Lane
Keyword(s):  
Surface Finish ◽  
Cell Walls ◽  
Surface Structures ◽  
Efficient Technique ◽  
Low Density ◽  
Polystyrene Foam ◽  
Planar Surfaces ◽  
Machining Characteristics

Diamond-point turning is an efficient technique for machining low-density polystyrene foam, and the surface finish can be substantially improved by grinding. However, both diamond-point turning and grinding tend to tear and fracture cell walls and leave asperities formed by agglomerations of fragmented cell walls. Vibratoming is proving to be an excellent technique to form planar surfaces in polystyrene, and the machining characteristics of vibratoming and diamond-point turning are compared.Our work has demonstrated that proper evaluation of surface structures in low density polystyrene foam requires stereoscopic examinations; tilts of + and − 3 1/2 degrees were used for the stereo pairs. Coating does not seriously distort low-density polystyrene foam. Therefore, the specimens were gold-palladium coated and examined in a Hitachi S-800 FESEM at 5 kV.

Masonry: the brittle or plastic material?

2019 ◽  
pp. 22-28
Keyword(s):  
Plastic Material ◽  
Experimental Studies ◽  
Point Of View ◽  
Plastic Properties ◽  
Plastic Deformations ◽  
Base Materials ◽  
Stress States ◽  
Creep Deformations ◽  
Structural Point

The results of experimental studies of masonry on the action of dynamic and static (short-term and long-term) loads are presented. The possibility of plastic deformations in the masonry is analyzed for different types of force effects. The falsity of the proposed approach to the estimation of the coefficient of plasticity of masonry, taking into account the ratio of elastic and total deformations of the masonry is noted. The study of the works of Soviet scientists revealed that the masonry under the action of seismic loads refers to brittle materials in the complete absence of plastic properties in it in the process of instantaneous application of forces. For the cases of uniaxial and plane stress states of the masonry, data on the coefficient of plasticity obtained from the experiment are presented. On the basis of experimental studies the influence of the strength of the so-called base materials (brick, mortar) on the bearing capacity of the masonry, regardless of the nature of the application of forces and the type of its stress state, is noted. The analysis of works of prof. S. V. Polyakov makes it possible to draw a conclusion that at the long application of the load, characteristic for the masonry are not plastic deformations, but creep deformations. It is shown that the proposals of some authors on the need to reduce the level of adhesion of the mortar to the brick for the masonry erected in earthquake-prone regions in order to improve its plastic properties are erroneous both from the structural point of view and from the point of view of ensuring the seismic resistance of structures. It is noted that the proposal to assess the plasticity of the masonry of ceramic brick walls and large-format ceramic stone with a voidness of more than 20% is incorrect, and does not meet the work of the masonry of hollow material. On the basis of the analysis of a large number of research works it is concluded about the fragile work of masonry.

Sign in / Sign up

Export Citation Format

Share Document