In Situ Decomposition of Silicon Nitride Particles in Titanium Composite and its Mechanical Properties

2017 ◽  
Vol 737 ◽  
pp. 38-43
Author(s):  
Hisashi Imai ◽  
Hiroyasu Yamabe ◽  
Katsuyoshi Kondoh ◽  
Junko Umeda ◽  
Anak Khantachawana
Keyword(s):  
Mechanical Properties ◽  
Silicon Nitride ◽  
Solid Phase ◽  
High Strength ◽  
Solid Solution Strengthening ◽  
Plasma Sintering ◽  
Spark Plasma ◽  
Solution Strengthening ◽  
Ti Powder

Dependence of the mechanical properties of PM extruded titanium with the silicon nitride (Si3N4) on solid phase decomposition of Si3N4 was investigated. Si3N4 particles within Ti composite powder were decomposed during spark plasma sintering at 1223 K with 30 MPa pressure for 3.6 ks; and then, decomposition by-products of nitrogen and silicon atoms were defused into titanium matrix. The extruded Ti-1.0 mass% Si3N4 composite showed ultimate tensile strength (UTS) of 1139 MPa, and yield stress (0.2%YS) of 1065 MPa. UTS and 0.2%YS of P/M extruded Ti-1.0 mass% Si3N4 composite were 2 and 2.5 times compared to extruded pure Ti powder material, respectively. It was considered that the solid solution strengthening of both nitrogen and silicon originated from Si3N4 caused the high strength of PM extruded Ti-1.0 mass% Si3N4 composite.

Influence of Carbon Reinforcements on the Mechanical Properties of Ti Composites via Powder Metallurgy and Hot Extrusion

2013 ◽  
Vol 750 ◽  
pp. 40-43 ◽  
Author(s):  
Shu Feng Li ◽  
Bin Sun ◽  
Katsuyoshi Kondoh ◽  
Takanori Mimoto ◽  
Hisashi Imai
Keyword(s):  
Mechanical Properties ◽  
Powder Metallurgy ◽  
Carbon Nanofiber ◽  
Hot Extrusion ◽  
Strengthening Mechanism ◽  
Matrix Composites ◽  
Solid Solution Strengthening ◽  
Plasma Sintering ◽  
Spark Plasma ◽  
Solution Strengthening

Ti metal matrix composites (Ti–MMCs) reinforced by vapor grown carbon nanofiber (VGCF) and graphite particle (Gr) were prepared via powder metallurgy and hot extrusion. Ti with 0~0.4wt% VGCF/Gr mixture powders were consolidated by using spark plasma sintering (SPS) at 800 °C. Hot extrusion was then performed at 1000 °C with an extrusion ratio of 37:1. Microstructures and mechanical properties of the as-extruded Ti composites were investigated. Tensile strength of Ti–VGCF/Gr composites was steadily augmented when additions of VGCF/Gr were increased from 0.1 to 0.4 wt%. YS and UTS were increased 40.2% and 11.4% for Ti–0.4wt%VGCF as compared to pure Ti, while those values were 30.5% and 2.1% for Ti–0.4wt%Gr. The strengthening mechanism including grain refinement, carbon solid solution strengthening and dispersion hardening of TiC/carbon was discussed in detail.

High-strength Al87Ni8La5 bulk alloy produced by spark plasma sintering of gas atomized powders

2009 ◽  
Vol 24 (9) ◽  
pp. 2909-2916 ◽  
Author(s):  
Sergio Scudino ◽  
Kumar B. Surreddi ◽  
Hoang V. Nguyen ◽  
Gang Liu ◽  
Thomas Gemming ◽  
...  
Keyword(s):  
Mechanical Properties ◽  
Spark Plasma Sintering ◽  
Room Temperature ◽  
Bulk Material ◽  
High Strength ◽  
Compression Tests ◽  
Bulk Alloy ◽  
Plasma Sintering ◽  
Spark Plasma

In situ devitrification and consolidation of gas atomized Al87Ni8La5 glassy powders into highly dense bulk specimens was carried out by spark plasma sintering. Room temperature compression tests of the consolidated bulk material reveal remarkable mechanical properties, namely, high compression strength of 930 MPa combined with plastic strain exceeding 25%. These findings demonstrate that the combined devitrification and consolidation of glassy precursors by spark plasma sintering is a suitable method for the production of Al-based materials characterized by high strength and considerable plastic deformation.

scholarly journals Sintering of Ti-based biomedical alloys with increased oxygen content from elemental powders

2020 ◽  
Vol 321 ◽  
pp. 05010
Author(s):  
J. Stráský ◽  
J. Kozlík ◽  
K. Bartha ◽  
D. Preisler ◽  
T. Chráska
Keyword(s):  
Mechanical Properties ◽  
Oxygen Content ◽  
High Strength ◽  
Simple Approach ◽  
Fine Tuning ◽  
Powder Metallurgy Method ◽  
Ti Alloys ◽  
Plasma Sintering ◽  
Spark Plasma ◽  
Low Modulus

Revived interest for beta Ti alloys with increased oxygen content is motivated by the prospect of achieving material with low modulus and high strength simultaneously. Fine tuning of amount of oxygen and beta stabilizing elements is critical for achieving good mechanical properties. This study shows that powder metallurgy method of spark plasma sintering is capable of producing Ti-Nb-Zr-O alloys from elemental powders. This simple approach allows for quick sampling and production of several alloys with various chemical composition. Elemental powders were mixed with appropriate amount of titanium dioxide to achieve Ti-29Nb-7Zr-0.7O alloy. Sintering was performed at 1400 - 1500 °C for 15 – 30 minutes.

Effect of VC Addition on Microstructure and Mechanical Properties of Ultrafine Grained WC-Co Alloys

2014 ◽  
Vol 893 ◽  
pp. 444-448 ◽  
Author(s):  
Xue Mei Liu ◽  
Xiao Yan Song ◽  
Hai Bin Wang ◽  
Yang Gao ◽  
Yao Wang
Keyword(s):  
Mechanical Properties ◽  
Composite Powder ◽  
Cemented Carbides ◽  
Comprehensive Properties ◽  
Microstructure And Mechanical Properties ◽  
Plasma Sintering ◽  
Ultrafine Grained ◽  
Spark Plasma ◽  
Co Alloys

This study was focused on the effect of VC addition on the microstructure and mechanical properties of the prepared ultrafine grained cemented carbides. VC was added to the rawoxide materials which were synthesized to the WC-Co composite powder by the in-situ reduction and carbonization process. The ultrafine grained WC-Co alloys were fabricated by the spark plasma sintering technique using the prepared WC-Co composite powder. The phase constitution, microstructure characteristics and mechanical properties of the sintered ultrafine grained cemented carbides were analyzed quantitatively. The study proposed that VC plays a significant role in decreaseing the grain size of the prepared WC-Co alloy. The ultrafine grained WC-Co alloy with high comprehensive properties can be obtained as an appropriate addition of VC in the developed process.

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