Morphology and Mechanical Properties of a Composite Coating by Electrostatic Dry Spray Method

2021 ◽  
Vol 886 ◽  
pp. 168-174
Author(s):  
Mohanad N. Al-Shroofy ◽  
Hanna A. Al-Kaisy ◽  
Rabab Chalaby

Powder spray coating was used for many applications such as paint decoration and protection against corrosive environments. The electrostatic spray method is used to lower the manufacturing cost and the environmental effect during the production process. It is done by electrostatic device and spray gun to create a layer on the substrate to play a protective role. Different dry powders were mixed to form a composite mixture consisted of Al2O3 and SiC or ZrSiO4 with Al powder as a binder. The powders mixture was deposited by electrostatic spray technique with a high voltage of 15 kV on a low carbon steel substrate of (40 x 10 x 4) mm in dimensions. Two groups of mixtures were used to form the coating layers. Powders of Al2O3 with (20 and 40) weight percent (wt%) of SiC as the first group and (20 and 40) wt% of ZrSiO4 as the second group were used. 5 wt% of Al powder was added as a binder, and the samples were heat treated at 900 C° for 2 hours. A detailed characterization of the composite coating layers was performed using XRD, SEM, and EDX, as well as, micro-hardness measurements. The obtained surface composite layers were smooth and having good particle distribution which leads to enhance roughness values (Ra). Furthermore, the hardness increased with increasing the amount of carbide and zirconia, and the obtained layers show no presence of defects or cracks.

2021 ◽  
Vol 39 (3A) ◽  
pp. 504-511
Author(s):  
Rasha A. Issa ◽  
Mohanad N. Al-Shroofy ◽  
Hanna A. Al-Kaisy

This work aims preparation of polymer-based biocomposite coating by electrostatic spray method onto 316L stainless steel substrate, the present work will compare the effects of incorporation of Al2O3 and TiO2 particles at a different percentage of (10,15 and 20 % wt. from Al2O3 and TiO2 with (90,85 and 80% wt. PMMA - based electrostatic deposition coating is studied. The structure and chemical composition of composite coatings were studied by using (SEM) & (EDS) and mechanical properties (Microhardness and adhesion strength) of Al2O3-TiO2-PMMA composite coating. The SEM&EDX result showed that the composite coating to be dense with uniform dispersants and continuous with a well homogenous mixture within coating exhibits a much-increased Microhardness and remarkably improved adhesion strength.


2013 ◽  
Vol 734-737 ◽  
pp. 2269-2272
Author(s):  
Hong Mei Zhu ◽  
Shu Mei Lei ◽  
Tong Chun Kuang

In this paper, a low carbon steel was used as the substrate to prepare the carbon nanostructural materials by the oxygen-acetylene flame method. The experimental results show that the composite products including nodular carbon nanoparticles and amorphous carbon were obtained on the substrate after a mechanical polishing pretreatment. Comparatively, the short tubular carbon nanofibers with the diameter of around 100 nm were deposited on the substrate pretreated by dipping in the concentrated nitric acid solution. The possible mechanism for the growth of such carbon nanofibers was discussed.


2012 ◽  
Vol 57 (2) ◽  
pp. 517 ◽  
Author(s):  
M. Żelechower ◽  
J. Kliś ◽  
E. Augustyn ◽  
J. Grzonka ◽  
D. Stróż ◽  
...  

The Microstructure of AnnealedGalfanCoating on Steel SubstrateThe commercially availableGalfancoating containing 5-7wt.% of Al deposited on the low carbon steel substrate by hot dipping has been examined with respect to the microstructure of the coating/substrate interface area. The application of several experimental techniques (SEM/EDS, XRD, TEM/AEM/EDS/ED) allowed demonstrating the two-phase structure of the alloy coating in non-treated, commercially availableGalfansamples: Zn-rich pre-eutectoidηphase grains are surrounded by lamellar eutectics ofβ-Al andη-Zn. The transition layer between the alloy coating and steel substrate with the considerably higher Al content (SEM/EDS, TEM/EDS) has been found in both non-treated and annealed samples (600°C/5 minutes). Only the monoclinic FeAl3Znxphase however was revealed in the annealed sample (TEM/electron diffraction) remaining uncertain the presence of the orthorhombic Fe2Al5Znxphase, reported by several authors.


Author(s):  
R Raveen ◽  
J Yoganandh ◽  
S SathieshKumar ◽  
N Neelakandeswari

Cobalt–graphene nanocomposite coatings possess unique mechanical and tribological properties which attract researchers to explore its potential for various industrial applications. This research work presents the investigation on cobalt–graphene nanocomposite coatings, with two different graphene compositions cobalt–graphene (0.15 and 0.45 wt%) prepared by pulsed electrodeposition from aqueous bath involving cobalt chloride, trisodium citrate, and citric acid on low carbon steel substrate. Studies on coating morphology, microhardness, tribological characteristics such as wear and corrosion for the cobalt–graphene nanocomposite coatings were reported. Cobalt–graphene (0.45 wt%) nanocomposite coating which exhibits low wear rate in all load conditions due to the self-lubricating property of graphene and cobalt–graphene (0.15 wt%) nanocomposite coating shows higher corrosion resistance due to its layered cauliflower surface morphology.


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