Effect of Heat Treatment Temperature on the Mechanical Property in Cast TiNi Shape Memory Alloy

2007 ◽  
Vol 561-565 ◽  
pp. 1493-1496
Author(s):  
Kazuhiro Kitamura ◽  
Yutaka Sawada ◽  
Toshio Kuchida ◽  
Tadashi Inaba ◽  
Masataka Tokuda ◽  
...  
Keyword(s):  
Mechanical Properties ◽  
Heat Treatment ◽  
Shape Memory Alloy ◽  
Tensile Test ◽  
Shape Memory ◽  
Treatment Temperature ◽  
Scanning Calorimetry ◽  
Temperature Synthesis ◽  
Treatment Conditions ◽  
High Temperature Synthesis

The heat treatment effect of a cast shape memory alloy (SMA) from self-propagating high temperature synthesis (SHS) ingot was investigated. The composition of SHS ingot was Ti-50.8at%Ni. DSC and Tensile test specimens were cast by lost-wax process from SHS ingot. The heat treatment conditions were 400°C-60min., 500°C-60min. and 600°C-60min. for DSC and 400°C-60min. and 500°C-60min. for tensile test. Transformation temperatures were measured by differential scanning calorimetry (DSC). Mechanical properties were measured by a tensile test at several temperatures. The effects of heat treatment temperatures were same as a general TiNi wire material.

The Effect of Heat Treatment on the Shape Memory Effect of Ni-Ti Alloy Ultra-Thin Wires

2011 ◽  
Vol 332-334 ◽  
pp. 912-915
Author(s):  
Dan Zhang ◽  
Lei Xu ◽  
Rui Wang ◽  
Li Feng Xu
Keyword(s):  
Heat Treatment ◽  
Shape Memory Alloy ◽  
Shape Memory ◽  
Shape Memory Effect ◽  
Memory Effect ◽  
Crystal Morphology ◽  
Treatment Temperature ◽  
Ti Alloy ◽  
Thin Wires ◽  
Treatment Conditions

Various heat treatment conditions with temperature scans of 300-700 °C, and annealing time scans of 1-4 hours were adopted in the annealing of Ti-49.5at.%-Ni shape memory alloy ultra thin wires. The mechanical hysteretic curves and the crystal morphology were obtained by the tensile-recovery testing and scan electric microscopes (SEM). The result shows that the shape memory effect of Ni-Ti alloy first decline after rising with the heat treatment temperature increases. Alloy with heat treatment effect in 500°C, presents the best. Time is not a significant factor for heat treatment.

INFLUENCES OF HEAT TREATMENT ON TRANSFORMATION BEHAVIORS OF NEAR-EQUIATOMIC POROUS NITI SHAPE MEMORY ALLOY

2010 ◽  
Vol 24 (15n16) ◽  
pp. 2410-2416
Author(s):  
H. C. JIANG ◽  
Y. CHEN ◽  
S. W. LIU ◽  
L. J. RONG
Keyword(s):  
Heat Treatment ◽  
Shape Memory Alloy ◽  
Shape Memory ◽  
Niti Alloy ◽  
Niti Shape Memory Alloy ◽  
Scanning Calorimetry ◽  
Pore Characteristics ◽  
Transformation Temperatures ◽  
Porous Niti ◽  
High Temperature Synthesis

The pore characteristics and pore size distribution of porous near-equiatomic NiTi shape memory alloy fabricated by self-propagating high-temperature synthesis (SHS) are described in detail. The effects of different heat treatments on the transformation of porous NiTi alloy were investigated by differential scanning calorimetry (DSC), x-ray diffraction (XRD), and scanning electron microscopy (SEM). The results indicate that heat treatment had strong influences on the transformation temperatures and latent heats of transformation. When the porous alloy was annealed at 648K and 748K for 3.6ks, two steps transformation including R transformation occurred during cooling and heating and the R transformation temperatures are lower than B 2↔ B 19' transformation temperatures. However, no transformation was detected within the experimental temperature range if the porous alloy was solution treated at 1133K for 2.4ks. This novel phenomenon was the results of extensive Ti2Ni intermetallic compound precipitation. The transformation temperatures of porous NiTi alloy after annealing at 1323K for 3.6ks were much lower than those of the untreated alloy.

scholarly journals Influence of Heat Treatment on Microstructure and Properties of NiTi46 Alloy Consolidated by Spark Plasma Sintering

Materials ◽  
2019 ◽  
Vol 12 (24) ◽  
pp. 4075 ◽  
Author(s):  
Pavel Salvetr ◽  
Jaromír Dlouhý ◽  
Andrea Školáková ◽  
Filip Průša ◽  
Pavel Novák ◽  
...  
Keyword(s):  
Mechanical Properties ◽  
Heat Treatment ◽  
Shape Memory ◽  
Spark Plasma Sintering ◽  
Scanning Calorimetry ◽  
Slow Cooling ◽  
Plasma Sintering ◽  
High Temperature Synthesis ◽  
Heat Treated ◽  
Spark Plasma

Ni-Ti alloys are considered to be very important shape memory alloys with a wide application area including, e.g., biomaterials, actuators, couplings, and components in automotive, aerospace, and robotics industries. In this study, the NiTi46 (wt.%) alloy was prepared by a combination of self-propagating high-temperature synthesis, milling, and spark plasma sintering consolidation at three various temperatures. The compacted samples were subsequently heat-treated at temperatures between 400 °C and 900 °C with the following quenching in water or slow cooling in a closed furnace. The influence of the consolidation temperature and regime of heat treatment on the microstructure, mechanical properties, and temperatures of phase transformation was evaluated. The results demonstrate the brittle behaviour of the samples directly after spark plasma sintering at all temperatures by the compressive test and no transformation temperatures at differential scanning calorimetry curves. The biggest improvement of mechanical properties, which was mainly a ductility enhancement, was achieved by heat treatment at 700 °C. Slow cooling has to be recommended in order to obtain the shape memory properties.

Effect of Heat Treatment Temperature on the Mechanical Property in Cast TiNi Shape Memory Alloy

2007 ◽  
pp. 1493-1496
Author(s):  
Kazuhiro Kitamura ◽  
Yutaka Sawada ◽  
Toshio Kuchida ◽  
Tadashi Inaba ◽  
Masataka Tokuda ◽  
...  
Keyword(s):  
Heat Treatment ◽  
Mechanical Property ◽  
Shape Memory Alloy ◽  
Shape Memory ◽  
Heat Treatment Temperature ◽  
Treatment Temperature

scholarly journals Effect of Heat Treatment Temperature on Martensitic Transformation and Superelasticity of the Ti49Ni51 Shape Memory Alloy

Materials ◽  
2019 ◽  
Vol 12 (16) ◽  
pp. 2539 ◽  
Author(s):  
Peiyou Li ◽  
Yongshan Wang ◽  
Fanying Meng ◽  
Le Cao ◽  
Zhirong He
Keyword(s):  
Heat Treatment ◽  
Martensitic Transformation ◽  
Shape Memory Alloy ◽  
Shape Memory ◽  
Thermal Hysteresis ◽  
Treatment Temperature ◽  
Heat Treated ◽  
Different Temperatures ◽  
Tini Phase ◽  
Rapidly Solidified

The martensitic transformation and superelasticity of Ti49Ni51 shape memory alloy heat-treatment at different temperatures were investigated. The experimental results show that the microstructures of as-cast and heat-treated (723 K) Ni-rich Ti49Ni51 samples prepared by rapidly-solidified technology are composed of B2 TiNi phase, and Ti3Ni4 and Ti2Ni phases; the microstructures of heat-treated Ti49Ni51 samples at 773 and 823 K are composed of B2 TiNi phase, and of B2 TiNi and Ti2Ni phases, respectively. The martensitic transformation of as-cast Ti49Ni51 alloy is three-stage, A→R→M1 and R→M2 transformation during cooling, and two-stage, M→R→A transformation during heating. The transformations of the heat-treated Ti49Ni51 samples at 723 and 823 K are the A↔R↔M/A↔M transformation during cooling/heating, respectively. For the heat-treated alloy at 773 K, the transformations are the A→R/M→R→A during cooling/heating, respectively. For the heat-treated alloy at 773 K, only a small thermal hysteresis is suitable for sensor devices. The stable σmax values of 723 and 773 K heat-treated samples with a large Wd value exhibit high safety in application. The 773 and 823 K heat-treated samples have large stable strain–energy densities, and are a good superelastic alloy. The experimental data obtained provide a valuable reference for the industrial application of rapidly-solidified casting and heat-treated Ti49Ni51 alloy.

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