Effect of Different Solid Amounts in the Physical and Microscopical Properties of SiC Porous Ceramics

2008 ◽  
Vol 591-593 ◽  
pp. 685-690 ◽  
Author(s):  
Jerusa Góes Aragão Santana ◽  
José Luiz Minatti ◽  
Élson de Campos ◽  
Francisco Cristóvão Lourenço de Melo ◽  
Tetunori Kajita

The presence of pores in ceramics is directly related to the chosen forming process. So, in the starch consolidation method, the ceramics show, after burning, pores with morphology similar to that presented by this organic material. On the other hand, the increase in solid load leads up to alterations in dispersion viscosity, increasing the thermal stresses during drying and sintering processes. In order to verify the solid percentage influence in ceramic final properties, samples were prepared with silicon carbide in different compositions using or not starch as binder agent and pore forming element. The characterization of the ceramic pieces was performed by superficial roughness measurements, porosity besides by optical and scanning electron microscopy. The results showed ceramics with SiC and starch presented physical and microscopic properties slightly higher in relation to those with only ceramic powder in their composition. The presence of organic material, agglomerated and foam during the forming were essential for the final properties of the studied samples.

2016 ◽  
Vol 881 ◽  
pp. 52-57
Author(s):  
Rodrigo Sampaio Fernandes ◽  
Elson de Campos ◽  
Jerusa Góes Aragão Santana ◽  
Rogério Pinto Mota

Slip/starch casting consolidation (SSCC) is a technique for obtaining porous ceramics, which joins the forming process by starch consolidation with the slip casting method. In this work, a slip which contains ceramic powders, starch and dispersant, is poured into a porous mold and is taken to an oven so that the gelling process occurs. After sintering, it is noticed that the ceramics show different characteristics from the ones obtained exclusively by slip casting or by starch consolidation. Alumina ceramics were produced by using the three methods presented in this work. The ceramics were characterized by apparent porosity, mechanical resistance and scanning electron microscopy. The ceramics produced by SSCC presented the highest mechanical resistance value (289 MPa), while the ones produced by starch consolidation and slip casting presented values of 126 MPa and 191 MPa, respectively.


Author(s):  
H. M. Kerch ◽  
R. A. Gerhardt

Highly porous ceramics are employed in a variety of engineering applications due to their unique mechanical, optical, and electrical characteristics. In order to achieve proper design and function, information about the pore structure must be obtained. Parameters of importance include pore size, pore volume, and size distribution, as well as pore texture and geometry. A quantitative determination of these features for high porosity materials by a microscopic technique is usually not done because artifacts introduced by either the sample preparation method or the image forming process of the microscope make interpretation difficult.Scanning electron microscopy for both fractured and polished surfaces has been utilized extensively for examining pore structures. However, there is uncertainty in distinguishing between topography and pores for the fractured specimen and sample pullout obscures the true morphology for samples that are polished. In addition, very small pores (nm range) cannot be resolved in the S.E.M. On the other hand, T.E.M. has better resolution but the specimen preparation methods involved such as powder dispersion, ion milling, and chemical etching may incur problems ranging from preferential widening of pores to partial or complete destruction of the pore network.


2021 ◽  
Vol 32 (3) ◽  
pp. 3232-3246
Author(s):  
R. P. Jebin ◽  
T. Suthan ◽  
T. R. Anitha ◽  
N. P. Rajesh ◽  
G. Vinitha

1996 ◽  
Vol 31 (8) ◽  
pp. 1033-1038
Author(s):  
A. C. Yanes ◽  
M. E. Torres ◽  
T. Lopez ◽  
J. Stockel ◽  
J. Peraza

1987 ◽  
Vol 153 (Part_1_2) ◽  
pp. 27-36 ◽  
Author(s):  
H. Rosenberger ◽  
H. Bürger ◽  
H. Schütz ◽  
G. Scheler ◽  
G. Maenz

2013 ◽  
Vol 845 ◽  
pp. 256-260 ◽  
Author(s):  
M. Abubakar ◽  
A.B. Aliyu ◽  
Norhayati Ahmad

Porous ceramics were produced by compaction method of Nigerian clay and cassava starch. The samples were prepared by adding an amount from 5 to 30%wt of cassava starch into the clay and sintered at temperature of 900-1300°C. The influence of cassava starch content on the bulk density and apparent porosity was studied. The result of XRD and DTA/TGA shows that the optimum sintering temperature was found to be 1300°C. The percentage porosity increased from 12.87 to 43.95% while bulk density decreased from 2.16 to 1.46g/cm3 with the increase of cassava starch from 5 to 30%wt. The effect of sintering temperature and cassava starch content improved the microstructure in terms of porosity and the thermal properties of porous clay for various applications which requires a specific porosity.


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