Microstructure and Texture Evolution during Friction Stir Processing of AZ31 Mg Alloy

2010 ◽  
Vol 654-656 ◽  
pp. 1195-1200 ◽  
Author(s):  
Ren Long Xin ◽  
Bo Li ◽  
Qing Liu
Keyword(s):  
Grain Size ◽  
Texture Evolution ◽  
Base Material ◽  
Alloy Sheet ◽  
Electron Back Scatter Diffraction ◽  
Mg Alloy ◽  
Gradual Change ◽  
Friction Stir ◽  
Az31 Mg Alloy ◽  
Average Grain Size

In this study, a well-textured AZ31 Mg alloy sheet was friction stir (FS) processed, and the microstructure and texture evolution in various regions of the processed alloy were examined by optical microscopy (OM) and electron back scatter diffraction (EBSD). The results showed that the grain size in the FS zone was significantly refined compared to that in the base material (BM). The average grain size in the thermomechanically affected zone (TMAZ) and heat-affected zone (HAZ) was comparable with that in the BM. There is a gradual change of local texture from BM to FS zone due to plastic flow together with heating input during the FS processing. The <0002> direction was roughly parallel to the cylindrical pin surface normal of the FS zone. The <0002> direction in the HAZ is similar to that in the BM, but more diffuse. The <0002> direction in the TMAZ was tilted 25~30o away from the ND and there is a distinct boundary between the FS zone and TMAZ at the advancing side which introduced an incompatibility between the FS zone and TMAZ. This might explain the fact that the transverse FS processed Mg alloys commonly fracture at the advancing side during tensile tests.

scholarly journals Evaluation of Cryogenic Mechanical Properties of Resistance Seam-Welded Invar Alloy Sheet by Instrumented Indentation Test

2020 ◽  
Vol 8 (12) ◽  
pp. 1009
Author(s):  
Seunghun Choi ◽  
Jongho Won ◽  
Jung-Jun Lee ◽  
Hee-Keun Lee ◽  
Seong-Min Kim ◽  
...  
Keyword(s):  
Grain Size ◽  
Plastic Zone ◽  
Base Material ◽  
Indentation Test ◽  
Welding Current ◽  
Optical Microscope ◽  
Alloy Sheet ◽  
Invar Alloy ◽  
Instrumented Indentation ◽  
Average Grain Size

Invar alloy sheet was welded by resistance seam welding (RSW) with a constant electrode force and three different welding currents. Tensile properties were evaluated using instrumented indentation testing (IIT) with a spherical indenter and microstructure observations were obtained under an optical microscope. IIT performed on the base material at room temperature (RT) and −163 °C, a cryogenic temperature (CT), gave results in good agreement with those of tensile testing. The strength of each zone was higher in the order of heat-affected zone (HAZ) < weld nugget (WN) < base material (BM) because the amount of cold working was least in the BM, heavy metal elements and carbon vaporized during melting, and the WN was formed more tightly than the HAZ, effectively constraining the plastic zone generated by the indentation. As for the welding current, the nugget, which becomes larger and tighter as the current increases, more effectively constrained the plastic zone in the indentation, and this soon increased the strength. Generally, Invar is known to consist of single-phase austenite, and microstructure observations have confirmed that the average grain size is ordered as BM < HAZ < WN. Fan-like columnar grains developed in the direction of the temperature gradient, and equiaxed grains were observed near the BM. It was confirmed that the grain size in the WN also increases as the current is increased. Interestingly, the constraint effect with increasing nugget size was more important for strength than the grain size.

Fatigue behavior of friction stir spot welded AZ31 Mg alloy sheet joints

2013 ◽  
Vol 23 (7) ◽  
pp. 1949-1956 ◽  
Author(s):  
Tian-jiao LUO ◽  
Bao-liang SHI ◽  
Qi-qiang DUAN ◽  
Jun-wei FU ◽  
Yuan-sheng YANG
Keyword(s):  
Fatigue Behavior ◽  
Alloy Sheet ◽  
Mg Alloy ◽  
Friction Stir ◽  
Az31 Mg Alloy ◽  
Spot Welded

Investigation of Microstructure and Mechanical Properties of Friction Stir Lap Jointed Ni Base Superalloy

2012 ◽  
Vol 724 ◽  
pp. 481-485
Author(s):  
Kuk Hyun Song ◽  
Kazuhiro Nakata
Keyword(s):  
Mechanical Properties ◽  
Grain Size ◽  
Friction Stir Welding ◽  
Base Material ◽  
Lap Joints ◽  
Stir Zone ◽  
Inconel 600 ◽  
Friction Stir ◽  
Microstructure And Mechanical Properties ◽  
Average Grain Size

This study evaluated the microstructure and mechanical properties of friction stir welded lap joints. Inconel 600 and SS 400 as experimental materials were selected, and friction stir welding was carried out at tool rotation speed of 200 rpm and welding speed of 100 mm/min. Applying the friction stir welding was notably effective to reduce the grain size of the stir zone, as a result, the average grain size of Inconel 600 was reduced from 20 μm in the base material to 8.5 μm in the stir zone. Joint interface between Inconel 600 and SS 400 showed a sound weld without voids and cracks. Also, the hook, along the Inconel 600 alloy from SS 400, was formed at advancing side, which directly affected an increase in peel strength. In this study, we systematically discussed the evolution on microstructure and mechanical properties of friction stir lap jointed Inconel 600 and SS 400.

Microstructure based modeling of friction stir welded joint of dissimilar metals using crystal plasticity

2021 ◽  
pp. 1-29
Author(s):  
Shank Kulkarni ◽  
Timothy Truster ◽  
Hrishikesh Das ◽  
Varun Gupta ◽  
Ayoub Soulami ◽  
...  
Keyword(s):  
Fracture Toughness ◽  
Grain Size ◽  
Crystal Plasticity ◽  
Mg Alloy ◽  
Interface Fracture ◽  
Zone Model ◽  
Dissimilar Metals ◽  
Friction Stir ◽  
Az31 Mg Alloy ◽  
Interface Fracture Toughness

Abstract The friction stir welding (FSW) process shows promising results in joining dissimilar metals which are otherwise almost impossible to join using traditional welding techniques. Being a new technique, the deformation and the failure mechanism of the joints made by the FSW process needs to be investigated. In this work, a joint between AZ31 Mg alloy and DP590 steel is modeled using phenomenological crystal plasticity formulation on the mesoscale in the form of a representative volume element (RVE). The interface of the two materials is modeled using a cohesive zone model. A parametric study has been performed to understand the effect of grain size and interface fracture toughness as well as strength on the mechanical performance of the joint. It was found that the grain size of AZ31 Mg alloy, as well as DP590 steel, has little effect on the overall joint performance. On the other hand, interface fracture toughness and strength have a significant impact on the mechanical properties of the joint.

Superplastic Forming Response of a Friction Stir Processed Mg Alloy Sheet – A Numerical Approach

2012 ◽  
Vol 735 ◽  
pp. 192-197 ◽  
Author(s):  
Mohammad Albakri ◽  
Bilal Mansoor ◽  
Ahmad Albakri ◽  
Marwan Khraisheh
Keyword(s):  
Thickness Distribution ◽  
Base Material ◽  
Superplastic Forming ◽  
Numerical Approach ◽  
Processing Technique ◽  
Alloy Sheet ◽  
Mg Alloy ◽  
Dome Height ◽  
Friction Stir ◽  
Forming Characteristics

Friction stir process (FSP) is a severe plastic deformation based secondary processing technique that can be utilized to engineer novel microstructures in metallic alloys. It is well known that such techniques are cumbersome and require significant experimental work and material to determine optimum processing conditions. Therefore in this work, we propose a new two step numerical approach, where: (i) CFD simulations coupled with Zener-Holloman relation are used to predict microstructure evolution in stirred, transition and heat affected zones of friction stir processed AZ31 Mg alloy sheets, (ii) Finite element simulations are carried out to evaluate superplastic forming characteristics of different microstructures developed after FSP. Simulation trends including forming pressure profiles, dome height evolution, and thickness distribution of friction stir processed sheets are compared with those of the base material. The proposed combination of numerical approaches to model both processing and forming aspects yields a powerful tool to study and optimize processing and forming technologies with limited experimentation.

Microstructures and Properties of FSW Joints of AZ31B Mg Alloy

2011 ◽  
Vol 291-294 ◽  
pp. 855-859 ◽  
Author(s):  
Si Rong Yu ◽  
Xian Jun Chen
Keyword(s):  
Mechanical Properties ◽  
Heat Affected Zone ◽  
Welded Joint ◽  
Base Material ◽  
Alloy Sheet ◽  
Weld Nugget ◽  
Mg Alloy ◽  
Material Strength ◽  
Nugget Zone ◽  
Friction Stir

The extruded AZ31B Mg alloy sheet was welded with friction stir welding. The microstructures and mechanical properties of the welded joint were investigated. The results show that the grains in the weld nugget zone were small, uniform and equiaxed. The grains in thermo-mechanical affected zone were stretched and relatively small, but were not as small and uniform as those in the weld nugget zone. The grains in the heat-affected zone were relatively coarse. The fracture of the welded joint occurred mainly in the heat affected zone. The tensile strength of the welded joints was up to 257.4 MPa and was 87.9% of the base material strength. The microhardness in the weld nugget zone was higher. The microhardness in the thermo-mechanical affected zone and heat affected zone were lower than that in the weld nugget zone. The microhardness in the weld nugget zone increased from the upper surface to the bottom.

Enhancement of Formability in Magnesium Alloy AZ31B via Friction Stir Processing

2007 ◽  
Vol 539-543 ◽  
pp. 3775-3780 ◽  
Author(s):  
Yutaka S. Sato ◽  
A. Sasaki ◽  
A. Sugimoto ◽  
A. Honda ◽  
Hiroyuki Kokawa
Keyword(s):  
Grain Size ◽  
Friction Stir Processing ◽  
Base Material ◽  
Mg Alloys ◽  
Stir Zone ◽  
Mg Alloy ◽  
Homogeneous Microstructure ◽  
Friction Stir ◽  
Magnesium Alloy Az31b ◽  
Plane Strain Deformation

Mg alloy has a poor formability at room temperature because of lack of the active slip systems, but the grain refinement improves its ductility. Friction stir processing (FSP) can create homogeneous microstructure consisting of fine grains in Mg alloys, thus it would be expected that FSP enhances the formability of Mg alloys. In this study, multi-pass FSP was applied to Mg alloy AZ31B, and then formability of FSPed alloy was evaluated. Multi-pass FSP produced the fine recrystallized grains in Mg alloy. The stir zone exhibited larger fracture limit major strains than the base material under uniaxial tension and plane strain deformation, and these values increased with decreasing grain size. The stir zone having grain size of 2.9 μm showed the fracture limit major strains which are roughly as same as those of an annealed pure Al. The present study suggests that FSP is an effective method to enhance the formability of Mg alloys.

The Effects of Heat Treatment and Cold Working on the Microstructure of Aluminum Alloys Welded by Friction Stir Welding (FSW) Technique

2011 ◽  
Vol 409 ◽  
pp. 287-292
Author(s):  
M. Mohammadtaheri ◽  
M. Haddad-Sabzevar ◽  
Mohammad Mazinani
Keyword(s):  
Grain Size ◽  
Friction Stir Welding ◽  
Aluminum Alloys ◽  
Cold Work ◽  
Base Material ◽  
Work Conditions ◽  
Weld Nugget ◽  
Hardness Profile ◽  
Friction Stir ◽  
Average Grain Size

The application of hot deformation during Friction Stir Welding (FSW) gives rise to produce a weld nugget consisting usually of dynamically recrystallized grains whose size is substantially lower than that of the base material. In the present study, several specimens with different conditions were first prepared using 2024 and 5083 aluminum alloys, which were then welded with FSW method. The microstructures of weld nugget in both series of specimens were examined using optical and scanning electron microscopes. The specimen of 2024 with anneal (O) and artificial aging (T6) conditions, and type 5083 with anneal (O), 30% and 50% cold work conditions were friction stir welded. Grain size distribution, hardness and temperature profiles in the welded zones were determined in order to obtain the relationship between the grain structure and the hardness profile in these regions. In each alloy, the average grain size in the weld nuggets was identical. The hardness of nugget zones in each alloy was the same due to their similar microstructures. According to the results obtained in this investigation, the initial microstructure showed no considerable effect on final microstructure and hardness of the weld nuggets, which this effect may be attributed to continuous dynamic recrystallization phenomenon.

scholarly journals Effect of Vanadium Reinforcement on the Microstructure and Mechanical Properties of Magnesium Matrix Composites

Crystals ◽  
2021 ◽  
Vol 11 (7) ◽  
pp. 806
Author(s):  
Liqing Sun ◽  
Shuai Sun ◽  
Haiping Zhou ◽  
Hongbin Zhang ◽  
Gang Wang ◽  
...  
Keyword(s):  
Grain Size ◽  
Grain Refinement ◽  
Milling Process ◽  
Mg Alloy ◽  
Matrix Composites ◽  
Magnesium Matrix Composites ◽  
Pinning Effect ◽  
Average Grain Size ◽  
The Matrix ◽  
Hot Press Sintering

In this work, vanadium particles (VP) were utilized as a novel reinforcement of AZ31 magnesium (Mg) alloy. The nanocrystalline (NC) AZ31–VP composites were prepared via mechanical milling (MM) and vacuum hot-press sintering. During the milling process, the presence of VP contributed to the cold welding and fracture mechanism, resulting in the acceleration of the milling process. Additionally, increasing the VP content accelerated the grain refinement of the matrix during the milling process. After milling for 90 h, the average grain size of AZ31-X wt % Vp (X = 5, 7.5, 10) was refined to only about 23 nm, 19 nm and 16 nm, respectively. In the meantime, VP was refined to sub-micron scale and distributed uniformly in the matrix, exhibiting excellent interfacial bonding with the matrix. After the sintering process, the average grain size of AZ31-X wt % VP (X = 5, 7.5, 10) composites still remained at the NC scale, which was mainly caused by the pinning effect of VP. Besides that, the porosity of the sintered composites was no more than 7.8%, indicating a good densification effect. As a result, there was little difference between the theoretical and real density. Compared to as-cast AZ31 Mg alloy, the microhardness of sintered AZ31-X wt % VP (X = 5, 7.5, 10) composites increased by 65%, 87% and 96%, respectively, owing to the strengthening mechanisms of grain refinement strengthening, Orowan strengthening and load-bearing effects.

Friction Stir Welding of Dissimilar Formed Mg Alloys (AZ31/AZ91)

2005 ◽  
Vol 486-487 ◽  
pp. 249-252 ◽  
Author(s):  
Chang Yong Lee ◽  
Won Bae Lee ◽  
Yun Mo Yeon ◽  
Seung Boo Jung
Keyword(s):  
Friction Stir Welding ◽  
Dynamic Recrystallization ◽  
Tensile Test ◽  
Intermetallic Compounds ◽  
Grain Growth ◽  
Weld Zone ◽  
Mg Alloys ◽  
Mg Alloy ◽  
Friction Stir ◽  
Az31 Mg Alloy

Friction stir welding of dissimilar formed Mg alloys(AZ31/AZ91) was successfully carried out at the limited welding conditions. In a sound joint, SZ was mainly consisted of AZ31 Mg alloy which was located the retreating side. Dynamic recrystallization and grain growth occurred and β intermetallic compounds of AZ 91 Mg alloy was not observed in SZ. BM had a higher hardness than that of the weld zone. The fracture location was not weld zone but BM of the AZ91 Mg alloy in tensile test.

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