Engineering Method for Assessing the Residual Life of Machines’ Complex Metal Structures Based on Crack Resistance

2020 ◽  
Vol 992 ◽  
pp. 712-717
Author(s):  
S.B. Budrin ◽  
Yu.N. Gorchakov ◽  
V.V. Ovsyannikov ◽  
N.S. Pogotovkina
Keyword(s):  
Fracture Mechanics ◽  
Crack Resistance ◽  
Critical Size ◽  
Residual Life ◽  
Fatigue Cracks ◽  
High Sensitivity ◽  
Weather Conditions ◽  
Metal Structures ◽  
Complex Metal

The authors present the experience of applying their methodology for calculating the residual life of metal structures of reloading machines by the criterion of the development of fatigue cracks to a critical size. The methodology is based on the well-known calculated dependencies of fracture mechanics, refined and supplemented with elements that take into account the specifics of the operation of transshipment machines in difficult weather conditions. Particular attention was paid to the accuracy of determining the stresses in the metalwork element when performing working operations because of the ever changing of the load acting on the metalwork, depending on the weight of the lifted load and the position of the machine in space. To confirm the high sensitivity to the accuracy of the determination of stresses, the dependence of the influence of the resource element metal with a crack from the amplitude of stress is graphically presented. The methodology for assessing the residual resource has been successfully tested on a number of complex metal.

Determination of the residual life of welded metal structures

1992 ◽  
Vol 28 (3) ◽  
pp. 311-313 ◽  
Author(s):  
V. N. Pustovoi ◽  
A. O. Nemchuk ◽  
N. V. Trikolenko
Keyword(s):  
Residual Life ◽  
Metal Structures

scholarly journals Reliability Estimation of Transport Means Elements Under the Action of Cyclic Loads and Corrosive Environment

2018 ◽  
Vol 15 (4) ◽  
pp. 5793-5802
Author(s):  
P. V. Popovych ◽  
Volodymyr Dzyura ◽  
O. S. Shevchuk
Keyword(s):  
Fracture Mechanics ◽  
Corrosion Fatigue ◽  
Residual Life ◽  
Fatigue Cracks ◽  
Reliability Estimation ◽  
Analytical Models ◽  
Cyclic Loads ◽  
Corrosive Environment ◽  
17G1s Steel ◽  
Kinetics Of

The approach for determining the residual life of the vehicles’ thin-walled metal elements with cracks under the action of cyclic loads and corrosive environment is developed based on the first law of thermodynamics and the fracture mechanics principles. Based on the results of the mathematical description of electrochemical reactions and separate data of fracture mechanics, the equation describing the kinetics of the corrosion-fatigue cracks propagation is deduced. This equation and the initial and final conditions are a mathematical model for determining the residual life of structural elements. The correctness of the developed analytical models is confirmed by the experimental data known in the literature. The performance of this model is demonstrated on the example of determining the residual life of a plate made of 17G1S steel. The plate was diluted by a crack in a 3% NaCl solution and subjected to cyclic loading. An increase in the initial size of corrosion-fatigue cracks is significant to reduce the period of their subcritical growth.

STOCHASTIC CALCULATION OF LIFETIME PREDICTION FOR COMPONENTS IN METAL STRUCTURES DUE TO THE GROWTH OF MICRODEFECTS

2020 ◽  
Vol 4 (97) ◽  
pp. 69-76
Author(s):  
IGOR N. SILVERSTOV
Keyword(s):  
Fatigue Strength ◽  
Fracture Mechanics ◽  
Stochastic Approach ◽  
Fatigue Curve ◽  
Probability Of Failure ◽  
Lifetime Prediction ◽  
Statistical Distributions ◽  
Metal Structures

A stochastic approach has been developed to evaluate fatigue strength using elements of the fracture mechanics. The article presents a method for determining the initial parameters of statistical distributions. It also considers the method for constructing a fatigue curve for a component of any size and configuration with any given probability of failure.

Complex study of the fracture processes in materials and structures

2018 ◽  
Vol 84 (11) ◽  
pp. 46-51 ◽  
Author(s):  
N. A. Makhutov
Keyword(s):  
Fracture Mechanics ◽  
Crack Resistance ◽  
Scientific Basis ◽  
Intensity Factors ◽  
Nonlinear Fracture Mechanics ◽  
Nonlinear Fracture ◽  
Linear Fracture ◽  
Science Technology ◽  
Fracture Processes

The results of comprehensive studies of multifactor processes, mechanisms and criteria for fracture at a variation of the crack-like defect state, loading conditions and mechanical properties of structural materials carried out in the 20th - 21st centuries are presented on the basis of monographic publications and articles published in the journal “Zavodskaya Laboratoriya. Diagnostika Materialov.” Crack resistance of materials and structures has become a key problem of the material science, technology, design, manufacture and service of structures. Fracture mechanics including estimation of the stress-strain and limiting states in a cracks tip formed a scientific basis of the crack resistance analysis Stress intensity factors (linear fracture mechanics) and strain intensity factors (nonlinear fracture mechanics) are accepted as the basic criteria of those states. The basic computational relations for construction of the fracture diagrammes which link the cracks growth with conditions of a static, cyclic, long-term, dynamic loading are presented. Parameters of computational relations are put into correspondence with the features of fracture processes on nano-, micro-, meso- and macrolevels. Prospects of the research and guidelines of further studing crack resistance are discussed.

Atomic absorption determination of Hg (II), Cd (II), and As (III) in natural and waste water after preliminary group preconcentration

2019 ◽  
Vol 85 (2) ◽  
pp. 12-16
Author(s):  
I. V. Saunina ◽  
E. N. Gribanov ◽  
E. R. Oskotskaya
Keyword(s):  
Waste Water ◽  
Atomic Absorption ◽  
High Sensitivity ◽  
Distribution Coefficients ◽  
Neutral Medium ◽  
Atomic Absorption Determination ◽  
Absorption Determination ◽  
Relative Standard ◽  
Preliminary Group

The sorption of Hg (II), Cd (II), and As (III) by natural aluminosilicate is studied. It is shown that the mineral absorbs those toxicants in a rather wide pH range, quantitative extraction of analytes being achieved in a neutral or close to neutral medium (pH values range within 7.0 - 8.0; 6.3 - 7.5; 7.4 - 8.5 for Hg (II), As (III), and Cd (II), respectively). The effect of the time of phase contact on the degree of extraction of elements is shown. The sorption capacity of the mineral in optimal conditions of the medium acidity (0.06 mmol/g for mercury, 0.31 mmol/g for cadmium, and 0.52 mmol/g for arsenic) is determined. The distribution coefficients attain values of aboutnX 103-nX 104. A new combined method for determination of Hg (II), Cd (II), and As (III) in natural and waste water is developed and tested. The method consists in a preliminary group sorption concentration of the analytes by aluminosilicate, desorption of the analytes from the surface of the mineral and their subsequent atomic absorption determination. The correctness of the method is verified in analysis of spiked samples. The method is easy to use and exhibits high sensitivity, reproducibility and accuracy of analyte determination. The relative standard deviation does not exceed 0.13. Economic availability and possibility of using domestic sorption materials are the important advantages of the proposed procedure which can be used in the practice of laboratories monitoring the quality and safety of environmental objects.

Determination of Selected Phthalates in Some Commercial Cosmetic Products by HPLC-UV

2020 ◽  
Vol 23 (10) ◽  
pp. 1010-1022
Author(s):  
Emrah Dural
Keyword(s):  
High Performance ◽  
Phthalate Esters ◽  
High Sensitivity ◽  
Hplc Method ◽  
Cosmetic Products ◽  
Limit Of Quantification ◽  
Nail Polish ◽  
Accuracy And Precision ◽  
Butyl Phthalate

Aim and scope: Due to the serious toxicological risks and their widespread use, quantitative determination of phthalates in cosmetic products have importance for public health. The aim of this study was to develop a validated simple, rapid and reliable high-performance liquid chromatography (HPLC) method for the determination of phthalates which are; dimethyl phthalate (DMP), diethyl phthalate (DEP), benzyl butyl phthalate (BBP), di-n-butyl phthalate (DBP), di(2- ethylhexyl) phthalate (DEHP), in cosmetic products and to investigate these phthalate (PHT) levels in 48 cosmetic products marketing in Sivas, Turkey. Materials and Methods: Separation was achieved by a reverse-phase ACE-5 C18 column (4.6 x 250 mm, 5.0 μm). As the mobile phase, 5 mM KH2PO4 and acetonitrile were used gradiently at 1.5 ml min-1. All PHT esters were detected at 230 nm and the run time was taking 21 minutes. Results: This method showed the high sensitivity value the limit of quantification (LOQ) values for which are below 0.64 μg mL-1 of all phthalates. Method linearity was ≥0.999 (r2). Accuracy and precision values of all phthalates were calculated between (-6.5) and 6.6 (RE%) and ≤6.2 (RSD%), respectively. Average recovery was between 94.8% and 99.6%. Forty-eight samples used for both babies and adults were successfully analyzed by the developed method. Results have shown that, DMP (340.7 μg mL-1 ±323.7), DEP (1852.1 μg mL-1 ± 2192.0), and DBP (691.3 μg mL-1 ± 1378.5) were used highly in nail polish, fragrance and cream products, respectively. Conclusion: Phthalate esters, which are mostly detected in the content of fragrance, cream and nail polish products and our research in general, are DEP (1852.1 μg mL-1 ± 2192.0), DBP (691.3 μg mL-1 ± 1378.5) and DMP (340.7 μg mL-1 ±323.7), respectively. Phthalates were found in the content of all 48 cosmetic products examined, and the most detected phthalates in general average were DEP (581.7 μg mL-1 + 1405.2) with a rate of 79.2%. The unexpectedly high phthalate content in the examined cosmetic products revealed a great risk of these products on human health. The developed method is a simple, sensitive, reliable and economical alternative for the determination of phthalates in the content of cosmetic products, it can be used to identify phthalate esters in different products after some modifications.

scholarly journals Electroanalytical Techniques for the Detection of Selenium as a Biologically and Environmentally Significant Analyte—A Short Review

Molecules ◽  
2021 ◽  
Vol 26 (6) ◽  
pp. 1768
Author(s):  
Miroslav Rievaj ◽  
Eva Culková ◽  
Damiána Šandorová ◽  
Zuzana Lukáčová-Chomisteková ◽  
Renata Bellová ◽  
...  
Keyword(s):  
Oxidative Stress ◽  
Essential Element ◽  
Analytical Techniques ◽  
High Sensitivity ◽  
Stripping Voltammetry ◽  
Short Review ◽  
Electroanalytical Methods ◽  
High Concentrations ◽  
Speed Of Analysis

This short review deals with the properties and significance of the determination of selenium, which is in trace amounts an essential element for animals and humans, but toxic at high concentrations. It may cause oxidative stress in cells, which leads to the chronic disease called selenosis. Several analytical techniques have been developed for its detection, but electroanalytical methods are advantageous due to simple sample preparation, speed of analysis and high sensitivity of measurements, especially in the case of stripping voltammetry very low detection limits even in picomoles per liter can be reached. A variety of working electrodes based on mercury, carbon, silver, platinum and gold materials were applied to the analysis of selenium in various samples. Only selenium in oxidation state + IV is electroactive therefore the most of voltammetric determinations are devoted to it. However, it is possible to detect also other forms of selenium by indirect electrochemistry approach.

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