Resin Bonding of Self-Etch Adhesives to Bovine Dentin Bleached from Pulp Chamber

This study evaluated the microtensile bond strength (μTBS) of 1-step self-etch adhesives (1-SEAs) and 2-step self-etch adhesives (2-SEAs) to pulp chamber dentin immediately after bleaching with 2 types of common bleaching techniques. Pulp chamber dentin of bovine teeth was bleached using 30% hydrogen peroxide (H2O2) solution with quartz-tungsten-halogen light-curing unit (Group 1) and 3.5% H2O2-containing titanium dioxide (TiO2) (Pyrenees®) activated with 405-nm violet diode laser for 15 min (Group 2). Unbleached specimens were placed in distilled water for 15 min and used as controls. After treatment, dentin was bonded with resin composite using 1-SEA or 2-SEA and stored in water at 37°C for 24 h. Each specimen was sectioned and trimmed to an hourglass-shape andμTBS was measured. Fractured specimens were examined under a scanning electron microscope to determine fracture modes. All specimens in Group 1 failed before proper bonding tests. In Group 2, theμTBS of 2-SEA was significantly greater (with no failed specimens) than 1-SEA (where 21 out of 36 failed). These results indicate that 2-SEA is a better adhesive system than 1-SEA on bleached dentin. Our results also demonstrated that application of H2O2significantly decreases bond strength of resin to dentin; however, in the case of nonvital tooth bleaching, Pyrenees® is a better alternative to the conventional 30% H2O2bleaching.

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Influence of adhesive system in bond strength of fiber glass posts to radicular dentin using dual cure resin cement

Brazilian Dental Science ◽

10.14295/bds.2014.v17i1.932 ◽

2014 ◽

Vol 17 (1) ◽

pp. 4 ◽

Cited By ~ 1

Author(s):

Daphne Camara Barcellos ◽

Maria Filomena Rocha Lima Huhtala ◽

Melissa Aline Silva ◽

Ana Paula Martins Gomes ◽

Lucas Teixeira Franco

Keyword(s):

Bond Strength ◽

Glass Fiber ◽

Adhesive System ◽

Single Bond ◽

Pull Out ◽

Fiber Posts ◽

Glass Fiber Posts ◽

Group 2 ◽

Self Etch ◽

Group 1

The purpose of this study was to evaluate the bond strength between root dentin and glass fiber posts cemented with dual cure resinous cement associated with the conventional and self-etching adhesive systems. Twenty-four single-rooted human teeth were selected, and the crowns were removed at the cement enamel junction. The roots received biomechanical preparation and obturation followed by the intraradicular preparation compatible with a drill diameter of the glass fiber posts. The roots were divided into two groups, according to cementation protocol (n-12): Group 1 - etched with 37% phosphoric acid for 30 seconds, total-etch adhesive system Single Bond (3M ESPE) and Enforce resinous cement (Dentsply); Group 2 – self-etch adhesive system One Up Bond F (Tokuyama) and Enforce resinous cement (Dentsply). After the posts cementation, the roots were kept at 370 C for one week, and submitted to pull out test on the universal testing machine Emic to a traction speed of 1 mm/min. Data in MPa were submitted to the statistical t-test (5%). The t-test showed significant differences between the two groups (p=0.003). The average values in MPa (±standard-deviation) were: Group 1: 5.28(±3.25), Group 2: 10.05(±3.78). Enforce associated with the self-etch adhesive system One Up Bond F showed significantly higher bond strength values than Group 1 - Enforce associated with the total-etch adhesive system Single Bond.

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Effect of Multiple Consecutive Applications of One-step Self-etch Adhesive on Microtensile Bond Strength

The Journal of Contemporary Dental Practice ◽

10.5005/jcdp-10-2-67 ◽

2009 ◽

Vol 10 (2) ◽

pp. 67-74 ◽

Cited By ~ 4

Author(s):

Hacer Deniz Arisu ◽

Hüma Ömürlü ◽

Evrim Eligüzeloğlu ◽

Mine Üçtaşli

Keyword(s):

Bond Strength ◽

Adhesive System ◽

Microtensile Bond Strength ◽

One Step ◽

Group 3 ◽

Group 2 ◽

Adhesive Application ◽

Self Etch ◽

Group 1

Abstract Aim The aim of this study was to evaluate the effects of multiple consecutive coatings of a one-step self-etch adhesive system (Clearfil Tri-S Bond) on the microtensile bond strength (MBS) to dentin. Methods and Materials Nine caries-free human lower third molars were sectioned perpendicular to the long axis to expose the mid-coronal dentin. The teeth were separated into three experimental groups (n=3) according to the number of adhesive resin coats applied. In Group 1 one layer of Clearfil Tri-S Bond was applied according to the manufacturer's instructions. In Group 2 and Group 3 the adhesive was applied in two and three layers, respectively. In these two groups the first layer was applied according to the manufacturer's instructions but the second and third layers of adhesive were not light cured after application. After the placement of the composite, the teeth were sectioned to obtain approximately 1 mm2 beams for testing. Eighteen beams were prepared for each group using the ‘non-trimming’ method. The MBS values of all specimens were tested, and fracture modes were then determined using a stereomicroscope. Results The mean MBS values (in MPa) of Group 1 (one coat of the adhesive) was significantly lower (p=0.04) than those of Group 3 (three applied coats of the adhesive). There were no statistically significant differences between Groups 1 and 2 and Groups 2 and 3. Conclusion Within the limitations of this in vitro study the application of multiple coats of a one-step self-etch adhesive may provide an increase in bond strength compared to the application of only one coat of adhesive. Clinical Significance Three consecutive coats of one-step self-etching adhesive application can improve MBS. Citation Arisu HD, Eligüzeloğlu E, Üçtaşli M, Ömürlü H. Effect of Multiple Consecutive Applications of One-step Self-etch Adhesive on Microtensile Bond Strength. J Contemp Dent Pract 2009 March; (10)2:067-074.

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Effect of Storage Temperature on Bond Strength of a Self-Etch Adhesive System to Pulp Chamber Dentin

European Journal of Dentistry ◽

10.1055/s-0039-1697450 ◽

2009 ◽

Vol 03 (04) ◽

pp. 314-317

Author(s):

Nazmiye Donmez ◽

Hale Ari ◽

Sema Belli

Keyword(s):

Bond Strength ◽

Storage Temperature ◽

Adhesive System ◽

Pulp Chamber ◽

Group 4 ◽

Significant Difference ◽

Molar Teeth ◽

Group 3 ◽

Group 2 ◽

Self Etch

ABSTRACTObjectives: The aim of this study was to evaluate the effect of storage temperature on bond strength of a self etching primer system to pulp chamber dentin.Methods: SE Bond (Kuraray, JAPAN) adhesive system and Clearfil Photo Posterior (Kuraray, JAPAN) composite resin were used. Eight extracted caries-free human molar teeth were used. Access cavities were prepared through the pulp chamber, randomly distributed into 4 groups and prepared as follows: Group 1 (Control): SE Primer and SE Bond (SEB) were applied to the pulp chamber dentin according to the manufacturer’s instructions, immediately after the delivery from the manufacturer and then the pulp chamber was restored with a resin restorative material. The primer agent of the following groups was stored in a refrigerator and kept at 4�C. Group 2: restored with SEB, kept at 4°C refrigerator for 1 year, Group 3: restored with SEB kept at 23°C room temperature for 1 year and Group 4: restored with SEB kept at 40°C incubator for 1 year. After 24 hrs the teeth were trimmed for microtensile bond testing and loaded to failure at 1mm/min. Data were analyzed using one-way ANOVA and Duncan test (P<.05).Results: The results indicated that Group 4 showed lowest bond strength when compared to the others (P<.05). No statistically significant difference was found among the other groups (P>.05).Conclusions: As a result of this study, it was concluded that increasing storing temperature or storing period decreases microtensile bond strength of a SEB system to pulp chamber dentin. (Eur J Dent 2009;3:314-317)

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The Effects of Prophylactic Ozone Pretreatment of Enamel on Shear Bond Strength of Orthodontic Brackets Bonded with Total or Self-Etch Adhesive Systems

European Journal of Dentistry ◽

10.1055/s-0039-1697855 ◽

2010 ◽

Vol 04 (04) ◽

pp. 367-373 ◽

Cited By ~ 6

Author(s):

Sevi Burcak Cehreli ◽

Asli Guzey ◽

Neslihan Arhun ◽

Alev Cetinsahin ◽

Bahtiyar Unver

Keyword(s):

Bond Strength ◽

Shear Bond Strength ◽

Orthophosphoric Acid ◽

Ozone Treatment ◽

Bond Failure ◽

Group 4 ◽

Group 3 ◽

Group 2 ◽

Self Etch ◽

Group 1

Objectives: The aim of this in vitro study is to determine (1) shear bond strength (SBS) of brackets bonded with self-etch and total-etch adhesive after ozone treatment (2) bond failure interface using a modified Adhesive Remnant Index (ARI).Methods: 52 premolars were randomly assigned into four groups (n=13) and received the following treatments: Group 1: 30 s Ozone (Biozonix, Ozonytron, Vehos Medikal, Ankara, Turkey) application + Transbond Plus Self-Etching Primer (SEP) (3M) + Transbond XT (3M), Group 2: Transbond Plus SEP + Transbond XT, Group 3: 30 s Ozone application + 37% orthophosphoric acid + Transbond XT Primer (3M) + Transbond XT, Group 4: 37% orthophosphoric acid + Transbond XT Primer + Transbond XT. All samples were stored in deionised water at 37oC for 24 hours. Shear debonding test was performed by applying a vertical force to the base of the bracket at a cross-head speed of 1 mm/min.Results: The mean SBS results were Group 1: 10.48 MPa; Group 2: 8.89 MPa; Group 3: 9.41 MPa; Group 4: 9.82 MPa. One-Way Variance Test revealed that the difference between the groups was not statistically significant (P=0.267). Debonded brackets were examined by an optical microscope at X16 magnification to determine the bond failure interface using a modified ARI. The results were (mean) Group 1: 2.38; Group 2: 1.31; Group 3: 3.00; Group 4: 1.92. Multiple comparisons showed that Groups 1 and 2, 2 and 3, 3 and 4 were statistically different (P=0.014, P<.001 and P=0.025).Conclusions: Ozone treatment prior to bracket bonding does not affect the shear bond strength. (Eur J Dent 2010;4:367-373)

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The Effect of SnCl2/AmF Pretreatment on Short- and Long-Term Bond Strength to Eroded Dentin

BioMed Research International ◽

10.1155/2018/3895356 ◽

2018 ◽

Vol 2018 ◽

pp. 1-8 ◽

Cited By ~ 1

Author(s):

Katrin Zumstein ◽

Anne Peutzfeldt ◽

Adrian Lussi ◽

Simon Flury

Keyword(s):

Bond Strength ◽

Failure Mode ◽

Resin Composite ◽

Adhesive System ◽

Adhesive Systems ◽

Short And Long Term ◽

One Year ◽

And Storage ◽

Self Etch

This study investigated the effect of SnCl2/AmF pretreatment on short- and long-term bond strength of resin composite to eroded dentin mediated by two self-etch, MDP-containing adhesive systems. 184 dentin specimens were produced from extracted human molars. Half the specimens (n=92) were artificially eroded, and half were left untreated. For both substrates, half the specimens were pretreated with SnCl2/AmF, and half were left untreated. The specimens were treated with Clearfil SE Bond or Scotchbond Universal prior to application of resin composite. Microtensile bond strength (μTBS) was measured after 24 h or 1 year. Failure mode was detected and EDX was performed. μTBS results were statistically analyzed (α=0.05). μTBS was significantly influenced by the dentin substrate (eroded < noneroded dentin) and storage time (24 h > 1 year; p<0.0001) but not by pretreatment with SnCl2/AmF or adhesive system. The predominant failure mode was adhesive failure at the dentin-adhesive interface. The content of Sn was generally below detection limit. Pretreatment with SnCl2/AmF did not influence short- and long-term bond strength to eroded dentin. Bond strength was reduced after storage for one year, was lower to eroded dentin than to noneroded dentin, and was similar for the two adhesive systems.

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Effect of Non-Thermal Argon Plasma on Bond Strength of a Self-Etch Adhesive System to NaOCl-Treated Dentin

Brazilian Dental Journal ◽

10.1590/0103-6440201600914 ◽

2016 ◽

Vol 27 (4) ◽

pp. 446-451 ◽

Cited By ~ 2

Author(s):

João Luiz Bittencourt de Abreu ◽

Maíra Prado ◽

Renata Antoun Simão ◽

Eduardo Moreira da Silva ◽

Katia Regina Hostilio Cervantes Dias

Keyword(s):

Bond Strength ◽

Plasma Treatment ◽

Ftir Spectroscopy ◽

Resin Composite ◽

Argon Plasma ◽

Adhesive System ◽

Strength Test ◽

Chemical Modifications ◽

Microtensile Bond Strength ◽

Self Etch

Abstract Studies have been showing a decrease of bond strength in dentin treated with sodium hypochlorite (NaOCl). The aim of this study was to evaluate the effect of non-thermal argon plasma on the bond strength of a self-etch adhesive system to dentin exposed to NaOCl. Thirty-two flat dentin surfaces of bovine incisors were immersed in 2.5% NaOCl for 30 min to simulate the irrigation step during endodontic treatment. The specimens were divided into four groups (n=8), according to the surface treatment: Control (without plasma treatment), AR15 (argon plasma for 15 s), AR30 (argon plasma for 30 s) and AR45 (argon plasma for 45 s). For microtensile bond strength test, 5 specimens were used per group. In each group, the specimens were hybridized with a self-etch adhesive system (Clearfil SE Bond) and resin composite buildups were constructed. After 48 h of water storage, specimens were sectioned into sticks (5 per tooth, 25 per group) and subjected to microtensile bond strength test (μTBS) until failure, evaluating failure mode. Three specimens per group were analyzed under FTIR spectroscopy to verify the chemical modifications produced in dentin. μTBS data were analyzed using ANOVA and Tamhane tests (p<0.05). AR30 showed the highest μTBS (20.86±9.0). AR15 (13.81±6.4) and AR45 (11.51±6.8) were statistically similar to control (13.67±8.1). FTIR spectroscopy showed that argon plasma treatment produced chemical modifications in dentin. In conclusion, non-thermal argon plasma treatment for 30 s produced chemical changes in dentin and improved the μTBs of Clearfil SE Bond to NaOCl-treated dentin.

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Aplikasi klorheksidin glukonat 2%pada dentin tidak mempengaruhi kuat rekat geserkomposit resinyangmenggunakansistem adesif self etch (2% Chlorhexidine gluconate application on dentine does not affect bond strength of resin composite using self etch adhesive system)

Journal of Dentomaxillofacial Science ◽

10.15562/jdmfs.v13i1.379 ◽

2014 ◽

Vol 13 (1) ◽

pp. 7

Author(s):

Dewi Puspitasari ◽

Andi Soufyan ◽

Ellyza Herda

Keyword(s):

Bond Strength ◽

Shear Bond Strength ◽

Composite Resin ◽

Resin Composite ◽

Testing Machine ◽

Adhesive System ◽

Chlorhexidine Gluconate ◽

Adhesive Systems ◽

Group I ◽

Self Etch

Composite resin is a widely used aesthetic restoration. The restoration can fail due to secondary caries. Chlorhexidinegluconate 2% is used as a cavity disinfectant to eliminate microorganisms on the prepared cavity and to prevent thesecondary caries. The purpose of this study was to analyze the effect of chlorhexidine gluconate 2% to the bondstrength of composite resin with self etch system adhesive on dentine. Sixteen specimens of buccal dentine of premolarscrown are divided into 2 different groups. Group I: Clearfil SE Bond self-etch primer was applied for 20 seconds,Clearfil SE Bond bonding was applied for 5 seconds and polymerized for 10 seconds. Composite resin was constructedincrementally and polymerized for 20 seconds. Group II: prior to self etch primer application as in group I,chlorhexidine gluconate 2% was applied for 15 seconds. Shear bond strength was tested using Testing machine andanalyzed with unpaired T test. The highest shear bond strength was obtained by applying chlorhexidine gluconate 2%.The study concludes that chlorhexidine gluconate 2% application to dentine did not affect significantly to the bondstrength composite resin using self etch adhesive systems.

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An Evaluation of Shear Bond Strength of Self-Etch Adhesive on Pre-etched Enamel: An in vitro Study

The Journal of Contemporary Dental Practice ◽

10.5005/jp-journals-10024-1446 ◽

2013 ◽

Vol 14 (6) ◽

pp. 1036-1038

Author(s):

Abdul Mujeeb ◽

Bhadra Rao ◽

Satti Narayana Reddy ◽

Kanchan Mehta ◽

G Saritha

Keyword(s):

Statistical Analysis ◽

Bond Strength ◽

Shear Bond Strength ◽

Occlusal Surfaces ◽

Group 3 ◽

The Mean ◽

Group 2 ◽

Self Etch ◽

Group 1

ABSTRACT Aim To determine the shear bond strength of self-etch adhesive G-bond on pre-etched enamel. Materials and methods Thirty caries free human mandibular premolars extracted for orthodontic purpose were used for the study. Occlusal surfaces of all the teeth were flattened with diamond bur and a silicon carbide paper was used for surface smoothening. The thirty samples were randomly grouped into three groups. Three different etch systems were used for the composite build up: group 1 (G-bond self-etch adhesive system), group 2 (G-bond) and group 3 (Adper single bond). Light cured was applied for 10 seconds with a LED unit for composite buildup on the occlusal surface of each tooth with 8 millimeters (mm) in diameter and 3 mm in thickness. The specimens in each group were tested in shear mode using a knife-edge testing apparatus in a universal testing machine across head speed of 1 mm/ minute. Shear bond strength values in Mpa were calculated from the peak load at failure divided by the specimen surface area. The mean shear bond strength of all the groups were calculated and statistical analysis was carried out using one-way Analysis of Variance (ANOVA). Results The mean bond strength of group 1 is 15.5 Mpa, group 2 is 19.5 Mpa and group 3 is 20.1 Mpa. Statistical analysis was carried out between the groups using one-way ANOVA. Group 1 showed statistically significant lower bond strength when compared to groups 2 and 3. No statistical significant difference between groups 2 and 3 (p < 0.05). Conclusion Self-etch adhesive G-bond showed increase in shear bond strength on pre-etched enamel. How to cite this article Rao B, Reddy SN, Mujeeb A, Mehta K, Saritha G. An Evaluation of Shear Bond Strength of Self-Etch Adhesive on Pre-etched Enamel: An In vitro Study. J Contemp Dent Pract 2013;14(6):1036-1038.

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Effect of Prior etching on Bond Strength of Self-Etch adhesive in case of Sensitive Teeth treated with CPP-ACP.

Dental Journal of Advance Studies ◽

10.1055/s-0038-1670585 ◽

2013 ◽

Vol 01 (01) ◽

pp. 009-014

Author(s):

Suruchi Chaudhary Tayal ◽

Jaidev Dhillon ◽

Abhishek Tayal

Keyword(s):

Phosphoric Acid ◽

Bond Strength ◽

Testing Machine ◽

Sensitive Teeth ◽

Permanent Molars ◽

Group 2 ◽

Tooth Mousse ◽

Dentinal Hypersensitivity ◽

Self Etch ◽

Group 1

Abstract Introduction: The management of dentinal hypersensitivity involves remineralization by various means, one of which being CPP-ACP paste, followed by restoration. It was speculated that the bond strength of self-etching adhesive was affected following the application of CPP-ACP paste and prior etching with phosphoric acid. Aims and objectives: To evaluate the tensile bond strength (TBS) of G-Bond (GB, self-etching adhesive) to dentin following the application of CPP-ACP (Tooth Mousse/TM), with and without prior etching. Materials and method: Freshly extracted forty five permanent molars were collected for the study. All the teeth were ground and polished to expose the flat dentinal surface. The teeth were embedded in the resin in separate molds and were divided into three equal groups of fifteen samples each Group 1: Samples treated with Tooth Mousse for 60 min daily for 7 days and then restored with GB and composite (Filtek Z350, 3M ESPE). Group 2: Samples treated with Tooth Mousse and etched with phosphoric acid prior to restoration with GB and composite. Group3: Samples restored with GB and composite. A split brass mold was placed over the predesigned location and with help of the plasma coated instrument, composite resin was placed. Tensile loading was done using Universal Testing Machine. Conclusion: TBS of GB was not significantly reduced after CPP-ACP application, but after prior etching the CPP-ACP specimens, the bond strength of GB was significantly reduced.

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Shear Bond Strengths of Different Adhesive Systems to Biodentine

The Scientific World JOURNAL ◽

10.1155/2013/626103 ◽

2013 ◽

Vol 2013 ◽

pp. 1-5 ◽

Cited By ~ 23

Author(s):

Mesut Enes Odabaş ◽

Mehmet Bani ◽

Resmiye Ebru Tirali

Keyword(s):

Shear Bond Strength ◽

Composite Resin ◽

Adhesive System ◽

Adhesive Systems ◽

Time Intervals ◽

Etch And Rinse ◽

Bond Strengths ◽

Group 2 ◽

Self Etch ◽

Group 1

The aim of this study was to measure the shear bond strength of different adhesive systems to Biodentine with different time intervals. Eighty specimens of Biodentine were prepared and divided into 8 groups. After 12 minutes, 40 samples were randomly selected and divided into 4 groups of 10 each: group 1: (etch-and-rinse adhesive system) Prime & Bond NT; group 2: (2-step self-etch adhesive system) Clearfil SE Bond; group 3: (1-step self-etch adhesive systems) Clearfil S3Bond; group 4: control (no adhesive). After the application of adhesive systems, composite resin was applied over Biodentine. This procedure was repeated 24 hours after mixing additional 40 samples, respectively. Shear bond strengths were measured using a universal testing machine, and the data were subjected to 1-way analysis of variance and Scheffé post hoc test. No significant differences were found between all of the adhesive groups at the same time intervals (12 minutes and 24 hours) (). Among the two time intervals, the lowest value was obtained for group 1 (etch-and-rinse adhesive) at a 12-minute period, and the highest was obtained for group 2 (two-step self-etch adhesive) at a 24-hour period. The placement of composite resin used with self-etch adhesive systems over Biodentine showed better shear bond strength.

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