particle size measurement
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2022 ◽  
Vol 72 (4) ◽  
pp. e431
Author(s):  
A.E. Edris

Different emulsifiable concentrates containing spearmint essential oil (SEO) were made and evaluated for their potential for giving ethanol-free nanoemulsion spontaneously upon dilution into water. Each one of these formulas had its specific composition regarding the type of excipients, surfactants, surfactant/SEO ratio and surfactant concentration. The results of this evaluation indicated that the chemical composition of SEO has a profound effect on the formation and physical stability of the nanoemulsion. The incorporation of excipients such as long chain triglyceride and propylene glycol into the emulsifiable concentrates at only 1.0% can lead to a stable nanoemulsion that resists Ostwald ripening. A particle size measurement showed that the diameter of SEO in the nanoemulsion was 28.2 nm and its nanostructure was maintained for 3 months. The application of a mixture of binary nonionic food-permitted surfactants enhanced the thermal stability of the nanoemulsion at up to 50 ᵒC. The developed ethanol-free SEO nanoemulsion has promising industrial applications in food and beverage flavoring.


Author(s):  
Farnam Razzaghi-Koolaee ◽  
Ghasem Zargar ◽  
Bahram Soltani Soulgani ◽  
Parviz Mehrabianfar

AbstractFormation damage is a general term, which refers to any process that reduces the production or injectivity of an oil well. Clay swelling formation damage, due to incompatible fluid invasion, is a common problem in the petroleum industry. In this research, the effect of Acanthophyllum root extract (ACRE), a bio-based surfactant, on the reduction in reservoir permeability impairment has been studied. Some static tests were applied to investigate the chemical interaction between the surfactant and montmorillonite (Mt), including Mt sedimentation test, Free swelling index (FSI) test, Zeta potential tests, particle size measurement, and scanning electron microscopy (SEM). Experiments were followed by coreflood and micromodel tests to verify their effect on preventing permeability reduction and pore plugging in porous media. According to the results, Mt dispersion is unstable in the presence of ACRE solution. ACRE can reduce the FSI from 233.3 (totally hydrated Mt) to 94.3%, representing the reduction in hydration potential. The zeta potential of Mt in ACRE aqueous solution moves toward the lowest magnitude, implying that the water molecules surrounding the Mt particles are unstable. Particle size measurement and SEM analysis proved simultaneously that ACRE solution sustains Mt particles flocculated and prevents delamination. The thermal stability of the ACRE was evaluated by thermogravimetric analysis (TGA), and it showed a suitable resistance to the temperature rise. Eventually, coreflood and micromodel tests revealed that ACRE has a high performance in lowering the permeability impairment and pore plugging. All in all, ACRE showed high potential in preventing Mt swelling and, therefore, formation damage in clay-bearing sandstones.


Author(s):  
Muhammad Imran Rashid

In education pedagogy, its necessary to prioritize tasks and jobs. Learn operating the reactor or required apparatus but most important first. Regarding measuring techniques (PSD measurement, pH measurement, XRD, SEM/EDS), learn more basic and fundamental techniques first followed by complimentary techniques. Regarding mineral carbonation, operation of reactor is a basic need followed by particle size measurement using Malvern Mastersizer and powders samples XRD analysis and identifying the phases and verifying those phases through TGA analysis. This article illustrates author personal research of 4 initial 4 months duration. Month wise progress is presented in this article in an interesting way.


Materials ◽  
2021 ◽  
Vol 14 (19) ◽  
pp. 5683
Author(s):  
Mengjie Wang ◽  
Jin Shen ◽  
John C. Thomas ◽  
Tongtong Mu ◽  
Wei Liu ◽  
...  

Dynamic light scattering (DLS) is a popular method of particle size measurement, but at ultra-low particle concentrations, the occurrence of number concentration fluctuations limits the use of the technique. Number fluctuations add a non-Gaussian term to the scattered light intensity autocorrelation function (ACF). This leads to an inaccurate particle size distribution (PSD) being recovered if the normal DLS analysis model is used. We propose two methods for inverting the DLS data and recovering the PSDs when number fluctuations are apparent. One is to directly establish the relationship between the non-Gaussian ACF and the PSD by the kernel function reconstruction (KFR) method while including the non-Gaussian term to recover the PSD. The other is to remove the effect of the non-Gaussian term in the ACF by the baseline reset (BR) method. By including the number fluctuation term, the ideal recovered PSD can be obtained from the simulated data, but this will not happen in the experimental measurement data. This is because the measured intensity ACF contains more noise than the simulated ACF at ultra-low concentration. In particular, the baseline noise at the tail of long delay time of ACF overwhelms the number fluctuation term, making it difficult to recover reliable PSD data. Resetting the baseline can effectively remove the digital fluctuation term in ACF, which is also a feasible method to improve PSD recovery under ultra-low concentration. However, increasing noise at ultra-low concentrations can lead to errors in determining an effective baseline. This greatly reduces the accuracy of inversion results. Results from simulated and measured ACF data show that, for both methods, noise on the ACF limits reliable PSD recovery.


Author(s):  
Jeong Wan Kim ◽  
Mun Ki Bae ◽  
Yeong Min Park ◽  
Byung Kwan Song ◽  
Tae Gyu Kim

In general, MgF2, which is a low-reflective coating material, has a refractive index of 1.38. The refractive index of a single layer of MgF2 is not sufficient for industrial applications. In this study, an anti-reflection MgF2 coating film with low reflectivity and high wear resistance was synthesized to be used as a single layer with a TEOS binder. The prepared anti-reflection coating film was coated in the form of nanoparticles on a curvature lens having an aspherical surface coefficient by spin coating, and the correlation with optical properties was confirmed through particle size measurement. The MgF2 nanoparticle AR coating film was characterized by LDPSA, UV-Vis, SEM and ellipsometry. Mechanical and optical properties were confirmed with a minimum reflectance of 0.1% or less and a low refractive index of 1.24–1.25.


2021 ◽  
Author(s):  
Zhihai Liu ◽  
Lu Wang ◽  
Yu Zhang ◽  
Yaxun Zhang ◽  
Xiaoyun Tang ◽  
...  

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