Microstructure Influenced by Controlled Rolling, Cooling and Thermal Processing of Seamless Tubes Made of Steel 25CrMo4

By use of physical simulations, it was studied the influence of finish rolling temperature (from 820 °C to 970 °C) on the microstructural and mechanical properties of seamless tubes with a different wall thickness (from 6.3 to 40 mm) – in the state after rolling as well as after quenching and tempering. In laboratory conditions, by use of the Simulator HDS-20, the bloom piercing and rolling of the seamless tubes from 25CrMo4 low-alloy steel in a pilger mill were in a simplified way simulated. The wall thickness of the tube influenced the total deformation of specimens at anisothermal multi-pass plain-strain compression tests as well as the final cooling rate. The quenching and tempering of the deformed specimens was subsequently performed with use of the electric resistance furnaces. The finish rolling temperature had only insignificant effect on the resulting properties. Markedly lower hardness was obtained only after the simulation of tube production with the wall thickness of 40 mm contrary to the wall thickness of 6.3 and 20 mm. Structural variations of the specimens after rolling simulations were more or less overlapped by the subsequent quenching from the temperature of 850 °C and tempering at the temperature of 680 °C.

Estimation of Impact Toughness Transition Temperatures of As-Quenched Steels

High strength and sufficient toughness are key requirements for modern high-performance structural steels. In an attempt to develop a suitable estimation of impact toughness transition temperatures for as-quenched steels, we investigated the determiners of low-temperature toughness with a group of thermomechanically rolled direct-quenched steels with varying martensite contents. These were produced by altering chemical composition, finish rolling temperature and reduction below the non-recrystallization temperature, i.e. austenite pancaking, and characterised in terms of microstructural constituents, grain size distributions, texture and fractography. Provided the finish rolling temperature is high enough to avoid the formation of granular bainite on subsequent cooling, high levels of austenite pancaking yield the best combinations of low-temperature toughness and strength by effectively refining the size of the coarsest grains and randomizing the texture. While absolutely no direct correlation is found within as-quenched steels between the impact toughness transition temperatures and yield strength alone, T28J and T50 do closely follow a dynamic reference toughness, i.e. the opening stress intensity factor defined by yield strength and the size of the coarsest grains in the effective grain size distribution. This parameter reflects the transition temperatures – the lower the temperature, the lower the reference toughness needed to cause a local brittle fracture. Finally, we show that the impact toughness transition temperatures T28J and T50 of as-quenched steels can be accurately estimated, irrespective of the test specimen orientation, by utilizing just the dynamic reference toughness and the fraction of {100} cleavage planes within ± 15° of the specimen notch plane.