Karaktristik proses destilasi asap cair grade 3

Distillation of liquid smoke is a process of heating liquid smoke based on the difference in its boiling point and then cooled to get liquid smoke with better quality. This heating aims to separate unwanted components in liquid smoke such as tar and benzopyrene. The process is strongly influenced by several things such as temperature and distillator. From these two measurements, several characteristics such as heating rate, distillation flow rate of liquid smoke, production capacity, heating temperature, steam temperature and distillation time, as well as the characteristics of the resulting liquid smoke can be known.The purpose of this study is to determine the characteristics of the 3rd grade liquid smoke distillation process with electric heating and water cooling condenser which includes the production capacity of liquid smoke and to determine the quality and quantity of liquid smoke, heating rate, electricity consumption, flow rate and to determine the efficiency of 2nd grade liquid smoke production.This research was conducted at the Laboratorium Teknik Mesin Universitas Muhammadiyah Metro, this study used a distillation apparatus made of Aluminium plate 1 mm thick, 180 mm in diameter, 250 mm high. Condenser with 0.5 inch diameter copper pipe 3,5 m long, 3 inch diameter PVC pipe, 3m long. The raw material for 3rd grade liquid smoke is 3 liters.The results obtained that the distillation apparatus has a capacity of 3 liters, the distillation temperature affects the rate of heating that occurs, namely the distillation temperature of 110oC, the heating rate is 707,42 J/second, the electricity consumption is 4,48kWh, the time is 45 minutes, and for a temperature of 120 oC the heating rate is 754,60 J/second, electricity consumption is 4,467 kWh in 65 minutes. The highest yield of liquid smoke is at a temperature of 110 oC, which is 2840 ml with a flow rate of 8,35 ml/minute and an efficiency of 94,6%, pH level of 2,15. And for a temperature of 120 oC it produces 2560 ml of liquid smoke, with a flow rate of 8,67 ml/minute and an efficiency of 85,3%, with a pH level of 2,10.

Vacuum Gasification-Directional Condensation for Separation of Tellurium from Lead Anode Slime

Tellurium is the indispensable base material of semiconductors in solar panels. Traditional tellurium recycling, a highly complicated separation process, has exhausted reagents and energy sources whilst producing waste residue and water containing multitudinous heavy metal that is hugely harmful to the ecological environment. A clean and eco-friendly vacuum distillation-directional condensation treatment was investigated for its potential to recycle tellurium from tellurium-rich lead anode slime (TLAS). The optimal distillation temperature and response time conditions of 1173 K and 50 min were obtained based on a large number of experiments. Gasification results indicated that under the optimal conditions of distillation temperature 1173 K, constant temperature time 50 min, and system pressure 5–15 Pa, 92% of tellurium was volatilized and enriched into the condenser from TLAS. Condensate results revealed that 88% of elemental tellurium was directly recovered in the volatile matter. The appropriate gasification-condensation processes realized a clean utilization to extract tellurium and separate multi valuable metals effectively.

Model Petri Net untuk Otomatisasi Destilasi Bioethanol

<p><em>Abstrak <strong>– </strong></em><strong>Petri net adalah satu di antara yang digunakan untuk pemodelan sistem otomatis. Tulisan ini melaporkan penggunaan model petri net pada purwarupa alat destilasi etanol otomatis, menggunakan PLC sebagai pengendali utama. Model proses mencakup perangkat keras dan lunak. Sistem pengaturan yang dimodelkan bertujuan menjaga agar suhu dalam wadah pemanas berada dalam kisaran titik didih etanol yaitu 80 ºC, serta pengamanan perangkat terutama terkait elemen pemanas. Pemodelan sistem pengaturan dikembangkan menggunakan petri net bebas, untuk implementasi pada PLC. Implementasi menghasilkan perangkat yang secara konsisten melakukan destilasi secara otomatis, dan menghasilkan cairan dengan kadar etanol 80% dari cairan awal berkadar 40%.</strong></p><p><strong> </strong></p><p><strong><em>Kata kunci</em></strong><em> – Petri net, PLC, destilasi, pengaturan suhu, pemanas</em><em></em></p><p><em>Abstract </em><strong>– Petri net is on of models commonly used for automation and manufacture. This paper reports the use of petri net in modeling automated distillation process of ethanol, using PLC as main controller. The model encompassed hardware and software parts of the prototype built. The control system was aimed to keep the system at ethanol’s boiling point of 80ºC, while maintaining the hardware’s safety especially the heater. Free style petri net was used, then implemented on PLC. The resulting prototype has performed consistent performance of automatic distillation, producing 80% ethanol out of 40% ethanol.</strong></p><p><strong><em>Keyword</em></strong><strong> </strong>– <em>Petri net, PLC, distillation, temperature control, heater</em></p>

Influence of Distillation Temperature in the Determination of Added Sulfites in Dehydrated Garlic Powders Using the Modified Optimized Monier-Williams Method

Influence of distillation temperature on the determination of added sulfites in dehydrated garlic originating from China and California using the modified optimized Monier-Williams method was evaluated. In the study, the temperature of the distillation was monitored and maintained from 90° to 95°C instead of boiling temperature (&gt;95°C). Samples from 38 unsulfited dehydrated garlic powders were analyzed at the 90° to 95°C temperature and at boiling temperature (&gt;95°C) at 94 m above sea level. At the boiling distillation temperature, 25 of the 38 unsulfited garlic samples had a positive result for sulfite content ranging from 10.2 to 14.1 ppm using the modified optimized Monier-Williams procedure. Maintaining distillation temperature between 90° and 95°C eliminated false-positive results for added sulfite and had an average spiked sulfite recovery of 95.6% with a coefficient of variation of 3.79%. Lowering of the distillation temperature decreases the possible acid hydrolysis of organosulfur compounds that can lead to positive added sulfite results in unsulfited dehydrated garlic samples.

Current Status of Comprehensive Use and Management Recommendations of Coal Tar in China

Based on dry distillation temperature and properties, coal tar can be divided into high temperature coal tar and medium & low temperature coal tar. This paper introduces current status of generation and comprehensive use of high temperature coal tar and medium & low temperature coal tar in China, analyzes poor practice and management problems in the process of comprehensive use of coal tar, and puts forward countermeasures and recommendations for comprehensive use of coal tar in China.

RANCANGAN ALAT PEMBUATAN BIOETANOL DARI BAHAN BAKU KULIT DURIAN

In this research, the bioethanol production unit using durian peel as raw material was designed with capacity process of 100 liters per cycle in batch process. The main equipments were designed fermenter and distillation unit. Fermenter tank was designed with 43 cm of diameter and 86 cm of height which was equipped with two manual paddle impeller of 30 cm in diameter. The other of main equipments, distillation tank was made of stainless steel with 48 cm of diameter and 54 cm of height, which was equipped with heater to heat the liquid of fermentation process and cooling tank to cool vaporised bioethanol. The time required for one cycle of fermentation with batch process was 7 days and 7 hours. While the time required for one cycle of bioethanol production with batch process was 8 days and 4 hours. The feasibility of bioethanol production unit in which consists of fermenter tank and distillation tank under condition process of 7 days and yeast concentration of 6% and distillation temperature of 80oC was tested. The results obtained were 8,98% of bioethanol concentration during fermentation and 74,96% of bioethanol concentration during distillation.