crystal size distribution
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Gels ◽  
2022 ◽  
Vol 8 (1) ◽  
pp. 39
Author(s):  
Varuzhan Sarkisyan ◽  
Roman Sobolev ◽  
Yuliya Frolova ◽  
Irina Vorobiova ◽  
Alla Kochetkova

Beeswax and beeswax hydrocarbon-based oleogels were studied to evaluate the quantitative relationship between their yield strength and crystal size distribution. With this aim, oleogels were prepared using four different cooling regimes to obtain different crystal size distributions. The microstructure was evaluated by polarized light microscopy. The yield strength is measured by the cone penetration test. Oleogels were characterized by average grain size, microstructure entropy, grain boundary energy per unit volume, and microstructure temperature. We have provided the theoretical basis for interpreting the microstructure and evaluating the microstructure-based hardening of oleogels. It is shown that the microstructure entropy might be used to predict the yield strength of oleogels by the Hall-Petch relationship.


CrystEngComm ◽  
2021 ◽  
Author(s):  
David Acevedo ◽  
Wei-Lee Wu ◽  
Xiaochuan Yang ◽  
Naresh Pavurala ◽  
Adil Mohammad ◽  
...  

Pharmaceutical crystallization affects the properties of APIs as it determines the purity and crystal size distribution, among other attributes. This work presents two CLD–CSD models, theoretical and empirical, for a model compound.


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