Determination of minimum speed required for solids suspension in stirred vessels using pressure measurements

2008 ◽  
Vol 86 (4) ◽  
pp. 661-666 ◽  
Author(s):  
Y. S. Selima ◽  
Y. S. Fangary ◽  
N. A. Mahmoud
Keyword(s):  
Pressure Measurements ◽  
Stirred Vessels ◽  
Minimum Speed ◽  
Solids Suspension

Imaging method for the determination of the minimum agitation speed, N, for solids suspension in stirred vessels and reactors

2021 ◽  
Vol 231 ◽  
pp. 116263
Author(s):  
Baran Teoman ◽  
Shriarjun Shastry ◽  
Sara Abdelhamid ◽  
Piero M. Armenante
Keyword(s):  
Agitation Speed ◽  
Imaging Method ◽  
Stirred Vessels ◽  
Solids Suspension

Zur Thermodynamik der hydrophoben Wechselwirkung; die Systeme Wasser + Glycin+ Harnstoff und Wasser + Alanin+ Harnstoff bei 25 °C / Thermodynamics of Hydrophobie Interaction in the Systems Water + Glycin + Urea and Water + Alanin + Urea at 25 °C

1973 ◽  
Vol 28 (9-10) ◽  
pp. 533-554 ◽  
Author(s):  
Lothar Rafflenbeul ◽  
Wa-Ming Pang ◽  
Hansjürgen Schönert ◽  
Klaus Haberle
Keyword(s):  
Amino Acid ◽  
Magnetic Resonance ◽  
Proton Magnetic Resonance ◽  
Pressure Measurements ◽  
Free Enthalpy ◽  
Heat Of Dilution ◽  
Ternary Solutions ◽  
Vapor Pressure Measurements ◽  
Calorimetric Determination

Abstract Isopiestic vapor pressure measurements and calorimetric determination of the heat of dilution have been performed and evaluated with respect to enthalpy, entropy and free enthalpy in the ternary solutions water+ glycin+ urea and water+ alanin + urea. The free enthalpy of transfer for the process: Amino acid from water to water+ urea, which can be derived from these measurements, does not agree with the value calculated from solubility measurements. The reason for this discrepancy and the values of entropy and enthalpy in terms of hydrophobic interaction are discussed. Supplementary measurements of the proton magnetic resonance in these solutions are included.

Thermisches Verhalten von festem LaAlCl6 und chemischer Transport von LaCl3 mit AlCl3/Thermical Behaviour of Solid LaAlCl6 and Chemical Transport of LaCl3 with AlCl3

1999 ◽  
Vol 54 (11) ◽  
pp. 1410-1416 ◽  
Author(s):  
H. Oppermann ◽  
H. Dao Quoc ◽  
A. Morgenstern
Keyword(s):  
Total Pressure ◽  
Chemical Transport ◽  
Lanthanum Chloride ◽  
Pressure Measurements ◽  
Melting Diagram

The thermodynamical data of solid aluminium lanthanum chloride LaAlCl6 have been obtained by determination of the decomposition equilibria from total pressure measurements. The melting diagram was determined by DTA. The chemical transport of LaCl3 with AlCl3 is suggesting the existence of the gaseous complex LaAl3Cl12. The data are:ΔH(LaAlCl6f,298) =-427,1 ±2,5 kcal/mol, S°(LaAlCl6,f,298) = 61 ±2,5 cal/K-mol,Δ(LaAl3Cl12,g ,298) =-712 ± 7 kcal/mol, S°(LaAl3Cl12,g,298) = 205 ± 3 cal/K-mol.

Determination of in-plane permeability of fiber preforms by the gas flow method using pressure measurements

2003 ◽  
Vol 24 (1) ◽  
pp. 34-44 ◽  
Author(s):  
Sun K. Kim ◽  
Jeremy G. Opperer ◽  
Dae-Hwan Kim ◽  
Isaac M. Daniel
Keyword(s):  
Gas Flow ◽  
Pressure Measurements ◽  
Flow Method ◽  
Fiber Preforms

scholarly journals Jet Fuel Deposition and Oxidation: Dilution, Materials, Oxygen, and Temperature Effects

1995 ◽  
Author(s):  
Steven Zabarnick ◽  
Paula Zelesnik ◽  
Rebecca R. Grinstead
Keyword(s):  
Thermal Stability ◽  
Electrode Materials ◽  
Batch Reactor ◽  
Jet Fuel ◽  
Pressure Measurements ◽  
Good Technique ◽  
Antioxidant Concentration ◽  
Fuel Deposition

The quartz crystal microbalance (QCM) and pressure measurements are used for determination of jet fuel thermal stability in a batch reactor. The QCM is able to monitor extremely small amounts of deposition in situ, while the pressure measurements provide qualitative data on the oxidation process. The dependence of the deposition amount was monitored as a function of the oxygen availability for two fuels. Also, the effect of QCM electrode materials was investigated. Deposition and oxidation were compared for the following electrode materials: gold, aluminum, silver, and platinum. We also studied the effect of dilution on oxidation and deposition. Jet fuel was diluted with increasing amounts of hydrocarbon solvent. It was observed that this dilution procedure can help characterize a fuel’s effective antioxidant concentration. Fuel dilution is also shown to be a good technique for improving thermal stability characteristics of poor fuels. Additionally we have studied the temperature effect on deposition for two fuels over the range 140 to 180 C.

scholarly journals Development of Characterization Techniques of Thermodynamic and Physical Properties Applied to the CO2-DMSO Mixture

2009 ◽  
Vol 7 (1) ◽  
Author(s):  
Brice Calvignac ◽  
Elisabeth Rodier ◽  
Jean-Jacques Letourneau ◽  
Jacques Fages
Keyword(s):  
Process Design ◽  
Published Data ◽  
Viscosity Data ◽  
Pressure Measurements ◽  
Co2 Solubility ◽  
Volumetric Expansion ◽  
Characterization Techniques ◽  
Dmso System ◽  
Good Agreement

This work is focused on the development of new characterization techniques of physical and thermodynamic properties. These techniques have been validated using the binary system DMSO-CO2 for which several studies of characterization have been well documented. We focused on the DMSO-rich phase and we carried out measurements of volumetric expansion, density, viscosity and CO2 solubility at 298.15, 308.15 and 313.15 K and pressures up to 9 MPa. The experimental procedures were compared and validated with the available literature data on SC-CO2-DMSO system. We made density and CO2 solubility measurements, using respectively the vibrating tube technology and two static analytical methods. Lastly, we developed an innovative falling body viscosimeter for high pressure measurements. All the measurements made are in good agreement with the already published data in spite of very different experimental techniques. This work is a contribution to the understanding of the DMSO-CO2 binary as it implements new viscosity data. Moreover, it opens new perspectives about the determination of the properties of other systems such as polymers-CO2 and fats-CO2, which are essential for supercritical process design such as extraction, crystallization, chromatography and synthesis reaction.

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