Oxygen heterocyclic compound screening in Citrus essential oils by linear retention index approach applied to liquid chromatography coupled to photodiode array detector

2019 ◽  
Vol 34 (5) ◽  
pp. 349-364 ◽  
Author(s):  
Adriana Arigò ◽  
Francesca Rigano ◽  
Giuseppe Micalizzi ◽  
Paola Dugo ◽  
Luigi Mondello
Keyword(s):  
Liquid Chromatography ◽  
Essential Oils ◽  
Heterocyclic Compound ◽  
Array Detector ◽  
Photodiode Array Detector ◽  
Index Approach ◽  
Compound Screening ◽  
Linear Retention Index ◽  
Photodiode Array ◽  
Citrus Essential Oils

Monitoring of Selected Banned Azo Dyes in Edible Oils by High-Performance Liquid Chromatography-Photodiode Array Detector

2021 ◽  
Author(s):  
Mousa S. Al-Tarabeen ◽  
Abdul-Wahab O. El-Rjoob ◽  
Yahya R. Tahboub ◽  
Mohammed Y. Rasheed
Keyword(s):  
High Performance Liquid Chromatography ◽  
Liquid Chromatography ◽  
Azo Dyes ◽  
High Performance ◽  
Edible Oils ◽  
Array Detector ◽  
Photodiode Array Detector ◽  
Photodiode Array

scholarly journals Acylated Flavonoid Glycosides are the Main Pigments that Determine the Flower Colour of the Brazilian Native Tree Tibouchina pulchra (Cham.) Cogn.

Molecules ◽  
2019 ◽  
Vol 24 (4) ◽  
pp. 718 ◽  
Author(s):  
Fernanda Rezende ◽  
Marcelo Ferreira ◽  
Mads Clausen ◽  
Magdalena Rossi ◽  
Claudia Furlan
Keyword(s):  
Liquid Chromatography ◽  
High Performance ◽  
Flower Colour ◽  
Metabolite Profile ◽  
Ultra Performance Liquid Chromatography ◽  
Flavonoid Glycosides ◽  
Array Detector ◽  
Flight Mass Spectrometry ◽  
Photodiode Array Detector ◽  
Photodiode Array

Tibouchina pulchra (Cham.) Cogn. is a plant native to Brazil whose genus and family (Melastomataceae) are poorly studied with regards to its metabolite profile. Phenolic pigments of pink flowers were studied by ultra-performance liquid chromatography with a photodiode array detector and electrospray ionization quadrupole time-of-flight mass spectrometry. Therein, twenty-three flavonoids were identified with eight flavonols isolated by preparative high-performance liquid chromatography and analysed by one- and two-dimensional nuclear magnetic resonance. Kaempferol derivatives were the main flavonols, encompassing almost half of the detected compounds with different substitution patterns, such as glucoside, pentosides, galloyl-glucoside, p-coumaroyl-glucoside, and glucuronide. Concerning the anthocyanins, petunidin p-coumaroyl-hexoside acetylpentoside and malvidin p-coumaroyl-hexoside acetylpentoside were identified and agreed with previous reports on acylated anthocyanins from Melastomataceae. A new kaempferol glucoside was identified as kaempferol-(2′′-O-methyl)-4′-O-α-d-glucopyranoside. Moreover, twelve compounds were described for the first time in the genus with five being new to the family, contributing to the chemical characterisation of these taxa.

Analysis of Rotenone in Cube and Derris Root Powders and Formulations by Liquid Chromatography

1988 ◽  
Vol 71 (2) ◽  
pp. 323-324
Author(s):  
Rodney J Bushway ◽  
Angela Yang ◽  
Ali AL-Yamany
Keyword(s):  
Liquid Chromatography ◽  
Mixed Solvent ◽  
Array Detector ◽  
Photodiode Array Detector ◽  
Coefficients Of Variation ◽  
Powder Samples ◽  
Photodiode Array ◽  
Aoac Official ◽  
Liquid Chromatographic ◽  
Good Agreement

Abstract A modified liquid chromatographic (LC) procedure, including an improved extraction, has been developed to analyze rotenone in root powders of derris and cube. The procedure is also applicable to formulations. Samples are sonicated for 5 min in chloroform or a mixed solvent of tetrahydrofuran-acetonitrile-water-glacial acetic acid, followed by liquid chromatography. Rotenone content of 4 lots of root powder samples showed good agreement between the new extraction and the AOAC official extraction; coefficients of variation ranged from 5 to 1.2%. Five formulations were also analyzed and showed good agreement with results for methanol extraction. Coefficients of variation were 4.5% or less. Purity of the rotenone peaks was tested by using a photodiode array detector in the spectrum and UV ratio modes. It is recommended that the new method be tested collaboratively.

scholarly journals ESTIMATION OF GUGGULSTERONE-Z IN GOKSHURADI GUGGULU USING REVERSED-PHASE HIGH-PERFORMANCE LIQUID CHROMATOGRAPHY

2018 ◽  
Vol 11 (11) ◽  
pp. 204
Author(s):  
Kanan G Gamit ◽  
Niraj Y Vyas ◽  
Nishit D Patel ◽  
Manan A Raval
Keyword(s):  
High Performance Liquid Chromatography ◽  
Liquid Chromatography ◽  
High Performance ◽  
Limit Of Detection ◽  
Reversed Phase ◽  
Array Detector ◽  
Limit Of Quantification ◽  
Photodiode Array Detector ◽  
Validation Parameters ◽  
Photodiode Array

Objective: A study was aimed to estimate guggulsterone-Z (GZ) in Gokshuradi Guggulu (GG).Methods: An analytical method was developed and validated using Waters Alliance high-performance liquid chromatography system (Empower software), equipped with photodiode array detector. Separation was achieved using Phenomenex, C-18 (250 mm×4.6 mm, 5 μ) column. Mobile phase consisted of acetonitrile:water (70:30,v/v). Flow rate was set to 1 ml/min and detection was performed at 251 nm.Results and Discussion: Validation parameters such as linearity, precision, accuracy, limit of detection, limit of quantification, and robustness were performed. Amount of GZ was estimated using linearity equation.Conclusion: GG was found to contain 0.815±0.03 g% w/w GZ. Validated method may be used as one of the parameters to standardize the formulation.

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