Dry fracturing and cutting for techniques for scanning electron microscopy of poly-vinyl chloride particles: Application to internal structure observations

1991 ◽  
Vol 19 (4) ◽  
pp. 468-472
Author(s):  
Maria Julia Yañez ◽  
Viviana Sorrivas De Lozano
2014 ◽  
Vol 68 (5) ◽  
Author(s):  
Kritsada Phatcharasit ◽  
Wirach Taweepreda ◽  
Kanoktip Boonkerd ◽  
Jin-Kuk Kim

Electrospun poly(vinyl chloride) (PVC) nanofibrous were prepared by electrospinning. Various concentration of polyurethane (PU) were added to PVC solution for plasticization of the electrospun nanofibrous. The pristine and plasticized nanofibrous were characterized by field emission scanning electron microscopy (FE-SEM), differencial thermal analysis (DTA), and thermogravimetry analysis (TGA), respectively. Thermal properties form DTA and TGA results indicated that the addition of PU decreased glass transition temperature (Tg) of PVC and increased heat resistance of PVC nanofiber. The dielectric constant of plasticized nanofibrous measured using precision LCR meter indicated that the membrane were dense.  


2013 ◽  
Vol 844 ◽  
pp. 507-510 ◽  
Author(s):  
Kritsada Phatcharasit ◽  
Wirach Taweepreda ◽  
Kanoktip Boonkerd ◽  
Jin Kuk Kim

Various electrospun epoxized natural rubber / poly (vinyl chloride) (ENR/PVC) blend nonwoven membranes were prepared by electrospinning technique. Various concentration of epoxidized natural rubber (ENR) solution in N,N-dimethylformamide (DMF) were directly added to PVC solution for plasticization of the electrospun nanofibrous. Differencial thermal analysis (DTA), thermogravimetry analysis (TGA), fourier transfrom infrared spectroscopy (FT-IR), and scanning electron microscopy (SEM) were used to characterize the pristine and plasticized nanofibrous. DTA results indicated that the addition of ENR resulted in the shifting of glass transition temperature (Tg) towards lower temperatures. The blending of PVC with ENR is thermodynamically incompatible.


2021 ◽  
Author(s):  
Soumia Touatou ◽  
Naima Belhaneche-Bensemra

Abstract The aim of this paper is the valorisation of fibres obtained from chicken feathers in developing new poly (vinyl chloride) (PVC) biocomposites. Feather fibres were first characterized by thermogravimetric analysis and scanning electron microscopy. Then, semi-rigid and flexible PVC biocomposites were prepared by varying the fibre (5, 10 and 15 wt %) and plasticizer (15, 30, 45, 60 wt %) contents. The density, mechanical, thermal and morphological properties of the composites were investigated. The water absorption was determined at two temperatures (23 and 60°C). The results showed the influence of fibre and plasticizer contents on the considered properties.


2021 ◽  
Vol 1021 ◽  
pp. 251-259
Author(s):  
Zeyad Fadhil ◽  
Hadeel Adil ◽  
Raghda Alsayed ◽  
Mohammed H. Al-Mashhadani ◽  
Ali H. Jawad ◽  
...  

Novel extracted natural stabilizer for the polymer was investigated in this study. The natural anti-aging was extracted from plants and it is demonstrated that this type of stabilizers are suitable for biodegradable polymers. Gynostemma pentaphyllum (0.01–0.03 wt%) were extracted and added to the poly(vinyl chloride) blend. The achieved polymeric films were exposed to an accelerated UV light aging process for 300 hours at ambient temperature. The efficiency of tested natural stabilizer was linked to blank PVC films. FTIR spectroscopy, weight loss, electronic microscope and scanning electron microscopy were performed. Using small amount of natural stabilizer is significantly beneficial because it does not influence the PVC properties.


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