scholarly journals Full 1 H and 13 C NMR spectral assignment of conjugated valerolactone metabolites isolated from urine of black tea consumers by means of SPE-prepLC-MS-LC-MS-NMR

2019 ◽  
Vol 57 (9) ◽  
pp. 548-557
Author(s):  
Niels de Roo ◽  
Sanne M. J. Wilmsen ◽  
Velitchka V. Mihaleva ◽  
Doris M. Jacobs ◽  
John P. M. van Duynhoven
Keyword(s):  

2004 ◽  
Vol 18 (3) ◽  
pp. 469-483
Author(s):  
Yoshikazu Hiraga ◽  
Satomi Niwayama

The structures of the half-esters from the monohydrolysis of (exo,exo)-, (endo,endo)-, and (endo,exo)-dialkyl bicyclo[2.2.1]hept-5-ene-2,3-dicarboxylates were determined by1H and13C NMR as well as 2D NMR spectra, and the complete spectral assignment has been made. After conversion of one of the carboalkoxy groups to a carboxyl group, different tendencies were observed for the differences in1H and13C NMR chemical shifts between half-esters and the corresponding diesters.



2020 ◽  
Vol 59 (6) ◽  
pp. 648-662
Author(s):  
Jihyun Park ◽  
Seunghyun Ahn ◽  
Youngshim Lee ◽  
Dongsoo Koh ◽  
Yoongho Lim
Keyword(s):  


1999 ◽  
Vol 14 (2) ◽  
pp. 61-66 ◽  
Author(s):  
Masao Toyota ◽  
Masami Tanaka ◽  
Yoshinori Asakawa

Complete assignment of the13C NMR spectrum of the aromadendrane‒type sesquiterpene alcohol, globulol was reported, however, it still remained to be ambiguous. We report here the unambiguous and complete assignment of the1>H and13C NMR spectra of (+)‒globulol, which was isolated from the liverwortsPlagiochila ovalifolia,Neotrichocolea bissetiiandPallavicinia subciliata



2008 ◽  
Vol 46 (12) ◽  
pp. 1175-1179 ◽  
Author(s):  
Matteo Incerti ◽  
Domenico Acquotti ◽  
Paola Vicini
Keyword(s):  


Author(s):  
J.-F. Revol ◽  
Y. Van Daele ◽  
F. Gaill

The only form of cellulose which could unequivocally be ascribed to the animal kingdom is the tunicin that occurs in the tests of the tunicates. Recently, high-resolution solid-state l3C NMR revealed that tunicin belongs to the Iβ form of cellulose as opposed to the Iα form found in Valonia and bacterial celluloses. The high perfection of the tunicin crystallites led us to study its crosssectional shape and to compare it with the shape of those in Valonia ventricosa (V.v.), the goal being to relate the cross-section of cellulose crystallites with the two allomorphs Iα and Iβ.In the present work the source of tunicin was the test of the ascidian Halocvnthia papillosa (H.p.). Diffraction contrast imaging in the bright field mode was applied on ultrathin sections of the V.v. cell wall and H.p. test with cellulose crystallites perpendicular to the plane of the sections. The electron microscope, a Philips 400T, was operated at 120 kV in a low intensity beam condition.





Planta Medica ◽  
2011 ◽  
Vol 77 (12) ◽  
Author(s):  
M Mizani ◽  
S Noori ◽  
A Gerami
Keyword(s):  


2013 ◽  
Author(s):  
Husna Zulkipli ◽  
Norita Salim ◽  
Gabriele Anisah Froemming ◽  
Aletza Mohd Ismail ◽  
Hapizah Nawawi


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