scholarly journals Mercury intrusion porosimetry and centrifuge methods for extended‐range retention curves of soil and porous rock samples

2021 ◽  
Author(s):  
Antonietta C. Turturro ◽  
Maria C. Caputo ◽  
Horst H. Gerke
Keyword(s):  
Mercury Intrusion Porosimetry ◽  
Porous Rock ◽  
Mercury Intrusion ◽  
Rock Samples ◽  
Extended Range

scholarly journals Nanoscale Pore Structure Characterization and Permeability of Mudrocks and Fine-Grained Sandstones in Coal Reservoirs by Scanning Electron Microscopy, Mercury Intrusion Porosimetry, and Low-Field Nuclear Magnetic Resonance

Geofluids ◽  
2018 ◽  
Vol 2018 ◽  
pp. 1-20 ◽  
Author(s):  
Na Zhang ◽  
Fangfang Zhao ◽  
Pingye Guo ◽  
Jiabin Li ◽  
Weili Gong ◽  
...  
Keyword(s):  
Electron Microscopy ◽  
Pore Size ◽  
Mercury Intrusion Porosimetry ◽  
Mercury Intrusion ◽  
Rock Samples ◽  
Fine Grained ◽  
Low Field ◽  
Water Saturated ◽  
Pore Types ◽  
Scanning Electron

Porosity and permeability of two typical sedimentary rocks in coal bearing strata of underground coal mines in China, i.e., mudrocks and fine-grained sandstones, were comprehensively investigated by multiple experimental methods. Measured porosity averages of the helium gas porosity (φg), MIP porosity (φMIP), water porosity (φw), and NMR porosity (φNMR) of the twelve investigated rock samples range from 1.78 to 16.50% and the measured gas permeabilities (Kg) range from 0.0003 to 2.4133 mD. Meanwhile, pore types, pore morphologies, and pore size distributions (PSD) were determined by focused ion beam scanning electron microscopy (FIB-SEM), mercury intrusion porosimetry (MIP), and low-field nuclear magnetic resonance (NMR). FIB-SEM image analyses showed that the mineral matrix pores including interparticle (interP) and intraparticle (intraP) pores with varied morphologies are the dominant pore types of the investigated rock samples while very few organic matter (OM) pores were observed. Results of the MIP and the full water-saturated NMR measurements showed that the PSD curves of the mudrock samples mostly present a unimodal pattern and nanopores with pore diameter less than 0.1 μm are their predominant pore type, while the PSD curves of the fine-grained sandstone samples are featured by a bimodal distribution. Furthermore, comparison of the full water-saturated and irreducible-water-saturated NMR measurements indicated that pores in the mudrocks are solely adsorption pores (normally pore size < 0.1 μm) whereas apart from a fraction of adsorption pores, a large part of the pores in the sandstone sample with relatively high porosity are seepage pores (normally pore size > 0.1 μm). Moreover, the PSD curves of NMR quantitatively converted from the NMR T2 spectra by T2Pc and weighted arithmetic mean (WAM) methods are in good agreement with the PSD curves of MIP. Finally, the applicability of three classic permeability estimation models based on MIP and NMR data to the investigated rock samples was evaluated.

scholarly journals Effect of Hydrogen Nanobubbles on the Mechanical Strength and Watertightness of Cement Mixtures

Materials ◽  
2021 ◽  
Vol 14 (8) ◽  
pp. 1823
Author(s):  
Won-Kyung Kim ◽  
Young-Ho Kim ◽  
Gigwon Hong ◽  
Jong-Min Kim ◽  
Jung-Geun Han ◽  
...  
Keyword(s):  
Mercury Intrusion Porosimetry ◽  
Cement Mortar ◽  
Stable State ◽  
Pozzolanic Reaction ◽  
Hydration Reaction ◽  
High Concentration ◽  
Mercury Intrusion ◽  
Electron Microscope Analysis ◽  
Mixing Water ◽  
Cement Mixtures

This study analyzed the effects of applying highly concentrated hydrogen nanobubble water (HNBW) on the workability, durability, watertightness, and microstructure of cement mixtures. The number of hydrogen nanobubbles was concentrated twofold to a more stable state using osmosis. The compressive strength of the cement mortar for each curing day was improved by about 3.7–15.79%, compared to the specimen that used general water, when two concentrations of HNBW were used as the mixing water. The results of mercury intrusion porosimetry and a scanning electron microscope analysis of the cement paste showed that the pore volume of the specimen decreased by about 4.38–10.26%, thereby improving the watertightness when high-concentration HNBW was used. The improvement in strength and watertightness is a result of the reduction of the microbubbles’ particle size, and the increase in the zeta potential and surface tension, which activated the hydration reaction of the cement and accelerated the pozzolanic reaction.

scholarly journals Insights into matrix compressibility of coals by mercury intrusion porosimetry and N2 adsorption

2018 ◽  
Vol 200 ◽  
pp. 199-212 ◽  
Author(s):  
Yidong Cai ◽  
Qian Li ◽  
Dameng Liu ◽  
Yingfang Zhou ◽  
Dawei Lv
Keyword(s):  
Mercury Intrusion Porosimetry ◽  
N2 Adsorption ◽  
Mercury Intrusion

scholarly journals Investigation of the Porosity of Certain Iraqi Clay Deposits by Mercury Porosimeter

2009 ◽  
Vol 6 (1) ◽  
pp. 163-172
Author(s):  
Baghdad Science Journal
Keyword(s):  
Pore Volume ◽  
Pore Diameter ◽  
Mercury Intrusion Porosimetry ◽  
Narrow Range ◽  
Volume Distribution ◽  
Natural Clay ◽  
Mercury Intrusion ◽  
Clay Deposits ◽  
Pore Area ◽  
Mercury Porosimeter

Pore volume, pore diameter, and pore volume distribution of three of Iraqi natural clay deposites were measured using mercury intrusion porosimetry .The clays are white kaolin, colored kaolin, and bentonite .The results showed that the variation of the pore area of the clay deposites followed the following order :- Coloured Kaolin > White Kaolin > Bentonite While the pore volume may be arranged as in the following sequence:- White Kaolin > Coloured Kaolin >Bentonite Also , Bentonite exhibits the narrow range pore size distribution than the white and coloured kaolin.

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