Solid Phase Microextraction for Analysis of Polymer Degradation Products and Additives

Author(s):  
Minna Hakkarainen
2013 ◽  
Vol 781-784 ◽  
pp. 591-595
Author(s):  
Di Liu ◽  
Yu Shao ◽  
Xiao Hong Yang

By solid phase microextraction - Gas Chromatography - mass spectrometry (SPME-GC-MS) technique against acid and methionine bad blood (ASA-Met) model of the reaction products were identified, studied the effect of Fe2+ on the formation of flavor compounds in the model reaction. 27 flavour compounds of furan, pyrazine, thiophene, sulfur and other compounds, were identified, of which, sulfur-containing compounds such as aliphatic cyclic sulfides, sulfide, pyrazine is the main flavor components. Fe2+ was added to the model in the system, on one hand the about adding some sulfur compounds yield, pyrazine compounds significantly increase; on the other hand, Thiophenes significantly reduced compounds or even disappear. This shows that in the model reaction, Fe2+ promotes the thermal degradation of Met, at the same time, suggesting that Fe2+ as oxidant to promote NH3, NH3 and H2S to generate competitive reaction and ASA degradation products formed compounds containing nitrogen, resulting in reduced Thiophenes compounds yield.


2001 ◽  
Vol 13 (6) ◽  
pp. 215-220 ◽  
Author(s):  
Fruzsina Doleschall ◽  
Zsolt Kemény ◽  
Katalin Recseg ◽  
Katalin Kővári

2014 ◽  
Vol 5 (7) ◽  
pp. 1495-1505 ◽  
Author(s):  
Hassan Sabik ◽  
Allaoua Achouri ◽  
Maria Alfaro ◽  
Marylène Pelletier ◽  
Denis Belanger ◽  
...  

A method was developed to quantify lemon oil components and their degradation products in oil-in-water emulsions.


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