Protective Layers for Special Types of Composites

1990 ◽  
pp. 327-336 ◽  
Author(s):  
P. Ehrburger
Keyword(s):  
Protective Layers

Cross-sectional TEM specimen preparation from magneto-optical disk by ultramicrotomy

1993 ◽  
Vol 51 ◽  
pp. 236-237
Author(s):  
F. Shaapur ◽  
M.J. Kim ◽  
Seh Kwang Lee ◽  
Soon Gwang Kim
Keyword(s):  
System Development ◽  
Thin Foil ◽  
Specimen Preparation ◽  
Material System ◽  
Cross Sectional ◽  
Protective Layers ◽  
New Material ◽  
Diamond Saw ◽  
Original Production ◽  
Thick Medium

TEM characterization and microanalysis of the recording media is crucial and complementary to new material system development as well as quality control applications. Due to the type of material generally used for supporting the medium, i.e., a polymer, conventional macro- and microthinning procedures for thin foil preparation are not applicable. Ultramicrotorny (UM) is a viable option and has been employed in previous similar studies. In this work UM has been used for preparation of XTEM samples from a magneto-optical (MO) recording medium in its original production format.The as-received material system consisted of a 4-layer, 2100 Å thick medium including a 300 Å TbFeCo layer enveloped by silicon nitride protective layers supported on a 1.2 mm thick × 135 mm (5.25 in.) diameter polycarbonate disk. Recording tracks had an approximate pitch of 1.6 μm separated by 800 Å deep peripheral grooves. Using a Buehler Isomet low-speed diamond saw, 1 mm wide and 20 mm long strips were cut out of the disk along the recording tracks.

Fullerene-like Nanoparticles of WS2 as a Promising Protection from Erosive Wear of Gun Bore Nozzles

2020 ◽  
Vol 16 (1) ◽  
pp. 62-70 ◽  
Author(s):  
Narimane Rezgui ◽  
Danica Simić ◽  
Choayb Boulahbal ◽  
Dejan Micković
Keyword(s):  
Mass Loss ◽  
Solid Lubricant ◽  
Erosive Wear ◽  
Mechanical Resistance ◽  
Protective Function ◽  
Protective Layers ◽  
Total Mass Loss ◽  
Mass Losses ◽  
Before And After ◽  
Tube Life

Background: Erosive wear causes increase in the bore diameter of firearms barrels and nozzles. Most responsible factors for this erosion are friction and heat generated during the shot. Protection from erosive wear is very important for gun tube life cycle, and various protection methods are used: adding phlegmatizers in gunpowder composition or applying protective layers on the gun bore inner surface. Objective: In this research, a possibility is examined to protect the surface of a nozzle exposed to gunpowder erosion applying a layer of tungsten disulfide fullerene-like nanoparticles, IF-WS2, known as outstanding solid lubricant of a great mechanical resistance. Methods: Nanoparticles on the nozzle surface before and after the gunfire tests were observed using scanning electron microscopy/energy dispersive X-ray spectroscopy. Gunfire tests were performed on designed erosion device. Temperatures in the defined position near the affected surface were measured with thermocouples and compared for the nozzles with and without nanoprotection, as well as the nozzle mass loss after each round. Results: For the sample with IF-WS2 lower temperatures after firing and lower mass losses were observed. Mass loss after first round was 25.6% lower for the sample with protective nanoparticles layer, and the total mass loss was about 5% lower after five rounds. After the first round the nozzle without IF-WS2 was heated up to a temperature which was for 150.8°C higher than the nozzle with IF-WS2. Conclusion: Protective function of IF-WS2 is the most pronounced for the first round. The observed results encourage its further application in firearms gun bores protection.

Pitting mechanism of mild steel in marginally sour environments—Part I: A parametric study based on formation of protective layers

2021 ◽  
Vol 183 ◽  
pp. 109305
Author(s):  
Wei Zhang ◽  
Bruce Brown ◽  
David Young ◽  
Gheorghe Bota ◽  
Srdjan Nesic ◽  
...  
Keyword(s):  
Mild Steel ◽  
Parametric Study ◽  
Protective Layers

scholarly journals Study of High-Temperature Properties of Asphalt Mixtures Used for Bridge Pavement with Concrete Deck

Materials ◽  
2021 ◽  
Vol 14 (15) ◽  
pp. 4238
Author(s):  
Piotr Pokorski ◽  
Piotr Radziszewski ◽  
Michał Sarnowski
Keyword(s):  
Permanent Deformation ◽  
Asphalt Mixture ◽  
Binder Content ◽  
Void Content ◽  
Concrete Bridge ◽  
Asphalt Mixes ◽  
Protective Layers ◽  
Concrete Bridge Decks ◽  
Air Void ◽  
Air Void Content

The paper presents the issue of resistance to permanent deformations of bridge pavements placed upon concrete bridge decks. In Europe, bridge asphalt pavement usually consists of a wearing course and a protective layer, which are placed over the insulation (waterproofing). Protective layers of bridge pavement are commonly constructed using low air void content asphalt mixes as this provides the suitable tightness of such layers. Due to increased binder content, asphalt mixes for bridge pavement may have reduced resistance to permanent deformations. The article presents test results of resistance to permanent deformations of asphalt mixes for the protective layers. In order to determine the composition of mixtures with low air void content and resistance to permanent deformation, an experimental design was applied using a new concept of asphalt mix composition. Twenty-seven different asphalt mixture compositions were analyzed. The mixtures varied in terms of binder content, sand content and grit ratio. Resistance to permanent deformation was tested using the laboratory uniaxial cyclic compression method (dynamic load creep). On the basis of experimental results and statistical analysis, the functions of asphalt mixture permanent deformation resistance were established. This enabled a determination of suitable mixture compositions for protective layers for concrete bridge decks.

Influence of the Deposition Parameters on the Properties of Bis-Triethoxysilylpropyl] Tetrasulphide (BTESPT) Layers on AA2024-T3 – An Ellipsometric Study

2006 ◽  
Vol 514-516 ◽  
pp. 682-686 ◽  
Author(s):  
Ana Cabral ◽  
Jorge P. Correia ◽  
Mário G.S. Ferreira
Keyword(s):  
Optical Absorption ◽  
Optical Model ◽  
Ex Situ ◽  
Water Molecules ◽  
Structural Reorganization ◽  
Final Thickness ◽  
Protective Layers ◽  
Deposition Parameters ◽  
Ellipsometric Study ◽  
Silane Concentration

A bis-sulphur silane (BTESPT) was used to produce thin protective layers on AA2024- T3, a structural aluminium alloy widely used in the aeronautic industry, being the coatings analysed ex-situ by ellipsometry. Despite a slight degree of film anisotropy evidenced by measurements at different angles of incidence, an optical model of a single homogeneous phase could be employed to describe the silane based layer. The information obtained allowed to characterize the influence of the operational deposition parameters on the film thickness and structural organization of the silane phase (evaluated by its optical absorption). It is shown that the silane concentration of the solution and immersion time determine the final thickness of the formed layer while the curing time does not affect significantly this parameter. On the other hand, it was observed a marked decrease of the optical absorption of the coatings submitted to curing temperatures of at least 100°C, which should be ascribed to a structural reorganization phenomena induced by the removal of water molecules from the film. The data gathered by ellipsometry were successfully corroborated by independent surface profilometry analysis of the films.

scholarly journals The Mechanism of Lubricants Protective Layers Formation in Friction Sliding

2016 ◽  
Vol 150 ◽  
pp. 458-463 ◽  
Author(s):  
V.G. Shram ◽  
A.V. Lysyannikov ◽  
M.A. Kovaleva
Keyword(s):  
Protective Layers

Reversal Tolerant Anodes Using Protective Layers for Highly Robust Automotive Fuel Cells

2021 ◽  
Vol 4 (1) ◽  
pp. 119-127
Author(s):  
Leiming Hu ◽  
Bo Ki Hong ◽  
Jong-Gil Oh ◽  
Shawn Litster
Keyword(s):  
Fuel Cells ◽  
Protective Layers ◽  
Automotive Fuel

Plasma Spraying of Solid Oxide Fuel Cell Components

1997 ◽  
Author(s):  
G. Schiller ◽  
M. Müller ◽  
R. Ruckdäschel ◽  
R. Henne ◽  
M. Lang
Keyword(s):  
Plasma Spraying ◽  
Plasma Spray ◽  
Solid Oxide ◽  
Rf Plasma ◽  
Spray Parameters ◽  
Oxide Fuel ◽  
Bipolar Plates ◽  
Metallic Bipolar Plates ◽  
Protective Layers ◽  
Near Net Shape

Abstract The central components for solid oxide fuel cells (SOFC) are the electrodes-electrolyte multilayer arrangement (PEN) and the separating bipolar plates. The PEN (Positive electrode- Electrolyte-Negative electrode) assembly consists of a dense gastight yttria-stabilized zirconia (YSZ) electrolyte and porous electrodes for which usually Ni-YSZ cermet anode and Sr-doped LaMnO3 cathode layers are used. The various PEN units are connected in a cell stack by bipolar plates which are either metallic or ceramic ones. Furthermore, a protective layer on the metallic bipolar plates consisting of a chromium alloy is required to prevent chromium evaporation leading to a rapid and strong degradation of the SOFC performance. At the DLR Stuttgart both the DC and the RF vacuum plasma spraying technique have been further developed and adapted to meet the requirements for the manufacture of the different SOFC components. The DCVPS process using specially developed Laval-like nozzles is especially appropriate to the production of thin and dense coatings as required for the electrolyte and the protective layers. However, applying special spray parameters and nozzles it is also possible to deposit porous electrode layers. The production of the entire PEN arrangement in one consecutive DC-VPS process is the objective of the actual development. On the other hand, the RF plasma spray technique is suitable for the near net-shape production of bulk components such as the metallic bipolar plate. The development of the deposition processes for the production of SOFC components using DC and RF plasma spray methods and the results obtained concerning PEN fabrication, deposition of protective layers and the near net-shape production of metallic bipolar plates are presented in the paper.

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