Influence of post-oxidation reactions on the physicochemical properties of TEMPO-oxidized cellulose nanofibers before and after amidation

Cellulose ◽  
2019 ◽  
Vol 27 (3) ◽  
pp. 1273-1288 ◽  
Author(s):  
L. A. Calderón-Vergara ◽  
S. A. Ovalle-Serrano ◽  
C. Blanco-Tirado ◽  
M. Y. Combariza
Keyword(s):  
Physicochemical Properties ◽  
Cellulose Nanofibers ◽  
Oxidized Cellulose ◽  
Oxidation Reactions ◽  
Before And After

Non-oxidized cellulose nanofibers as a topical hemostat: in vitro thromboelastometry studies of structure vs function

2021 ◽  
pp. 118043
Author(s):  
Elmira Mohamed ◽  
Lucy A. Coupland ◽  
Philip J. Crispin ◽  
Ailene Fitzgerald ◽  
David R. Nisbet ◽  
...  
Keyword(s):  
Cellulose Nanofibers ◽  
Oxidized Cellulose

The physicochemical properties of white sorghum (Sorghum bicolor L.) flour in various particle sizes by soaking the seeds before and after dehulling

Food Research ◽  
2021 ◽  
Vol 5 (3) ◽  
Author(s):  
S.S. Antarlina ◽  
T. Estiasih ◽  
E. Zubaidah ◽  
Harijono
Keyword(s):  
Physicochemical Properties ◽  
Amylose Content ◽  
Particle Sizes ◽  
Sorghum Flour ◽  
Applied Technology ◽  
Before And After ◽  
Good Nutrition ◽  
Food Needs ◽  
Home Industries ◽  
Sorghum Bicolor L

Sorghum seeds have good nutrition for human health. Therefore, preparation for food needs to be done by various methods. This study aimed to investigate the physicochemical properties of sorghum flour at various particle sizes obtained from soaked seeds in water before and after dehulling. This study used white sorghum seeds (KD-4 variety), and the experiment involved three factors: seeds soaking in water before and after dehulling, the soaking duration of the seeds (0, 12, 24, 36, 48 hrs), and the particle size of the flour passed through 40, 60, 80, 100 mesh sieves. This result showed, was chosen method of making white sorghum flour that was to soak the seeds in water for 24 hrs after dehulling. Followed by drying, milling, and sieving on various particle fractions will be adjusted according to their use. The physicochemical properties of sorghum flour were whiteness: 66.85±0.85–73.44±0.99%; bulk density: 514.35±0.95–584.10±1.00 g/L; initial temperature of gelatinization: 87.80±1.20 – 92.25±1.45°C; gelatinization time: 16.00±0.01 –18.00±1.00 mins; viscosity at temperature 50°C: 1250.1±46.7–3568.3±230.9 Cp; setback viscosity: 1250.6±46.7–3568.3±230.9 Cp; moisture content: 8.26±0.14 - 9.56±0.30% wet basis; ash content: 0.14±0.01–0.35±0.02% dry basis; protein content: 5.30±0.05– 6.77±0.38% dry basis; fat content: 1.02±0.01–2.40±0.01% dry basis; carbohydrate content: 81.66±0.60–84.33±0.18% dry basis; and amylose content: 12.43±0.28– 24.35±0.06% dry basis. The method for making white sorghum flour can be used to produce applied technology in home industries and suitable for cake and extrusion products.

scholarly journals Interfacial Hydrolysis of Acetals on Protonated TEMPO-oxidized Cellulose Nanofibers

2018 ◽  
Vol 8 (1) ◽  
Author(s):  
Yuya Tamura ◽  
Kyohei Kanomata ◽  
Takuya Kitaoka
Keyword(s):  
Cellulose Nanofibers ◽  
Oxidized Cellulose ◽  
Hydrolysis Of

scholarly journals Three-Dimensional Stable Alginate-Nanocellulose Gels for Biomedical Applications: Towards Tunable Mechanical Properties and Cell Growing

Nanomaterials ◽  
2019 ◽  
Vol 9 (1) ◽  
pp. 78 ◽  
Author(s):  
Priscila Siqueira ◽  
Éder Siqueira ◽  
Ana Elza De Lima ◽  
Gilberto Siqueira ◽  
Ana Delia Pinzón-Garcia ◽  
...  
Keyword(s):  
Electron Microscopy ◽  
Mechanical Properties ◽  
Tissue Engineering ◽  
Wound Healing ◽  
Cellulose Nanocrystals ◽  
Biomedical Applications ◽  
Cellulose Nanofibers ◽  
Oxidized Cellulose ◽  
Freeze Dried ◽  
Alginate Gels

Hydrogels have been studied as promising materials in different biomedical applications such as cell culture in tissue engineering or in wound healing. In this work, we synthesized different nanocellulose-alginate hydrogels containing cellulose nanocrystals, TEMPO-oxidized cellulose nanocrystals (CNCTs), cellulose nanofibers or TEMPO-oxidized cellulose nanofibers (CNFTs). The hydrogels were freeze-dried and named as gels. The nanocelluloses and the gels were characterized by different techniques such as Fourier-transform infrared spectroscopy (FTIR), scanning electron microscopy (SEM), transmission electron microscopy (TEM), thermogravimetric analysis (TGA), and dynamic mechanical thermal analysis (DMTA), while the biological features were characterized by cytotoxicity and cell growth assays. The addition of CNCTs or CNFTs in alginate gels contributed to the formation of porous structure (diameter of pores in the range between 40 and 150 μm). TEMPO-oxidized cellulose nanofibers have proven to play a crucial role in improving the dimensional stability of the samples when compared to the pure alginate gels, mainly after a thermal post-treatment of these gels containing 50 wt % of CNFT, which significantly increased the Ca2+ crosslinking density in the gel structure. The morphological characteristics, the mechanical properties, and the non-cytotoxic behavior of the CNFT-alginate gels improved bioadhesion, growth, and proliferation of the cells onto the gels. Thus, the alginate-nanocellulose gels might find applications in tissue engineering field, as for instance, in tissue repair or wound healing applications.

scholarly journals Facile Synthesis of Calcium Hydroxide Nanoparticles onto TEMPO-Oxidized Cellulose Nanofibers for Heritage Conservation

ACS Omega ◽  
2019 ◽  
Vol 4 (24) ◽  
pp. 20606-20611
Author(s):  
Mounir El Bakkari ◽  
Vivek Bindiganavile ◽  
Yaman Boluk
Keyword(s):  
Calcium Hydroxide ◽  
Cellulose Nanofibers ◽  
Heritage Conservation ◽  
Oxidized Cellulose ◽  
Facile Synthesis

scholarly journals Physicochemical properties of meat from Bos taurus and Bos indicus

2011 ◽  
Vol 40 (6) ◽  
pp. 1250-1259 ◽  
Author(s):  
Maria Cristina Bressan ◽  
Erika Cristina Rodrigues ◽  
Lizandra Vercezi Rossato ◽  
Eduardo Mendes Ramos ◽  
Luis Telo da Gama
Keyword(s):  
Physicochemical Properties ◽  
Meat Quality ◽  
Shear Force ◽  
Positive Relationship ◽  
Bos Taurus ◽  
Bos Indicus ◽  
Post Mortem ◽  
Fresh Meat ◽  
Lower Shear ◽  
Before And After

The objective of this study was to characterize meat quality in Bos taurus and Bos indicus and to determine the influence of finishing system and genetic group on the physicochemical properties of the longissimus thoracis at 24 hours and 10 days post mortem (1ºC). The sample included 160 bulls of the B. taurus (n=75) and B. indicus (n=85) groups, finished either on pasture (n=46) or with grain supplementation (n=114), slaughtered at a carcass weight of 270 to 300 kg. Pasture-finished animals had higher pH, lower red content and a fat content 2.5 times lower than those finished with supplementation. Meat from supplement-finished animals had lower shear force in comparison to that from animals finished on pasture, with means of 7.7 and 8.5 kg at 24 hours, and of 5.5 and 5.9 kg at 10 days, respectively. Samples of B. taurus and B. indicus were similar in moisture and protein, but B. taurus presented higher means for ash and lower means for fat. Aged samples of B. indicus finished on pasture showed lower values for lightness and yellowness. Overall, lightness and yellow content increased and red content decreased with 10-day ageing. Means for shear force were lower in B. taurus than in B. indicus, with differences of 1.4 kg in fresh meat and 0.6 kg in aged samples. The reduction in shear force with ageing was more pronounced in samples with higher initial shear force, in spite of the positive relationship between shear force before and after ageing.

scholarly journals Advanced microscopy and spectroscopy reveal the adsorption and clustering of Cu(ii) onto TEMPO-oxidized cellulose nanofibers

Nanoscale ◽  
2017 ◽  
Vol 9 (22) ◽  
pp. 7419-7428 ◽  
Author(s):  
Chuantao Zhu ◽  
Alexander Soldatov ◽  
Aji P. Mathew
Keyword(s):  
Cellulose Nanofibers ◽  
Oxidized Cellulose
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