Injection molding of ultra-fine Si3N4 powder for gas-pressure sintering

2015 ◽  
Vol 22 (6) ◽  
pp. 654-659 ◽  
Author(s):  
Xian-feng Yang ◽  
Jiang-hong Yang ◽  
Xie-wen Xu ◽  
Qi-cheng Liu ◽  
Zhi-peng Xie ◽  
...  
Keyword(s):  
Injection Molding ◽  
Gas Pressure ◽  
Si3n4 Powder ◽  
Gas Pressure Sintering

Development of α-β SiAlON Ceramics from Different Si3N4 Starting Powders

2008 ◽  
Vol 403 ◽  
pp. 107-108 ◽  
Author(s):  
Nurcan Calis Acikbas ◽  
Ferhat Kara ◽  
Hasan Mandal
Keyword(s):  
Fracture Toughness ◽  
Process Parameters ◽  
Gas Pressure ◽  
Economic Viability ◽  
Si3n4 Powder ◽  
Gas Pressure Sintering

- SiAlON ceramics were produced from different starting Si3N4 powders including β-Si3N4 and α-Si3N4 powders and mixtures of these powders. Gas pressure sintering was used for sintering. After sintering, resultant fracture toughness values were correlated with microstructure and starting powders. By optimizing chemistry and process parameters; - SiAlON ceramics with reasonable fracture toughness can be produced from rather coarse β-Si3N4 powder. This could improve the economic viability of SiAlON ceramics since -Si3N4 powders are less costly.

Determination of Optimum Process Parameters in Gas-Assisted Injection Molding

2011 ◽  
Vol 143-144 ◽  
pp. 494-498
Author(s):  
Ke Ming Zi ◽  
Li Heng Chen
Keyword(s):  
Injection Molding ◽  
Delay Time ◽  
Optimization Design ◽  
Gas Pressure ◽  
Optimum Process ◽  
Injection Molding Process ◽  
Technological Parameters ◽  
Molding Process ◽  
Element Analysis ◽  
Melt Temperature

With finite element analysis software Moldflow, numerical simulation and studies about FM truck roof handle were conducted on gas-assisted injection molding process. The influences of melt pre-injection shot, gas pressure, delay time and melt temperature were observed by using multi-factor orthogonal experimental method. According to the analysis of the factors' impact on evaluation index, the optimized parameter combination is obtained. Therefore the optimization design of technological parameters is done. The results show that during the gas-assisted injection molding, optimum pre-injection shot is 94%,gas pressure is 15MPa,delay time is 0.5s,melt temperature is 240 oC. This study provided a more practical approach for the gas-assisted injection molding process optimization.

Luminescence properties of a green-emitting Eu2+-doped Sr-containing SiAlON phosphors by gas pressure sintering

2015 ◽  
Vol 26 (6) ◽  
pp. 3805-3812 ◽  
Author(s):  
Chunlei Zhao ◽  
Qian Ma ◽  
Ronghui Liu ◽  
Huibing Xu ◽  
Hongqi Ye ◽  
...  
Keyword(s):  
Gas Pressure ◽  
Luminescence Properties ◽  
Gas Pressure Sintering

Influence of powder characteristics on gas pressure sintering of Si3N4

1988 ◽  
Vol 23 (9) ◽  
pp. 3413-3419 ◽  
Author(s):  
M. Mitomo ◽  
N. Yang ◽  
Y. Kishi ◽  
Y. Bando
Keyword(s):  
Gas Pressure ◽  
Powder Characteristics ◽  
Gas Pressure Sintering

Thermal Conductivity of Si₃N₄ Ceramics Fabricated From Carbothermal-reduction-derived Powder

2021 ◽  
Author(s):  
Yuelong Wang ◽  
Xingyu Li ◽  
Haoyang Wu ◽  
Baorui Jia ◽  
Deyin Zhang ◽  
...  
Keyword(s):  
Mechanical Properties ◽  
Thermal Conductivity ◽  
Fracture Toughness ◽  
Grain Size ◽  
Flexural Strength ◽  
Grain Boundaries ◽  
Carbothermal Reduction ◽  
Secondary Phase ◽  
Gas Pressure ◽  
Gas Pressure Sintering

Abstract Si3N4-based ceramic (Si3N4-5wt%Y2O3-3wt%MgO) was obtained from carbothermal-reduction-derived powder combined with gas pressure sintering. The phase, microstructure, thermal conductivity and mechanical properties of Si3N4 ceramics were comprehensively analyzed. Dense Si3N4 ceramic with uniform grain size was obtained after sintering at 1900°C for 7 h under a N2 pressure of 1.2 MPa. The secondary phase consisted of Y4Si2O7N2 and Y2Si3O3N4 was found to gather around triangular grain boundaries. The thermal conductivity, flexural strength, hardness and fracture toughness of the Si3N4 ceramics were 95.7 W·m-1·k-1, 715 MPa, 17.2 GPa and 7.2 MPa·m1/2, respectively. The results were compared with product derived from commercial powder, the improvement of thermal conductivity (~8.3%) and fracture toughness (~4.3%) demonstrating the superiority of Si3N4 ceramics prepared from carbothermal-reduction-derived powder.

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