Determination of Warm Working Temperature Range for In Situ Alm–TiB2p Composite

2014 ◽  
Vol 96 (1) ◽  
pp. 15-19
Author(s):  
R. Mishra ◽  
A. Alexander ◽  
K. Srinivasan
Keyword(s):  
Temperature Range ◽  
Working Temperature ◽  
Warm Working

Determination of the stability of cable thermocouples at the upper limit of their working temperature range

Metallurgist ◽  
2011 ◽  
Vol 54 (9-10) ◽  
pp. 641-646 ◽  
Author(s):  
A. A. Ulanovskii ◽  
S. I Kalimulina ◽  
A. M. Belenkii ◽  
A. N. Bursin ◽  
L. N. Dergausova
Keyword(s):  
Temperature Range ◽  
Working Temperature ◽  
Upper Limit ◽  
The Stability

scholarly journals Compositional optimization for molding of bioactive glasses in the SIO2 -NA2O-CAO-P2 O5 System / Otimização composicional para moldagem de vidros bioativos no sistema SIO2 -NA2O-CAO-P2 O5

2021 ◽  
Vol 5 (4) ◽  
pp. 1820-1827
Author(s):  
Nícolas Lara ◽  
Maria Inês Basso Bernardi
Keyword(s):  
Energy Efficient ◽  
Bioactive Glasses ◽  
Temperature Range ◽  
Working Temperature ◽  
P2o5 System

This paper shows the determination of the most energy efficient composition for molding of bioglasses in the SiO2 -Na2O-CaO-P2O5 system. Ten compositions were formulated in the range where the glass has a bioactivity index greater than 8 and the curves of viscosity as a function of temperature were drawn using the Vogel-Fulcher-Tammann (VFT) equation. Analyzing the curves, the composition 43SiO2 -30CaO-21Na2O-6P2O5 has the lowest viscosity over the entire working temperature range, requiring less heat to be molded and consequently consuming less energy in the ovens.

The reaction of amorphous Ni-Nb films with Si in the presence of a native SiO2 layer

1990 ◽  
Vol 48 (4) ◽  
pp. 664-665
Author(s):  
N. Rozhanski ◽  
A. Barg
Keyword(s):  
High Temperature ◽  
Crystallization Temperature ◽  
Diffusion Barriers ◽  
Sio2 Layer ◽  
Si Substrate ◽  
Cross Sectional ◽  
Plan View ◽  
Temperature Range ◽  
Sputter Deposited

Amorphous Ni-Nb alloys are of potential interest as diffusion barriers for high temperature metallization for VLSI. In the present work amorphous Ni-Nb films were sputter deposited on Si(100) and their interaction with a substrate was studied in the temperature range (200-700)°C. The crystallization of films was observed on the plan-view specimens heated in-situ in Philips-400ST microscope. Cross-sectional objects were prepared to study the structure of interfaces.The crystallization temperature of Ni5 0 Ni5 0 and Ni8 0 Nb2 0 films was found to be equal to 675°C and 525°C correspondingly. The crystallization of Ni5 0 Ni5 0 films is followed by the formation of Ni6Nb7 and Ni3Nb nucleus. Ni8 0Nb2 0 films crystallise with the formation of Ni and Ni3Nb crystals. No interaction of both films with Si substrate was observed on plan-view specimens up to 700°C, that is due to the barrier action of the native SiO2 layer.

INDIREKTE PAPIERCHROMATOGRAPHISCHE METHODE ZUR BESTIMMUNG DER HARNOESTROGENE

1961 ◽  
Vol 38 (4) ◽  
pp. 545-562 ◽  
Author(s):  
L. Kecskés ◽  
F. Mutschler ◽  
I. Glós ◽  
E. Thán ◽  
I. Farkas ◽  
...  
Keyword(s):  
Pregnant Women ◽  
Granulosa Cell ◽  
Iron Content ◽  
List Type ◽  
Granulosa Cell Tumour ◽  
Hydrolysis Of ◽  
Phenol Fraction ◽  
Qualitative Determination

ABSTRACT 1. An indirect paperchromatographic method is described for separating urinary oestrogens; this consists of the following steps: acidic hydrolysis, extraction with ether, dissociation of phenol-fractions with partition between the solvents. Previous purification of phenol fraction with the aid of paperchromatography. The elution of oestrogen containing fractions is followed by acetylation. Oestrogen acetate is isolated by re-chromatography. The chromatogram was developed after hydrolysis of the oestrogens 'in situ' on the paper. The quantity of oestrogens was determined indirectly, by means of an iron-reaction, after the elution of the iron content of the oestrogen spot, which was developed by the Jellinek-reaction. 2. The method described above is satisfactory for determining urinary oestrogen, 17β-oestradiol and oestriol, but could include 16-epioestriol and other oestrogenic metabolites. 3. The sensitivity of the method is 1.3–1.6 μg/24 hours. 4. The quantitative and qualitative determination of urinary oestrogens with the above mentioned method was performed in 50 pregnant and 9 non pregnant women, and also in 2 patients with granulosa cell tumour.

Single Crystal Growth of High-Pressure Phases of Ice and Salt Hydrate Far Below the Original Melting Point by Mixing Alcohol: Crystal Structure Determination of Magnesium Chloride Heptahydrate

2020 ◽  
Author(s):  
Keishiro Yamashita ◽  
Kazuki Komatsu ◽  
Hiroyuki Kagi
Keyword(s):  
Crystal Structure ◽  
High Pressure ◽  
Crystal Growth ◽  
Single Crystal ◽  
Room Temperature ◽  
Growth Technique ◽  
Salt Hydrate ◽  
X Ray

An crystal-growth technique for single crystal x-ray structure analysis of high-pressure forms of hydrogen-bonded crystals is proposed. We used alcohol mixture (methanol: ethanol = 4:1 in volumetric ratio), which is a widely used pressure transmitting medium, inhibiting the nucleation and growth of unwanted crystals. In this paper, two kinds of single crystals which have not been obtained using a conventional experimental technique were obtained using this technique: ice VI at 1.99 GPa and MgCl<sub>2</sub>·7H<sub>2</sub>O at 2.50 GPa at room temperature. Here we first report the crystal structure of MgCl2·7H2O. This technique simultaneously meets the requirement of hydrostaticity for high-pressure experiments and has feasibility for further in-situ measurements.

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