Transformation of ordered face-centered tetragonal θ-MnNi phase to face-centered cubic austenite during isothermal aging of an Fe–Mn–Ni alloy

2008 ◽  
Vol 56 (6) ◽  
pp. 1306-1314 ◽  
Author(s):  
Y HEO
2005 ◽  
Vol 475-479 ◽  
pp. 3459-3462
Author(s):  
Hong Bin Wang ◽  
Xiao Yu Wang ◽  
J.H. Zhang ◽  
T.Y. Hsu

The grain growth and mechanical properties of nanograined bulk Fe-25at%Ni alloy prepared by an inert gas condensation and in-situ warm consolidation technique were investigated. About 43% high temperature face-centered-cubic (FCC) phase and 57% low temperature body-centered-cubic (BCC) phase were observed in the sample at room temperature, which was significantly different from that of the corresponding conventional coarse-grained alloy. The in-situ X-ray diffraction results show that the start and the finish temperature of BCC to FCC phase transformation are 450°C and 600°C, respectively. The isothermal grain growth exponent n from t k D D n n ¢ = − 1 0 1 for nanograined single FCC phase Fe-25at%Ni alloy is 0.38 at 750 °C . The mechanical properties changing with the grain size were studied by means of microindentation test.


2016 ◽  
Vol 22 (6) ◽  
pp. 1244-1250 ◽  
Author(s):  
Jingxu Zheng ◽  
Zhongyuan Luo ◽  
Lida Tan ◽  
Bin Chen

AbstractIn the present study, nano-sized cuboid-shaped particles in Mg–Nd–Y are studied by means of Cs-corrected atomic-scale high-angle annular dark-field scanning transmission electron microscopy. The structure of the cuboid-shaped phase is identified to be yttrium (major component) and neodymium atoms in face-centered cubic arrangement without the participation of Mg. The lattice parameter a=5.15 Å. During isothermal aging at 225°C, Mg3(Nd,Y) precipitates adhere to surface (100) planes of the cuboid-shaped particles with the orientation relationship: $[100]_{{{\rm Mg}_{{\rm 3}} {\rm RE}}} \,/\,\,/\,[100]_{{{\rm Cuboid}}} $ and $[310]_{{{\rm Mg}_{{\rm 3}} {\rm RE}}} \,/\,\,/\,[012]_{{{\rm Cuboid}}} $ . The fully coherent interfaces between the precipitates and the cuboid-shaped phases are reconstructed and categorized into two types: $(400)_{{{\rm Mg}_{{\rm 3}} {\rm RE}}} $ interface and $(200)_{{{\rm Mg}_{{\rm 3}} {\rm RE}}} $ interface.


1988 ◽  
Vol 3 (1) ◽  
pp. 40-44 ◽  
Author(s):  
H. M. Ledbetter ◽  
S. A. Kim

This study involved the ultrasonic measurement of the polycrystalline elastic constants of six face-centered-cubic Fe–Cr–Ni alloys, nominally Fe–19Cr–12Ni (at. %). In these alloys, Mo content ranged up to 2.4 at. %. Molybdenum lowers the Young and shear moduli, and it raises the Poisson ratio. Against expectation (because it increases volume), Mo raises the bulk modulus. Qualitatively, the results show that Ni raises the bulk modulus and Poisson ratio; but Ni lowers the Young and shear moduli. (Nickel decreases the alloy's atomic volume.) The discussion includes existing models based on 3d-electron theory.


2009 ◽  
Vol 57 (4) ◽  
pp. 1176-1187 ◽  
Author(s):  
Yoon-Uk Heo ◽  
Masaki Takeguchi ◽  
Kazuo Furuya ◽  
Hu-Chul Lee

Author(s):  
Robert C. Rau ◽  
Robert L. Ladd

Recent studies have shown the presence of voids in several face-centered cubic metals after neutron irradiation at elevated temperatures. These voids were found when the irradiation temperature was above 0.3 Tm where Tm is the absolute melting point, and were ascribed to the agglomeration of lattice vacancies resulting from fast neutron generated displacement cascades. The present paper reports the existence of similar voids in the body-centered cubic metals tungsten and molybdenum.


Author(s):  
F. Monchoux ◽  
A. Rocher ◽  
J.L. Martin

Interphase sliding is an important phenomenon of high temperature plasticity. In order to study the microstructural changes associated with it, as well as its influence on the strain rate dependence on stress and temperature, plane boundaries were obtained by welding together two polycrystals of Cu-Zn alloys having the face centered cubic and body centered cubic structures respectively following the procedure described in (1). These specimens were then deformed in shear along the interface on a creep machine (2) at the same temperature as that of the diffusion treatment so as to avoid any precipitation. The present paper reports observations by conventional and high voltage electron microscopy of the microstructure of both phases, in the vicinity of the phase boundary, after different creep tests corresponding to various deformation conditions.Foils were cut by spark machining out of the bulk samples, 0.2 mm thick. They were then electropolished down to 0.1 mm, after which a hole with thin edges was made in an area including the boundary


Author(s):  
V. N. Filimonenko ◽  
M. H. Richman ◽  
J. Gurland

The high temperatures and pressures that are found in a spark gap during electrical discharging lead to a sharp phase transition and structural transformation in the surface layer of cemented carbides containing WC and cobalt. By means of X-ray diffraction both W2C and a high-temperature monocarbide of tungsten (face-centered cubic) were detected after electro-erosion. The W2C forms as a result of the peritectic reaction, WC → W2C+C. The existence and amount of the phases depend on both the energy of the electro-spark discharge and the cobalt content. In the case of a low-energy discharge (i.e. C=0.01μF, V = 300v), WC(f.c.c.) is generally formed in the surface layer. However, at high energies, (e.g. C=30μF, V = 300v), W2C is formed at the surface in preference to the monocarbide. The phase transformations in the surface layer are retarded by the presence of larger percentages of cobalt.Metallographic examination of the electro-eroded surfaces of cemented carbides was carried out on samples with 5-30% cobalt content. The specimens were first metallographically polished using diamond paste and standard procedures and then subjected to various electrical discharges on a Servomet spark machining device. The samples were then repolished and etched in a 3% NH4OH electrolyte at -0.5 amp/cm2. Two stage plastic-carbon replicas were then made and shadowed with chromium at 27°.


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