Microstructural characterization and oxidation performance of solution-annealed and precipitation hardened wire-arc additively manufactured Inconel 718 superalloys

2022 ◽  
pp. 102602
Author(s):  
G.K. Sujan ◽  
Huijun Li ◽  
Zengxi Pan ◽  
Daniel Liang ◽  
Nazmul Alam
Author(s):  
Wesley A. Tayon ◽  
Ravi N. Shenoy ◽  
MacKenzie R. Redding ◽  
R. Keith Bird ◽  
Robert A. Hafley

Electron beam freeform fabrication (EBF3), a metallic layer-additive manufacturing process, uses a high-power electron beam in conjunction with a metal feed wire to create a molten pool on a substrate, which on solidification produces a component of the desired configuration made of sequentially deposited layers. During the build-up of each solidified layer, the substrate is translated with respect to the electron beam and the feed wire. EBF3 products are similar to conventional cast products with regard to the as-deposited (AD) microstructure and typical mechanical properties. Inconel 718 (IN 718), a high-temperature superalloy with attractive mechanical and oxidation properties well suited for aerospace applications, is typically used in the wrought form. The present study examines the evolution of microstructure, crystallographic texture, and mechanical properties of a block of IN 718 fabricated via the EBF3 process. Specimens extracted out of this block, both in the AD and in a subsequently heat treated (HT) condition, were subjected to (1) microstructural characterization using scanning electron microscopy (SEM); (2) in-plane elastic modulus, tensile strength, and microhardness evaluations; and (3) crystallographic texture characterization using electron backscatter diffraction (EBSD). Salient conclusions stemming from this study are: (1) mechanical properties of the EBF3-processed IN 718 block are strongly affected by texture as evidenced by their dependence on orientation relative to the EBF3 fabrication direction, with the AD EBF3 properties generally being significantly reduced compared to wrought IN 718; (2) significant improvement in both strength and modulus of the EBF3 product to levels nearly equal to those for wrought IN 718 may be achieved through heat treatment.


2020 ◽  
Vol 49 (4) ◽  
pp. 494-509
Author(s):  
Sumit K. Sharma ◽  
K. Biswas ◽  
A. K. Nath ◽  
I. Manna ◽  
J. Dutta Majumdar

MRS Advances ◽  
2020 ◽  
Vol 5 (59-60) ◽  
pp. 3035-3043
Author(s):  
Luis E. Gonzalez A. ◽  
Arnoldo Bedolla-Jacuinde ◽  
Francisco V. Guerra ◽  
A. Ruiz

AbstractThis work analyzes the effect of rare earth additions to an Inconel 718 superalloy; for this purpose, two 8 kg ingots of a commercial composition of Inconel 718 were made in a vacuum induction furnace. One of them (In718) with the base composition and the other one (In718RE) with an addition of 0.04wt% of mischmetal (rare earths alloy based on cerium and lanthanum). Both alloys were cast into metallic molds into the vacuum chamber and let to solidify. The alloys were then solubilized for two hours at 1155 °C to eliminate deleterious phases, rolled at 1100 °C to get a reduction of 50% in thickness, then aged for 16 hours at 720 °C and 620 °C by 8 hours each. A complete microstructural characterization was undertaken by optical and electronic (SEM and TEM) microscopy and X-ray diffraction. Mechanical characterization was done by hardness tests, tensile and Charpy impact tests. Results show a slight improvement of the tensile and hardness values for the alloy with rare earth additions. However, no notorious difference was observed during the impact tests, since both alloys show the same values. These mechanical results are discussed in terms of the obtained microstructure. Both alloys are mainly composed by γ, γ´, γ´´ and carbides. It was observed that primary carbides nucleate rare earth particles; therefore, higher number of carbides and of larger size (according to a size distribution) are observed in the alloy with rare earth additions. The presence of such carbides prevents the grain growth during the thermomechanical processing which in turn improve the mechanical properties.


2020 ◽  
Vol 1012 ◽  
pp. 354-359
Author(s):  
Renato Paulo Rezende ◽  
Mauricio David Martins das Neves

The spacer grids are part of the Fuel Element (FE) set of the PWR (Pressurized Water Reactor) type reactor. These grids maintain the position of the fuel rods within the arrangement of the FE, conserving among them the spacing necessary for the operation of the reactor. The grids are manufactured from the union of the intersecting points of stamped strips of Base Material (BM) Inconel 718, by a joint process called brazing. The addition metal (AM) used consists of a brazing paste based on Ni-Cr-P (nickel-chromium-phosphorus), which is added dropwise in the intersection of grids with a clearance of 0.025 mm. For this purpose, Inconel 718 smooth strips of 0.35 mm thick nickel plated samples were prepared, the AM was added and the vacuum oven was 10-3 mbar, in different time and temperatures. The samples were prepared by metallography and characterized using optical microscopy (OM), scanning electron microscopy (SEM) and mechanical microhardness test. The purpose of this work is to characterize the brazing joint by means evaluate the size of precipitates and the different compounds formed in the joint. It was found different precipitates composed mainly of titanium and niobium. Phosphorus rich phases were found in the brazed region. The mean hardness of the BM was 469 ± 12 HV and in the joint region hardness of 1345 ± 34 HV was found in the lighter phases.


2018 ◽  
Vol 28 (8) ◽  
pp. 1530-1537 ◽  
Author(s):  
Lin-jiang CHAI ◽  
Shan-shan YUAN ◽  
Wei-jiu HUANG ◽  
Xu-sheng YANG ◽  
Fang-jun WANG ◽  
...  

Author(s):  
Madhavrao Govindaraju ◽  
N. Sastry Cheruvu ◽  
Ken Natesan

Nanocrystalline coatings were developed on austenitic alloys to meet the high temperature oxidation and corrosion requirements of the waterwalls and superheater/reheater sections of ultra-supercritical (USC) boilers. Nanocoatings were deposited on 304 stainless steels alloys using Plasma Enhanced Magnetron Sputtering (PEMS) process. Coatings of Fe-18Cr-8Ni-xAl (where x = 0, 4, 10%) were deposited on all 304L steel substrates. The as-deposited Fe-based nano-crystalline coatings exhibited ultra-fine grain structure. The long-term oxidation behavior of nanocrystalline coatings was evaluated through cyclic oxidation tests. The results showed that the fine grain structure improved oxidation resistance, promoted selective oxidation of Cr or Al. High temperature corrosion tests were performed in simulated combustion and gasification environment with and without the presence of deposits such as coal ash, alkali sulfates, and sodium chloride. The weight loss or gain for the exposed samples was measured followed by microstructural characterization. Exposed samples were sectioned and characterized by energy dispersive x-ray analysis to identify the corrosion-product phases in the specimen scales. The results highlighted the importance of bonding between the coating and base alloys to resist the coal ash corrosion. Increasing amount of Al content is required to resist sulfur corrosion. Evaluation of samples tested in flue gas environment with SO2 showed an increase in corrosion resistance with increase in aluminum content in the coating.


Author(s):  
Manuel Guzmán-Tapia ◽  
Gonzalo Mariano Domínguez Almaraz ◽  
Ishvari Fernanda Zúñiga Tello ◽  
Alberto Gutiérrez Martínez ◽  
Julio Cesar Verduzco Juárez

2017 ◽  
Vol 23 (S1) ◽  
pp. 788-789 ◽  
Author(s):  
A. Martinez-Hernandez ◽  
M.T. Santoyo-Arreguin ◽  
O. Vazquez-Gomez ◽  
J.M. Herrera-Ramirez

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