scholarly journals Sodium insertion and de-insertion mechanism of spinel-type sodium titanium oxide studied by in situ XRD

2022 ◽  
Vol 890 ◽  
pp. 161763
Author(s):  
Riki Kataoka ◽  
Toshikatsu Kojima ◽  
Mitsunori Kitta ◽  
Akihiko Machida
Keyword(s):  
Titanium Oxide ◽  
Spinel Type ◽  
In Situ Xrd ◽  
Insertion Mechanism

Zirconium phase transformations observed by “in-situ” XRD analysis

Vacuum ◽  
2012 ◽  
Vol 86 (6) ◽  
pp. 785-788 ◽  
Author(s):  
Jan Riha ◽  
Pavol Sutta ◽  
Andrej Vincze ◽  
Rostislav Medlin
Keyword(s):  
Phase Transformations ◽  
Xrd Analysis ◽  
In Situ Xrd

Evolution of Phase Transformation Behavior in Li(Mn1.5Ni0.5)O4 Cathodes Studied By In Situ XRD

2011 ◽  
Vol 158 (8) ◽  
pp. A890 ◽  
Author(s):  
Kevin Rhodes ◽  
Roberta Meisner ◽  
Yoongu Kim ◽  
Nancy Dudney ◽  
Claus Daniel
Keyword(s):  
Phase Transformation ◽  
Transformation Behavior ◽  
Phase Transformation Behavior ◽  
In Situ Xrd

A flexible lead-free piezoelectric nanogenerator based on vertically aligned BaTiO3 nanotube arrays on a Ti-mesh substrate

RSC Advances ◽  
2016 ◽  
Vol 6 (84) ◽  
pp. 81426-81435 ◽  
Author(s):  
Ermias Libnedengel Tsege ◽  
Gyu Han Kim ◽  
Venkateswarlu Annapureddy ◽  
Beomkeun Kim ◽  
Hyung-Kook Kim ◽  
...  
Keyword(s):  
Low Temperature ◽  
Titanium Oxide ◽  
Hydrothermal Process ◽  
Lead Free ◽  
Nanotube Arrays ◽  
Titanium Oxide Nanotubes ◽  
Vertically Aligned ◽  
Ti Mesh

A novel, flexible lead-free piezoelectric nanogenerator was developed using a uniform BaTiO3 film; synthesized by in situ conversion of titanium oxide nanotubes in a low temperature hydrothermal process.

In Situ X-Ray Diffraction Studies of Crystallization Growth Behavior in ZnO-Bi2O3-B2O3 Glass as a Route to Functional Optical Devices

MRS Advances ◽  
2018 ◽  
Vol 3 (11) ◽  
pp. 563-567 ◽  
Author(s):  
Quentin Altemose ◽  
Katrina Raichle ◽  
Brittani Schnable ◽  
Casey Schwarz ◽  
Myungkoo Kang ◽  
...  
Keyword(s):  
Heat Treatment ◽  
Glass Ceramics ◽  
Treatment Temperature ◽  
Crystal Phase ◽  
X Ray Diffraction ◽  
X Ray ◽  
In Situ Xrd ◽  
Dsc Measurements ◽  
Transmission Window

ABSTRACTTransparent optical ZnO–Bi2O3–B2O3 (ZBB) glass-ceramics were created by the melt quenching technique. In this work, a melt of the glass containing stoichiometric ratios of Zn/Bi/B and As was studied. Differential scanning calorimeter (DSC) measurements was used to measure the thermal behavior. VIS/NIR transmission measurements were used to determine the transmission window. X-ray diffraction (XRD) was used to determine crystal phase. In this study, we explore new techniques and report a detailed study of in-situ XRD of the ZBB composition in order to correlate nucleation temperature, heat treatment temperature, and heat treatment duration with induced crystal phase.

In situ XRD, Raman, and TPR studies of CuO/Al2O3 catalysts for CO oxidation

2005 ◽  
Vol 239 (1-2) ◽  
pp. 243-248 ◽  
Author(s):  
Meng-Fei Luo ◽  
Ping Fang ◽  
Mai He ◽  
Yun-Long Xie
Keyword(s):  
Co Oxidation ◽  
In Situ Xrd

In situ XRD studies of the structural changes of ZrO2-coated LiCoO2 during cycling and their effects on capacity retention in lithium batteries

2006 ◽  
Vol 163 (1) ◽  
pp. 185-190 ◽  
Author(s):  
Kyung Yoon Chung ◽  
Won-Sub Yoon ◽  
Hung Sui Lee ◽  
James McBreen ◽  
Xiao-Qing Yang ◽  
...  
Keyword(s):  
Lithium Batteries ◽  
Structural Changes ◽  
Capacity Retention ◽  
In Situ Xrd ◽  
Xrd Studies

Observation on the Structure of Ordered Mesoporous Materials at High Temperature via In Situ X-Ray Diffraction

2010 ◽  
Vol 132 ◽  
pp. 29-37
Author(s):  
Chun Fang Zhou ◽  
Jian Hua Zhu
Keyword(s):  
High Temperature ◽  
Mesoporous Materials ◽  
Pore Wall ◽  
Short Paper ◽  
Structure Variation ◽  
Ordered Mesoporous Materials ◽  
In Situ Xrd ◽  
Mesoscopic Structure ◽  
Xrd Patterns

This short paper reports the direct observation of the structure variation of mesoporous silica at temperatures higher than 600 oC by use of an in situ XRD technique. The mesostructure of SBA-15 or other mesoporous materials such as MCM-41 became almost invisible when the temperature rose to above 600 oC, but recovered or partially recovered once the temperature decreased. Contrarily, the characteristic XRD patterns of zeolites such as ZSM-5 kept unchangeable under the same conditions. On the basis of comparative experiments performed on various mesoporous samples, it is inferred that the reversible variation of XRD patterns probably originates from the thermal shock of the pore wall, not from the permanent collapse of the mesoscopic structure in these samples. This observation indicates the special features of SBA-15 at high temperature.

Ultra-high vacuum chemical vapor deposition and in situ characterization of titanium oxide thin films

1991 ◽  
Vol 6 (9) ◽  
pp. 1913-1918 ◽  
Author(s):  
Jiong-Ping Lu ◽  
Rishi Raj
Keyword(s):  
Thin Films ◽  
Chemical Vapor Deposition ◽  
Titanium Oxide ◽  
Vapor Deposition ◽  
Photoelectron Spectroscopy ◽  
High Vacuum ◽  
Chemical Vapor ◽  
Titanium Isopropoxide ◽  
Ultra High Vacuum

Chemical vapor deposition (CVD) of titanium oxide films has been performed for the first time under ultra-high vacuum (UHV) conditions. The films were deposited through the pyrolysis reaction of titanium isopropoxide, Ti(OPri)4, and in situ characterized by x-ray photoelectron spectroscopy (XPS) and Auger electron spectroscopy (AES). A small amount of C incorporation was observed during the initial stages of deposition, through the interaction of precursor molecules with the bare Si substrate. Subsequent deposition produces pure and stoichiometric TiO2 films. Si–O bond formation was detected in the film-substrate interface. Deposition rate was found to increase with the substrate temperature. Ultra-high vacuum chemical vapor deposition (UHV-CVD) is especially useful to study the initial stages of the CVD processes, to prepare ultra-thin films, and to investigate the composition of deposited films without the interference from ambient impurities.

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