Digital Light Processing stereolithography of zirconia ceramics: slurry elaboration and orientation-reliant mechanical properties

2022 ◽  
Author(s):  
Bartolomeo Coppola ◽  
Julien Schmitt ◽  
Tanguy Lacondemine ◽  
Caroline Tardivat ◽  
Laura Montanaro ◽  
...  
Keyword(s):  
Mechanical Properties ◽  
Zirconia Ceramics ◽  
Digital Light Processing

scholarly journals Biofabrication of Cell-Laden Gelatin Methacryloyl Hydrogels with Incorporation of Silanized Hydroxyapatite by Visible Light Projection

Polymers ◽  
2021 ◽  
Vol 13 (14) ◽  
pp. 2354
Author(s):  
Jimmy Jiun-Ming Su ◽  
Chih-Hsin Lin ◽  
Hsuan Chen ◽  
Shyh-Yuan Lee ◽  
Yuan-Min Lin
Keyword(s):  
Mechanical Properties ◽  
Visible Light ◽  
3D Structure ◽  
Three Dimensional ◽  
3D Cell Culture ◽  
Composite Hydrogel ◽  
Digital Light Processing ◽  
Mg63 Cells ◽  
Marrow Mesenchymal Stem Cells ◽  
Low Cytotoxicity

Gelatin methacryloyl (GelMA) hydrogel is a photopolymerizable biomaterial widely used for three-dimensional (3D) cell culture due to its high biocompatibility. However, the drawback of GelMA hydrogel is its poor mechanical properties, which may compromise the feasibility of biofabrication techniques. In this study, a cell-laden GelMA composite hydrogel with a combination incorporating silanized hydroxyapatite (Si-HAp) and a simple and harmless visible light crosslinking system for this hydrogel were developed. The incorporation of Si-HAp into the GelMA hydrogel enhanced the mechanical properties of the composite hydrogel. Moreover, the composite hydrogel exhibited low cytotoxicity and promoted the osteogenic gene expression of embedded MG63 cells and Human bone marrow mesenchymal stem cells (hBMSCs). We also established a maskless lithographic method to fabricate a defined 3D structure under visible light by using a digital light processing projector, and the incorporation of Si-HAp increased the resolution of photolithographic hydrogels. The GelMA-Si-HAp composite hydrogel system can serve as an effective biomaterial in bone regeneration.

scholarly journals Mechanical Properties and Biocompatibility of Urethane Acrylate-Based 3D-Printed Denture Base Resin

Polymers ◽  
2021 ◽  
Vol 13 (5) ◽  
pp. 822
Author(s):  
Jy-Jiunn Tzeng ◽  
Tzu-Sen Yang ◽  
Wei-Fang Lee ◽  
Hsuan Chen ◽  
Hung-Ming Chang
Keyword(s):  
Mechanical Properties ◽  
3D Printing ◽  
Flexural Modulus ◽  
Measurement Data ◽  
Uv Exposure ◽  
Control Group ◽  
Urethane Acrylate ◽  
Shore Hardness ◽  
Digital Light Processing ◽  
Denture Base

In this study, five urethane acrylates (UAs), namely aliphatic urethane hexa-acrylate (87A), aromatic urethane hexa-acrylate (88A), aliphatic UA (588), aliphatic urethane triacrylate diluted in 15% HDD (594), and high-functional aliphatic UA (5812), were selected to formulate five UA-based photopolymer resins for digital light processing (DLP)-based 3D printing. Each UA (40 wt%) was added and blended homogenously with ethoxylated pentaerythritol tetraacrylate (40 wt%), isobornyl acrylate (12 wt%), diphenyl (2,4,6-trimethylbenzoyl) phosphine oxide (3 wt%), and a pink acrylic (5 wt%). Each UA-based resin specimen was designed using CAD software and fabricated using a DLP 3D printer to specific dimensions. Characteristics, mechanical properties, and cytotoxicity levels of these designed UA-based resins were investigated and compared with a commercial 3D printing denture base acrylic resin (BB base) control group at different UV exposure times. Shore hardness-measurement data and MTT assays were analyzed using a one-way analysis of variance with Bonferroni’s post hoc test, whereas viscosity, maximum strength, and modulus were analyzed using the Kruskal–Wallis test (α = 0.05). UA-based photopolymer resins with tunable mechanical properties were successfully prepared by replacing the UA materials and the UV exposure times. After 15 min of UV exposure, the 5812 and 594 groups exhibited higher viscosities, whereas the 88A and 87A groups exhibited lower viscosities compared with the BB base group. Maximum flexural strength, flexural modulus, and Shore hardness values also revealed significant differences among materials (p < 0.001). Based on MTT assay results, the UA-based photopolymer resins were nontoxic. In the present study, mechanical properties of the designed photopolymer resins could be adjusted by changing the UA or UV exposure time, suggesting that aliphatic urethane acrylate has good potential for use in the design of printable resins for DLP-type 3D printing in dental applications.

scholarly journals Mechanical properties of ultra-fine grained zirconia ceramics

1992 ◽  
Vol 27 (16) ◽  
pp. 4429-4438 ◽  
Author(s):  
G. S. A. M. Theunissen ◽  
J. S. Bouma ◽  
A. J. A. Winnubst ◽  
A. J. Burggraaf
Keyword(s):  
Mechanical Properties ◽  
Zirconia Ceramics ◽  
Fine Grained

Mechanical properties of Nd2O3/Y2O3-coated zirconia ceramics

2004 ◽  
Vol 374 (1-2) ◽  
pp. 239-243 ◽  
Author(s):  
Tao Xu ◽  
Jef Vleugels ◽  
Omer Van der Biest ◽  
Peiling Wang
Keyword(s):  
Mechanical Properties ◽  
Zirconia Ceramics

Novel Baddeleyite-Based Zirconia Ceramics for Biomedical Applications

2017 ◽  
Vol 13 ◽  
pp. 9-14
Author(s):  
Alexander I. Tyurin ◽  
Andrey O. Zhigachev ◽  
Alexey V. Umrikhin ◽  
Vyacheslav V. Rodaev ◽  
Tatyana S. Pirozhkova
Keyword(s):  
Mechanical Properties ◽  
Fracture Toughness ◽  
Tetragonal Phase ◽  
Biomedical Applications ◽  
Zirconia Ceramics ◽  
Engineering Ceramics ◽  
Synthesis Conditions ◽  
Microstructure And Mechanical Properties ◽  
First Time

For the first time nanostructured engineering ceramics were prepared from natural zirconia mineral (baddeleyite) with CaO as a tetragonal phase stabilizer. The effect of synthesis conditions on microstructure and mechanical properties of the baddeleyite-based ceramics is reported, furthermore, the effect of calcia content on hardness and fracture toughness is studied. Optimal calcia concentration and synthesis conditions are found, corresponding hardness and fracture toughness values are 10,8 GPa and 13,3 MPa×m1/2. The reported mechanical properties are comparable to those typically reported for yttria-stabilized engineering zirconia ceramics, prepared from chemically synthesized zirconia.

scholarly journals Mechanical Properties of Zirconia Ceramics at Low Temperature

1990 ◽  
Vol 98 (1142) ◽  
pp. 1132-1138 ◽  
Author(s):  
Kazunori JIKIHARA ◽  
Mamoru ISHIHARA
Keyword(s):  
Mechanical Properties ◽  
Low Temperature ◽  
Zirconia Ceramics

Mechanical Properties of Dental Zirconia Ceramics Changed with Sandblasting and Heat Treatment

2008 ◽  
Vol 27 (3) ◽  
pp. 408-414 ◽  
Author(s):  
Hideo SATO ◽  
Kiyotaka YAMADA ◽  
Giuseppe PEZZOTTI ◽  
Masahiro NAWA ◽  
Seiji BAN
Keyword(s):  
Mechanical Properties ◽  
Heat Treatment ◽  
Zirconia Ceramics ◽  
Dental Zirconia Ceramics

Influence of Silica and Alumina Doping on the Microstructure and the Mechanical Properties of Zirconia Ceramics Used for Joint Prostheses Applications

2001 ◽  
Vol 206-213 ◽  
pp. 1633-1636
Author(s):  
Laurent Gremillard ◽  
Anne Claire Bruneau ◽  
Jérôme Chevalier ◽  
Thierry Epicier ◽  
Gilbert Fantozzi
Keyword(s):  
Mechanical Properties ◽  
Zirconia Ceramics ◽  
Joint Prostheses

Effect of small amount of alumina on structure, wear and mechanical properties of 3Y-TZP ceramics

2014 ◽  
Vol 11 (1) ◽  
pp. 9-16 ◽  
Author(s):  
Igor Danilenko ◽  
Serhii Prokhorenko ◽  
Tetyana Konstantinova ◽  
Leonid Ahkozov ◽  
Valerii Burkhovetski ◽  
...  
Keyword(s):  
Mechanical Properties ◽  
Fracture Toughness ◽  
Composite Structures ◽  
Tribological Behavior ◽  
Ceramic Composites ◽  
Synthesis Methods ◽  
Zirconia Ceramics ◽  
Alumina Composites ◽  
Co Precipitation ◽  
Metallic Parts

The use of ceramic instead of metallic parts in devices that operate in aggressive conditions increases the service life of machines and equipment for chemical, metallurgical and other industries. The wear resistant zirconia/alumina composites were sintered from nanopowders obtained by co-precipitation technique. In the case of addition of 1wt% of alumina in zirconia ceramics the wear resistance increased by approximately 30%.The formation of complex multilevel composite structures, such as Al3+ ion segregation on zirconia grain boundaries and intracrystalline alumina inclusions in zirconia grains, increased the fracture toughness values of composites obtained from co-precipitated nanopowders and consequently decreased the volume loss of ceramic material.In this study, we investigated the effect of nanopowders synthesis methods and alumina concentration on composite structure, fracture toughness and tribological behavior of 3Y-TZP/alumina ceramic composites and searched correlation between structures and mechanical properties.

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