Effect of sintering temperature and holding time on the microstructure and mechanical properties of ZrB2–SiCw composites

2009 ◽  
Vol 116 (1) ◽  
pp. 76-80 ◽  
Author(s):  
Shanyi Du ◽  
Lin Xu ◽  
Xinghong Zhang ◽  
Ping Hu ◽  
Wenbo Han
Materials ◽  
2020 ◽  
Vol 13 (18) ◽  
pp. 3938
Author(s):  
Kaixun Ji ◽  
Yanxin Meng ◽  
Fuzeng Wang ◽  
Yousheng Li

In this study, a Ti(C,N)-based cermet material was prepared through vacuum sintering. The research also investigates how holding time and maximum sintering temperature influence the material microstructure and mechanical properties. X-ray diffraction (XRD), energy dispersive spectroscopy (EDS) were used to analyze the composition of the cermet. The microstructure of the cermet was analyzed and examined using a scanning electron microscope (SEM). A Vickers hardness tester was used to test the mechanical properties of the materials. As indicated by testing results, the hardness of the material decreases as the temperature of sintering increases, and its fracture toughness increases gradually as holding time increases. Ti(C,N)-based cermet manifested the optimal mechanical properties when sintering was conducted under 1400 °C with 80 min of holding time. Moreover, the material microstructure is significantly affected by the sintering process. The grain size of Ti(C,N) cermets increases as the sintering temperature increases. The microstructure tends to be uniform and the complete core-rim structures are established as the holding time increases.


Crystals ◽  
2021 ◽  
Vol 11 (4) ◽  
pp. 422
Author(s):  
Kuai Zhang ◽  
Yungang Li ◽  
Hongyan Yan ◽  
Chuang Wang ◽  
Hui Li ◽  
...  

An Fe/FeAl2O4 composite was prepared with Fe-Fe2O3-Al2O3 powder by a hot press sintering method. The mass ratio was 6:1:2, sintering pressure was 30 MPa, and holding time was 120 min. The raw materials for the powder particles were respectively 1 µm (Fe), 0.5 µm (Fe2O3), and 1 µm (Al2O3) in diameter. The effect of sintering temperature on the microstructure and mechanical properties of Fe/FeAl2O4 composite was studied. The results showed that Fe/FeAl2O4 composite was formed by in situ reaction at 1300 °C–1500 °C. With the increased sintering temperature, the microstructure and mechanical properties of the Fe/FeAl2O4 composite showed a change law that initially became better and then became worse. The best microstructure and optimal mechanical properties were obtained at 1400 °C. At this temperature, the grain size of Fe and FeAl2O4 phases in Fe/FeAl2O4 composite was uniform, the relative density was 96.7%, and the Vickers hardness and bending strength were 1.88 GPa and 280.0 MPa, respectively. The wettability between Fe and FeAl2O4 was enhanced with increased sintering temperature. And then the densification process was accelerated. Finally, the microstructure and mechanical properties of the Fe/FeAl2O4 composite were improved.


2013 ◽  
Vol 589-590 ◽  
pp. 572-577 ◽  
Author(s):  
Hua He Liu ◽  
Han Lian Liu ◽  
Chuan Zhen Huang ◽  
Bin Zou ◽  
Ya Cong Chai

Al2O3-MgO, Al2O3-Y2O3 and Al2O3-MgO-Y2O3 composite ceramics were fabricated respectively by hot-press sintering technique. With the analysis of the mechanical properties and microstructure, it was found that single additive MgO could be more favorable to the grains’ refinement and densification than Y2O3; the composite additive including both MgO and Y2O3 was better than single additive MgO or Y2O3, because their interactions could improve the mechanical properties of the Al2O3 ceramics; The sintering temperature could be reduced by adding the suitable amount of composite additives.


2007 ◽  
Vol 46 (9-10) ◽  
pp. 449-453 ◽  
Author(s):  
Yonglin Yan ◽  
Yong Zheng ◽  
Haijun Yu ◽  
Haijian Bu ◽  
Xin Cheng ◽  
...  

Author(s):  
I Aatthisugan ◽  
Aishik Banerjee ◽  
Mohammed Moinuddin Hasan ◽  
Aditya Singh Patel ◽  
Kumar Pushkar ◽  
...  

2013 ◽  
Vol 750-752 ◽  
pp. 687-690 ◽  
Author(s):  
Su Zhang ◽  
Gang Yang ◽  
Jian Hong Yi ◽  
Hong Yan

Effects of the holding time and the stirring time on the microstructure and mechanical properties of A356 alloy modified by Sc are researched. According to the test results, most of the eutectic silicon phases have changed to the shape of creeping point, dispersed in the grain boundary of α (Al) phase while stirring 1 minute, in which case both the tensile strength and elongation reach the highest, resulting in the best modification effect. The results also indicate that microstructure and mechanical properties of the alloy reach are the best modification effect when the melt is held 15 minute. It can be known that the optimal stirring time is 1 minute and the optimal holding time is 15 minute in the experiment condition of the work.


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